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It was found that,under comparable conditions,the rate of formation of N-carbobenzoxy-L-serine anilide is the...

在最适pH,酶浓度自1.31毫克蛋白N/毫升反应液提高到2.27毫克蛋白N/毫升反应液时,N-苯甲氧羰酰-L-丝氨酸酰苯胺的产率,在24小时自76.43%提高到100%。

Anisaldehyde was synthesized from p-hydroxybenzaldehyde with dimethyl carbonate by microwave irradiation under phase transfer catalyst tetrabutylammonium bromide, The effect of power, time, solvent and catalyst of reaction on yield were researched.

以四丁基溴化铵为相转移催化剂,采用对羟基苯甲醛和碳酸二甲酯为原料,微波辐射下合成大茴香醛。考察了反应溶剂、功率、时间和催化剂对反应产率的影响。

After comparison of 30 and 50℃ treatments, AQDS were added into 3 kinds of microorganism biocoenosis from Jiling, Tianjin and Sichuan paddy soil, and it showed that AQDS could accelerate the reduction of Fe 10%-288%, meanwhile, temperature could accelerate the reduction of Fe 6%-17%. In axenic culture treatment of 6 kinds of bacterial strains from Sichuan and Jiangxi paddy soil, the maximum accumulation amount of Fe reduction rate was constant, the maximum reaction rate and ferric reduction rate of ferric strain JX-a08 all increased as temperature rose, which showed that bacterial strain JX-a08 were suitable to 50℃.

在30和50℃培养温度下,来源于吉林、天津和四川的3种水稻土微生物群落添加AQDS可使Fe还原的反应速率常数增加10%~288%,而温度变化的增加幅度仅为6%~17%;对分离自四川和江西水稻土中的6株铁还原菌的纯培养试验发现,菌株JX-a08的Fe最大累积量、还原速率常数、最大反应速率及铁还原率均随培养温度的升高明显增加,表明菌株JX-a08更适于在50℃下生长。

Under different conditions, acetic acid conversion and the yield of butyl acetate were close or reached to 100% in a short operating time.

在不同反应条件下,较短的反应时间内,乙酸的转化率、乙酸正丁酯的产率都能接近或达到100%。

By means of GC, GC-MS, GC-IR, IR, H1-NMR,the reaction products were investigated and the results showed that there are camphene, limoneneN terpinolene, Me a -fenchyl ether, Me -terpinyl ether, Me bornyl ether and Me isobornyl ether containing in the products,and the content of the main product Me a -terpinyl ether is up to 42.5%,the selectivity is 44.7%.

采用GC、GC-IR、GC-MS、IR、H~1-NMR等对反应产物进行定量和定性分析,结果表明:微波辐射下α-蒎烯与甲醇的反应产物含有莰烯、柠檬烯、α-小茴香甲醚、异松油烯、异菠基甲醚、菠基甲醚、α-松油基甲醚等,在较好的工艺条件下,主产物α-松油基甲醚的得率为42.5%,选择性为44.7%。

Under optimum conditions, the yield of nitration of chlorobenzene was 70%, and para-selectivity was 85%.

研究表明,在最佳反应条件下,氯苯硝化反应得率达到70%,对位选择性为85%。

The 〓 of the used reverse micelles was optimized.The results demonstrated that the isolated yield could reach 86% when 〓=6, 400μmol/1 α-chymotrypsin in the water pool and stirring for 24 hours.

实验结果表明,当反相胶束体系的〓值为6,反应时间为24h,内核水池中酶的浓度为400μmol/1时,反应产率可以达到86%。

The investigation of the catalytic activity and stereoselectivity of ligand 10 was also carried out under another standard set of K〓Fe 〓 conditions (〓/ligand/substrate=0.002: 0.01: 1). The AD reaction of seven olefins gave corresponding diols in 72~99% yield (except for ethyl cinnamate, 48%) and 91~99% ees, which was comparable to those obtained from the reactions using the commercial ligand 〓PHAL.

将单季铵盐手性配体10用于AD反应的另一个催化体系〓BuOH-H〓O/K〓Fe〓中考察其催化活性和立体选择性,在七种烯烃的AD反应中,〓、配体与底物的摩尔比为0.002:0.01:1时,化学产率为72~99%(肉桂酸乙酯除外,为48%),ee值为91~99.9%,与商品配体〓PHAL的催化结果相当。

The influence of sintering time and sintering temperature on the crystalline structure of cordierite synthesized from waste aluminum sludge was studied in this paper.

本研究主要探讨反应温度和反应时间对铝型材厂工业污泥合成堇青石材料的得率和晶相结构的影响。

During a reactor startup, the first reactivity addition caused the count rate to increase

在一反应炉启动时,第一次反应度添加导致计数率从20增加至40cps。

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