反应率

Leuco crystal violet lactone was prepared by heating the mixture of dimethylaniline, p- dimethylaminobenzaldehyde and m- dimethylaminobenzoic acid at 60 ℃ for 5 hours in presence of hydrochioric acid and unea and in the nitrogen atmosphere with 72% yield of LCVL.

等摩尔比的N，N-二甲基苯胺和对二甲氨基苯甲醛在盐酸和脲的存在及氮气保护下，80℃反应0.5h，加入间二甲氨基苯甲酸于90℃反应5h。将反应混合物中和，抽滤，得到无色结晶紫内酯，产率为72%。

Leuco crystal violet lactone was prepared by heating the mixture of dimethylaniline, p-dimethylaminobenzaldehyde and m-dimethylaminobenzoic acid at 60℃ for 5 hours in presence of hydrochloric acid and urea and in the nitrogen atmosphere with 72%yield of LCVL.

等摩尔比的N，N-二甲基苯胺和对二甲氨基苯甲醛在盐酸和脲的存在及氮气保护下，80℃反应0.5h，加入间二甲氨基苯甲酸于90℃反应5h。将反应混合物中和，抽滤，得到无色结晶紫内酯，产率为72%。

The n-butyl lactate was synthesied by the esterification of lactic acid and n-butyl alcohol in presence of ammonium ferric sulfate dodecahydrate NH4Fe(SO4)212H2O,and the factor influencing on the yield of reaction were discussed.

摘 要：在十二水合硫酸铁铵催化下，由乳酸和正丁醇发生酯化反应合成了乳酸正丁酯。实验考察了该催化剂催化酯化合成乳酸正丁酯的醇酸比、催化剂用量、反应时间、反应温度诸因素对酯化率的影响。

Thirdly,in the view of some different results between the reaction of complexes(2)、(3)and[(Me_3Si)_2N]_3LnLi_3 with aromatic aldehydes, the reaction of 2 equiv of aromatic aldehydes with 1 equiv of lithium amide(1) catalyzed by the YCl_3 was subsequently studied,and better yields of the corresponding amides and alcohols can be isolated.These results indicated that the enolate ligand in complexes(2)、(3)may have impact on the Cannizzaro disproportionation reaction.

第三，鉴于上述配合物2、3和[(Me_3Si_2)2_N]_3LnLi_3与芳香醛反应结果上的一些差别，我们又以三氯化钇为催化剂，将两当量的芳香醛与一当量化合物1的锂盐直接进行反应，结果以较好的产率得到了相应的酰胺和醇，这说明配合物2、3中所含的乙烯醇基可能对此Cannizzaro-型歧化反应存在一定的影响。

Considering the effect of m any factors when the reaction reaches balance, and in order to increase t he rate of the product, the rate of the changing of sulfate dimthyle, we det ermined the best condition at last. The temperature is between 80 ℃ and 90 ℃. The for mula of the materials is 3∶1～4∶1.The time of reaction is between 4 and 5 hour s.

考虑反应达平衡时诸多因素的影响以及有利于提高产品的产率、硫酸二甲酯的转化率等问题，最后确定了最佳条件：反应温度为80～90 ℃之间，原料配比为3∶1～4∶1，反应时间为4～5 h。

Through changing various conditions, the conversion of polymerization was determined gravimetrically by sampling with an injector at different time in the course of polymerization system and it was found that conversion was increased linearly firstly and non-linearly finally along with reaction time.

通过改变单一聚合条件，在不同反应时间，利用注射器进行取样，称重法测定聚合物转化率，考察聚合条件的影响，说明此合成体系受单体/引发剂、催化体系、聚合温度、反应时间等因素的影响(如聚合温度90℃，反应时间12h时，产率可达90%以上)。

Butyl bromide was synthesized from hydrobromic acid(48%) and 2-butylalcohol by adding concentrated sulfuric acid.

以质量分数为48%的氢溴酸水溶液、仲丁醇为反应原料，浓硫酸为催化剂合成仲溴丁烷，考察了反应原料和催化剂用量以及反应时间对产率的影响。

Isoamyl isovalerate was synthesized through esterification reaction by using isovaleric acid and isoamyl alcohol as raw materials and nano-H4SiW12O40/SiO2 as catalyst, the influencing factors in the reaction were studied, and the results showed that the esterification rate could reach 98.6 % under the conditions of the ratio of alcohol-acid 1.4∶1, the use level of catalyst 5 %, and the reaction time 1.5 h.

以纳米复合钨硅杂多酸为催化剂，异戊酸和异戊醇为原料，通过酯化反应合成苹果油，对酯化反应的影响因素进行了研究，结果表明，在醇酸物质的量比为1.4∶1，催化剂用量5%，反应时间1.5h的条件下，酯化率可达98.6%。

The optimal technological parameters of oil transesterification from Kosteletzkya virginica oil should be as follows: the rate of rotation 1800r.min-1, catalyst dosage 0.6%, mole ratio of methanol to Kosteletzkya virginica oil 6/1,reaction time 60min and reaction temperature 65℃, and under such conditions, the total oil transesterification ratio after transesterification three times is 97.8%.

海滨锦葵油制备生物柴油的最佳工艺参数为：搅拌强度为1800r.min-1，催化剂KOH用量为海滨锦葵油质量的1%，醇油摩尔比6/1，反应时间60min，反应温度65℃，在该工艺条件下，酯交换反应三次，酯交换率达到97.8%。

To avoid the low yield in direct hydrosilylation addition of allyamine, 1, 1, 1, 3, 3, 3-hexamethyldisilazane is used to protect the amino groups, and the protective groups are removed easily after hydrosilylation addition, then the high yield of ladderlike copolymethyl-aminpropylsilsesquioxane was obtained.

为了克服将烯丙基胺直接与聚氢基甲基倍半硅氧烷进行硅氢加成反应接枝效率低的缺点，探索用六甲基二硅氮烷对烯丙基胺预保护，硅氢加成反应后再脱保护，从而以较高产率制备了含胺丙基、甲基的反应性梯形共聚倍半硅氧烷。

In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国，慢性酒精中毒，肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题，你可以随时联系我。