反应物

A phosphorus-containing triazine oligomer was synthesized from triethyl phosphite, cyanuric chloride ,pentaerythritol and morpholine through three steps.

以亚磷酸三乙酯、三聚氰氯、季戊四醇和吗啉为原料，经3步反应合成了含磷三嗪环低聚物，考察了反应条件对中间体及产物收率的影响，对中间体及产物的结构和热性能进行了表征。

By following the "self-assisted molecular editing" protocol first established in our labs,a number of Aphos ligands were efficiently prepared from a single starting material and they were screened for catalytic efficacy, leading to the discovery of the best-performing Aphos appended with a 3-nitrophenyl group at the C4 position.Combination of this Aphos with Pd_2 offers a precatalyst for successful cross-coupling of unactivated aryl chlorides with aryl boronic acids at room temperature.The reactions took place under mild basic conditions to produce the products in high yields.

通过我们首次提出的&自助分子剪裁&的概念从单一起始物快速合成和筛选了一系列膦配体，并发现C4位含3-硝基苯基的的膦配体和醋酸钯联用可以在室温下顺利地催化不活泼氯代芳烃和芳基硼酸的偶联反应，反应条件温和且产物收率很高。

Therefore, early reactions to an affect-laden stimulus (e.g., a smiling man) are cognitively unappraised and thus diffuse (e.g.,"positive"), whereas later affective reactions can be more specific and distinct (e.g.,"a smiling man").

所以，对一个承载感情讯息的刺激物之初始反应在认知上未被体悟，因而发生弥漫，反而，稍后的情感性反应则可以是更加明确和区别性的（例如，「一个微笑的男人」）。

The initiation temperature of the exotherm of P was little influenced by the atmosphere, however, distinctly decreased with the enhancement of IA content in the copolymer, which implied that the initiation of nitrile cyclization reaction preceded the onset of oxidation reaction through an ionic mechanism.

P共聚物的放热峰起始温度受气氛影响不大，却随着IA含量的增加而明显降低，表明在热稳定化过程中它可能首先以离子机理发生氰基环化反应，再发生氧化反应。

The labelled conjugates were stable in aqueous solution and serum solution in vitro, but they were not stable when challenged with cysteine and in vivo.

实验结果表明，标记物在反应溶液和小牛血清中较稳定，但在与半胱氨酸的竞争反应中及在生物体内的稳定性较差。

Especially, chiral metal complexes and organo-catalysts in combination with electrophilic fluorinating reagents have found applications to the synthesis of a variety of chiral fluoroorganic compounds.

特别是，手性金属配合物和有机催化剂诱导的不对称催化氟化反应被广泛应用于各类手性氟化物的合成，已成为不对称氟化反应研究的热点。

According to the Box-Benhnken design principle,the method of response surface method with 3 factors and 3 levels was used. The factors influencing the technological parameters were determined by means of regression analysis. Response surfaces were finally graphed with the yield as the response value. The synthesis conditions were optimized as follows:reaction reagent was NBS,stoichiometric proportion between NBS and anhydrovinblastine was 1.07; the dosage of TFA was 22 mL/L; reaction temperature was －68 ℃ and duration was 90 min.

在单因素实验基础上，根据Box-Benhnken实验设计原理，采用三因素三水平的响应面分析法，研究了各个因素及其交互作用后，得到了合成7′-Br-脱水长春碱的最佳工艺条件：以二氯甲烷为溶剂，采用NBS为溴代剂，其用量与底物的物质的量比为1.07∶1，TFA的加入量22 mL/L，在－68 ℃下反应90 min，终止反应后，得到卤代产物。

The total reaction could be explained by two steps.The first was a fast pre-equilibrium,activation nitrating reagent transferred to the catalyst.

反应共分两部进行：第一步是快速的预平衡步骤，活性硝化剂转移至催化剂上；第二步是缓慢的速率控制步骤，粘结在催化剂上的活性硝化进攻试剂与底物反应生成目标产物。

The reaction showed 0 order with overfeeding of substrate-penicillin.

该酶在过量青霉素底物下，酶促反应为0级反应。

Part I, the Friedel-Crafts acylation on DAA and methyl dehydroabietic acid was carried out with acetyl chloride, benzoyl chloride or phthalic anhydride as acylating regents, anh- ydrous aluminum chloride as catalyst and with different solvents to compare with, we have got t- hree new compounds.

第一部分，分别以脱氢松香酸和脱氢松香酸甲酯为底物，乙酰氯、苯甲酰氯、邻苯二甲酸酐为酰化试剂，无水三氯化铝作催化剂，采用不同的溶剂及反应条件进行傅克酰基化反应，得到3个新化合物。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。