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High molecular weight polymer Ⅰ and Ⅱ with decomposition temperature of 560℃ were prepared from condensation of two diamine and terephthaloyl chloride respectively.

两种二胺分别与对苯二甲酰氯进行直接缩聚反应,得到的聚合物分别为缩聚物Ⅰ和Ⅱ,两种缩聚物的热分解温度均超过560℃。

The influence of these complexes on the hydrolysis of dipeptide was investigated using 1H NMR techniques.

制备了它们与Pd形成的配合物,并研究了这些配合物促进下的二肽水解反应动力学。

Stable pharmaceutical compositions containing 8-chloro-6,11-dihydro-11-(4-piperidylidene)-5H-benzo[5,6] cycloheptic [1,2-b] pyridine and a DCL protective amount of a pharmaceutically acceptable basic salt such as calcium dibasic phosphate and an amount of at least one disintegrant, preferably two disintegrates such as microcrystalline cellulose and starch sufficient to provide dissolution of at least about 80% by weight of the pharmaceutical composition in about 45 minutes and suitable for oral administration to treat allergic reactions in mammals such as man are disclosed.

本发明公开了含有8-氯-6,11-二氢-11-(4-亚哌啶基)-5H-苯并[5,6]环庚三烯并[1,2-b]吡啶和DCL保护量的可药用碱性盐如磷酸氢钙以及其含量足以使至少约80%的药物组合物在约45分钟内溶解的至少一种崩解剂、优选两种崩解剂如微晶纤维素和淀粉并且适于口服给药以治疗哺乳动物、例如人的过敏反应的稳定的药物组合物。

The rate constants and IC50 values of the dismutation of O2 catalyzed by these complexes have been determined by riboflavin-nitroblue tetrazolium illumination method.

采用核黄素-NBT光照法测定了配合物催化O_2~-歧化的反应速率常数K_Q以及IC_(50)值。结果表明,七种配合物具有相当好的SOD活性,它们的K_Q和IC_(50)值分别在4.08×10~6-1.65×10~7'mol·L~(-1)s~(-1)和1.42×10~(-6)-2.93×10~(-7)mol·L~(-1)范围之内。

One is a bimodal volcanic assemblage, which formed during the rifting stage of the continental breakup theother is represented by flysch rocks, formed when the passive margin becomes stable. The composition of mafic rocks in the volcanic margin reflect their mantle origin and their crustal contamination. High temperature and low-pressure metamorphism can occur during the rifting stage and reflects a temporal trend of increasing temperature and decreasing pressure during the continental breakup.

被动陆缘的沉积建造由两套沉积物组成,一套是大陆解体的裂谷阶段所形成的陆相沉积物和双模式火山岩组合,另一套是稳定陆缘的复理石组合;岩装作用中基性岩类反应了物质直接源于上地慢的主要特点,并有部分受到地壳混染的特征;变质作用中高温低压环境主要发生在裂谷作用阶段,其特点反映了大陆解体过程中随着时间的增温和减压过程,而拆离伸展阶段则被脆性变形所代替。

The RAPD system of Gladiolus was optimized. Of the 12 random primers analyzed in this research, 9 primers can show steady and polymorphic amplification profiles.

建立了适用于唐菖蒲RAPD分子标记的反应体系,从12条随机引物中筛选出9条可扩增出多态性条带的引物。

The level of tumor necrosis factore alpha, interleukin-6 (IL-6) and interleukin-8 (IL-8) were evaluated using ELISA method. Western blotting was used to detect the protein expression of protein kinase B and lipid phosphatase PTEN. Immunoprecipitations and radioactivity of γ〓P incorporated into its specific substrate histon H〓B was utilized to determine the PKB activation. Phosphate concentration released from PTEN-specific substrat diC16PIP3 was assessed using green reagent method.

以细胞计数、噻唑蓝比色法测定细胞增殖能力,酶联免疫法检测培养上清液中细胞因子TNFα、IL-6、IL-8水平,Western免疫印记定量蛋白激酶B、蛋白磷酸酶PTEN表达水平,免疫沉淀、特异底物组蛋白H2Bγ〓P掺入量测定PKB活性,特异底物dic16PIP3脱磷酸绿色试剂法反应PTEN活性。

Under the condition of reaction system developed, primers designed specific to ESTs were screened against genomic DNA of inbreed line A from which the cDNA library was constructed. Among them, 18 pairs of primers showed the amplification.

在此反应体系下,以构建EST的白菜自交系A的DNA为模板,对设计的引物进行了筛选,发现有18对引物能对白菜DNA扩增出产物。

The substituted half-sandwich titaconece with bulky alkoxyl group [CpTiC1〓 or CpTi 〓] or indene ring can not be fluorinated by BF〓·Et〓O under the selected condition, but still coordinates with the BF〓, this coordination then enhances the steric effect that stabilizes the precursor and hinders the reduction of the Ti to the Ti species, reflected in the decrease in polymerization activity.

但是这个转化受主催化剂分子的空间位阻和聚合反应温度的影响,当主催化剂为大位阻的烷氧基取代茂钛络合物或茚钛络合物时,在一般的聚合温度下BF〓不能对它们进行氟化,但可以和其中的OR配位,这种配位进一步加剧了空间位阻,从而阻碍了活性中心的形成,导致催化活性的下降。

It is proved that the electrochemical reaction of the Be〓 complex is irreversible process, and the equation of electrode reaction had been proposed.

讨论了络合物的伏安行为,认为络合物的氧化是一不可逆吸附波,写出了可能的电极反应式。

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