反应作用

It has been observed that pyrocatechol and m-phenylenediamin can sensitively inhibit the discoloration of neutral red oxidation by the H2O2 and in the presence of catalyzer Fe in dilute sulfuric acid solution but the inhibitory effects of two organic compounds can not be added. Based on this research, the advantages of artificial neural network were adopted to handle the experimental data and a new inhibitory kinetic spectrophotometry of simultaneous determination for pyrocatechol and m-phenylenediamin with artificial neural networks was established.

在硫酸性介质中，Fe能够催化H2O2氧化中性红褪色反应，邻苯二酚和间苯二胺都能阻抑该催化氧化褪色反应的速度，研究发现：两者对Fe催化H2O2氧化中性红褪色反应阻抑作用不具有加和性，根据这一现象，用人工神经网络处理非线性体系的优势进行数据处理，从而建立了一种新的测定邻苯二酚和间苯二胺混合物的人工神经网络阻抑动力学光度法。

ResultsPe Min Kam Wan, Lam Kam Sang Nasalin and Wo Chun Tong clearly inhibited PCA in mice and reduced histamine release from rat mast cells induced by compound 48/80. But,Sinuwell did not affect the PCA. In addition, the ethanol extracts from Senecio scandens, Selaginella tamariscina and Xanthium sibiricum significantly inhibited PCA in mice, but the extracts from Angelica dahurica, Magnolia liliflora and Cassia tora failed to affect it.

结果速效鼻敏感丸、林金生鼻敏清胶囊及和春堂鼻敏清片明显抑制小鼠异种被动皮肤过敏反应，减少compound 48/80诱导的组胺释放，而速效鼻敏素胶囊对被动皮肤过敏反应无明显影响；速效鼻敏感丸及和春堂鼻敏清片主要组成药物九里明、卷柏和苍耳子显著抑制小鼠异种被动皮肤过敏反应，而白芷、辛夷和决明子无明显作用。

Some approved aneugens Trip terygiuwlIypogaucum (evelHutch, colchicine, thiabendazole, a tropine sulfate,d-ubocurarine was added into the reactive system respectively and the changes of their absorption values were taken down during different periods under the conditions of 37 0C and 350nm .

本研究通过多步聚合和解聚合反应从猪脑中分离纯化微管蛋白，建立微管蛋白的体外聚合和解聚合反应平衡体系，并将已证实的非整倍体诱发剂（昆明山海棠根部水抽提物、2-（4′-噻唑）苯丙咪唑、硫酸阿托品、d-筒箭毒碱）分别加入此反应平衡体系中，于37℃、350nm条件下，记录此体系不同时期的吸光值变化，与阳性对照物和溶剂对照处理平衡体系后的吸光值在相同时间点作比较，以此评估这几类非整倍体诱发剂对离体条件下的微管蛋白聚合的影响，寻求这几类非整倍体诱发剂是否可通过抑制微管蛋白聚合作用途径而诱发非整倍体。

The novel vacuum furnace is employed in laboratory study. Compared with atmosphere magnesium carbothermic reduction furnace, this new one has the merits of high automation, easy manipulation and fine safety. Vacuum coking, vacuum carbothermic reduction process and magnesium vapory condensation process can be carried out in a furnace.

小型实验结果证明：还原温度升高，还原时间延长，氧化镁还原率增大，添加适量的氟化物对还原反应有促进作用；还原过程中真空度随时间的变化具有规律性，由此可以判断还原反应进行的速度与程度；真空中煤还原氧化镁的条件是：配料时保证C：MgO=3：1，并加入占总料重10％的氟化钙作为催化剂，尽可能的提高反应温度至1500℃以上，保温30～40分钟。

Based on reviewing the banking reform experience of Eastern European countries, we propose seven propositions on China's banking sector reform and empirically vitrify seven propositions using data from 21 banks between 1999 and 2006 ,then draw final conclusions: foreign banks entry lower the profit rate of hosting country banking industry in short-term, improve host country banking's risk management skills

本文在综述东欧国家银行业改革经验的基础上提出中国银行业改革的七个命题，并用中国24家银行1999-2006年间的数据构建模型进行检验，最后得出结论：短期内外资银行进入导致东道国银行业利润水平下降、风险管理水平上升，在中国的背景下可以认定这是外资银行积极作用开始发挥；外资银行机构数量的增加和持股比重的上升都能刺激中国银行业效率的改进，但是外资银行持股比重的影响更具普遍性；不同类型银行对外资银行进入的反应存在差异，国有商业银行反应比较迟钝而股份制和城市商业银行反应比较迅速。

In the field of visible photosensitive resin, the absorption spectrum, excited state, solvent polarity effect, fluorescence spectrum, fluorescence quenching, concentration effect, photo fading, reaction mechanism as well as photopolymerization kinetics of xanthene iodonium salts and cyanine dye-borate were discussed. It is found that under the radiation of visible light, intra-ion-pair electron transfer reactions occur in bis salt of fluorescein and unsymmetrical trimethine cyanines containing quinoline end group triphenyl-butylboron, and the fading rate is very high.

在可见光敏树脂部分，通过对呫吨染料碘鎓盐和菁染料-硼盐体系的吸收光谱性质、激发态性质、溶剂极性效应、荧光光谱、荧光猝灭、浓度效应、光褪色反应、光聚合动力学等的研究，结果发现：荧光黄双二苯基碘鎓盐体系和含喹啉环端基不对称三甲川菁染料-三苯基丁基硼盐体系在可见光作用下均发生离子对内电子转移反应，且光褪色反应速率很高。

Yields from chiral bisoxazolines (5a) with diethyl oxalate using NaOCH〓 as base for the first time. The structures of chiral multioxazolines and their intermediates, multi (β-hydroxylamide) s, were characterized by 〓H NMR, IR, mass spectra and elemental analysis. The catalytic activities and enantioselectivities of chiral multi (β-hydroxylamide) s (4) and chiral multioxazolines (5～8) were investigated by using acetophenone and β-acetonaphthone as former chiral ketone, KBH〓 or NaBH〓 as reductive reagent in chapter three.

在此基础上，对合成方法作了创新，以羧酸或酯为原料，在无催化剂的条件下与手性α-氨基醇反应，通过回流分水或脱醇的方法，一步反应合成了手性多噁唑啉（5～8），产率为89.2%～98.4%；以手性双噁唑啉（5a）为原料，在NaOCH〓的作用下，与草酸二乙酯反应，首次合成了呋喃类双嗯唑啉（6a），产率为72.9%～75.6%。

The experiments also show that adding NaHSO3 into the reaction liquid of hydroxylation reaction can inhibit the catalytic effect of benzoquinone and residual catalyst on the phenolic tars formation caused by oxo-condensation of the diphenols and therefore reduce the tars formation of the diphenols in the reaction solution.

在羟基化反应液中加入亚硫酸氢钠可以抑制对苯醌和残留催化剂对苯二酚氧化缩合生成焦油的催化作用，从而减少了反应液中苯二酚的生焦反应。

Reaction trends of catalytic desulfurization of thiophene were determined based on the reaction energy needed, which was obtained with the AM1 calculation results of thiophene and possible carbonium ions on transition state.

采用半经验AM1计算方法，利用静态理论对噻吩在分子筛催化剂上的催化裂化脱硫机理进行了量子化学计算研究，通过对噻吩分子和可能产生的中间正碳离子的量子化学计算，得到各中间反应所需的能量，从而判断噻吩催化裂化脱硫反应的趋势，证实了氢转移反应在催化裂化脱硫中所起的作用。

Firstly, 3-ethylthiobutanal was prepared from crotonaldehyde reacting with ethanehiol in triethylamine with high yield. Secondly, methyl acetoacetate was converted to 6-ethylthiohept-3-en-2-one by three steps via hydrolysis, condensation with 3-ethyltio-butanal and dehydration, then 6-ethylthiohept-3-en-2-one was cycloco ndensed with dimethyl malonate by Michael addition and Claisen condensation, followed by saponification and decarboxylation to give the intermediate of 5-(2-ethylthiopropyl)-cyclohexane-1,3-dione.

首先，以巴豆醛与乙硫醇为原料，在三乙胺的催化作用下高收率制得3-乙硫基丁醛；然后从乙酰乙酸甲酯出发，通过碱水解、与3-乙硫基丁醛缩合、脱水三步反应合成6-乙硫基-3-烯-2-庚酮，接着6-乙硫基-3-烯-2-庚酮与丙二酸二甲酯通过Michael加成和Claisen缩合成环，再通过皂化和脱羧反应生成中间体5-[2-丙基]-1，3-环己二酮；再与丙酸酐反应丙酰化，最后与0-3-氯-2-丙烯基羟胺肟化，得到目标化合物烯草酮。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。