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These results were different from the observation in the reaction of Cp2LnNPr2 and PhEtCCO,indicating that ligand, steric effect, electronic effect and solvents have an important effect on the insertion of a ketene into the Ln-N bond.

与phEtCCO不同的是,phZCCO偶联插入LoN键形成的新配体不发生1,5一H迁移的异构化反应,可以直接分离得到苯环参与共扼加成反应的中间体CpZLn〔oe(e6HSCphCON'p几)CphZLn-Er(11,孔(12),Y(13)。

We propose that SEPT7 forms a link between kinetochore localization of CENP-E and the mitotic spindle checkpoint.

同时我还发现SEPT的敲除会导致双极定向的染色体之间的张力减弱以及纺锤体检验点的激活,SEPT7可能将CENP-E的动点定位与纺锤体检验点信号的级联反应相联系起来。

Observe the latent period of the stretching reaction and record the number of stretching in 15 min.

注射醋酸后,观察出现扭体反应的潜伏期及15min内的扭体次数。

Methods Star anise were extracted from Illicium verum Hook.f. using ethanol and ethyl acetate as solvents. After macron absorption resin layer separation, a kind of white fine powder shikimic acid were obtained. The extracted shikimic acid were determined for chemical qualitative analysis.

采用乙醇提取、乙酸乙酯等有机溶剂萃取八角茴香,经大孔吸附树脂柱分离,得到白色精细粉末的莽草酸,并对莽草酸进行化学定性分析,镇痛实验采用扭体法和温浴法,观察腹腔注射莽草酸溶液后小鼠痛阈潜伏期和扭体反应的次数,设阿司匹林和生理盐水为对照组。

Methods Star anise were extracted from Illicium verum Hook.f. using ethanol and ethyl acetate as solvents. After macron absorption resin layer separation, a kind of white fine powder shikimic acid were obtained. The extracted shikimic acid were determined for chemical qualitative analysis. Writhing test and warm bathing test were performed and observed the mice pain threshold latency and writhing reaction times after giving peritoneal shikimic acid extraction solutions.

采用乙醇提取、乙酸乙酯等有机溶剂萃取八角茴香,经大孔吸附树脂柱分离,得到白色精细粉末的莽草酸,并对莽草酸进行化学定性分析,镇痛实验采用扭体法和温浴法,观察腹腔注射莽草酸溶液后小鼠痛阈潜伏期和扭体反应的次数,设阿司匹林和生理盐水为对照组。

After macron absorption resin layer separation, a kind of white fine powder shikimic acid were obtained. The extracted shikimic acid were determined for chemical qualitative analysis. Writhing test and warm bathing test were performed and observed the mice pain threshold latency and writhing reaction times after giving peritoneal shikimic acid extraction solutions. Aspirin and normal saline were used as controls.

采用乙醇提取、乙酸乙酯等有机溶剂萃取八角茴香,经大孔吸附树脂柱分离,得到白色精细粉末的莽草酸,并对莽草酸进行化学定性分析,镇痛实验采用扭体法和温浴法,观察腹腔注射莽草酸溶液后小鼠痛阈潜伏期和扭体反应的次数,设阿司匹林和生理盐水为对照组。

The tin atom of the title molecule exists in a distorted- trigonal- bipyramidal geometry, defined by three carbon,one iodineand one oxygen atoms leading to a five - membered chelate ring. The x- ray analysis show tha...

标题化合物分子中的锡原子被配体的三个碳、一个碘和一个氧原子配位;配位原子是畸变的三角双锥构型;标题化合物具有与卤素发生取代反应而不发生加成反应的性质。

Alkylation of methylnaphthalene and methanol over HZSM-5 zeolite can make 2, 6-dimethylnaphthalene (2, 6-DMN) and the product stream contains isomers of 2, 6-DMN and unreacted MN, which requires efficient separation.

以甲基萘和甲醇为原料,采用HZSM-5烷基化催化剂制取2,6-二甲基萘(2,6-DMN)。由于产物中含有2,6-DMN的异构体以及未反应的MN,需对反应产物进行有效分离。

RESULTS AND CONCLUSION: After purification, the cell body of SGCs from cochlear modiolus was ellipse or triangle, with slender processes in cytoplasm. Nuclei were positive for Nuen.

结果与结论:蜗轴组织细胞纯化后,胞体呈椭圆形或三角形,有细长的突起,Nuen染色胞核呈棕黄色阳性反应,β3-Tubulin染色细胞胞浆与轴突均呈棕黄色阳性反应。

RESULTS AND CONCLUSION: After purification, the cell body of SGCs from cochlear modiolus was ellipse or triangle, with slender processes in cytoplasm. Nuclei were positive for Nuen. Cytoplasm and axon were positive for β3-Tubulin.

结果与结论:蜗轴组织细胞纯化后,胞体呈椭圆形或三角形,有细长的突起,Nuen染色胞核呈棕黄色阳性反应,β3-Tubulin染色细胞胞浆与轴突均呈棕黄色阳性反应。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。