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Three open chain crown ether s and triglycolyl isopropylidene hydrazide complexes of rare earth nitrate were synthesized for the first time with isoproylidene hydrazide as the terminal group and through IR, 1HNMR, MS, characterized their structures have been characterized.

首次合成了以丙酮酰腙为端基的3种双酰腙型开链冠醚及三甘双酰丙酮腙稀土硝酸盐配合物,并通过元素分析,IR,1HNMR,MS对分子结构进行了表征

115 caprine right femurs were taken and created to simulate AO/33-A3 fracture. All fracture models were fixed by the right 5 hole LISS Plate, which treated differently by using unicortical or bicortical screws in the proximal end of the LISS plate. And then withdrawal force and torsional force were given on them to make comparison.

取115根新鲜羊右侧股骨,造成股骨远端AO分型33-A3型骨折,并均采用5孔右侧股骨远端LISS钢板予以固定,在骨折近端固定螺钉单双皮质不同分布状态下,分别作拔出和扭转的生物力学对比试验研究。

Common fault components and differential fault components are introduced into the algorithm to uncouple mutual electromagnetic coupling effect between two parallel circuits.

基于反序故障网络和故障边界条件,本文提出了一种利用双回线单端工频电流量的同杆双回线准确测距新算法。

Methods analyzed the 60 cases of patients whom were conducted salpingography with tubal patent test apparatus by liquid instillation.results in 60 cases, both oviduct get through in 42 cases , account for 70%;one oviduct incompletely get through in 6 cases, account for 10%;both oviduct were blocked in 12 cases, account for 20%.among them ,2 cases of hydrosalpinx ,4 cases of ampulla of uterine tube obstruction,6 cases of scarcity in one side oviduct,10 cases of absence of develop in interstitial portion of the tube.

分析研究60例子宫输卵管造影患者应用输卵管通液诊疗仪进行检查的病例资料。结果:60例中,双侧通畅者42例,占70%;一侧通而不畅者6例,占10%;双侧输卵管不通者12例,占20%。其中2条输卵管伞端积水;4条输卵管壶腹部阻塞,6条输卵管一侧缺如。10条输卵管间质部不显影。

This malunion produced a cosmetic defor- mity only, without impairment of function.

其中4例患者,骨折近端只有一根克氏针贯穿;1例患者两根克氏针中的一根未贯穿双皮质;3例患者骨折端克氏针间隔不够,导致结果为单针固定。

Finally, the cytotoxic and antibacterial activities of the oxamido-bridged binuclear complexes were studied in vitro.. This dissertation consists of three sections as follows:1. The crystal structure of a oxamide dinitrate,(1) [H_4dmaeoxd](NO_3)_2 H_2dmaeoxd = N,N\'-bis[2-ethyloxamide, has been obtained. The diversity of complexes with different structures is carried out by successful synthetic strategy of controlling species of metal ions, counter anions, pH values and solvents in the course of synthesis. Four dinuclear complexes bridged by trans-dmaeoxd2-: [Cu_2_2](ClO_4)_2 (2), [Cu_2_2](ClO_4)_2 (3),、[Cu_2(Me_2phen)_2](ClO_4)_2 (4), [Cu_2_2(H_2O)_2] (5); Four dinuclear complexes bridged by cis-dmaeoxd2-: [NiNi_2](ClO_4)_2 (6), [CuNi_2](ClO_4)_2·2CH_3OH (7), [CuZn_2]-(ClO_4)_2·2H_2O (8), [Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9); three 1-D polynuclear complexes: [Cu_2]_n·nH_2O (10), [Cu_2(H_2O)_2-]_n·4nH_2O (11), [Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12); one 2-D polynuclear complex,[Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n).2nH_2O (13); the others: [VO(H_2O)]·2H_2O (14), [Zn_2_4](ClO_4)_2·H_2O (15), [Cu_2]·2DCM (16) have been synthesized and characterized by X-ray single crystal diffraction, elemental analysis, IR spectra.

本论文主要包括以下三部分:一、合成得到了一个草酰胺配体硝酸盐的单晶结构,[H_4dmaeoxd](NO_3)_2 (1);通过调控金属离子的种类、端基配体、抗衡阴离子、溶剂、pH值等条件定向合成了四个反式草酰胺桥联双核铜配合物:[Cu_2_2](ClO_4)_2 (2)、[Cu_2_2](ClO_4)_2 (3)、、[Cu_2(Me_2phen)_2](ClO_4)_2 (4)、[Cu_2_2(H_2O)_2] (5);四个顺式草酰胺桥联同/异双核配合物:[NiNi_2](ClO_4)_2 (6)、[CuNi_2](ClO_4)_2·2CH_3OH (7)、[CuZn_2]-(ClO_4)_2·2H_2O (8)、[Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9);三个一维聚合物: [Cu_2]_n·nH_2O (10)、[Cu_2(H_2O)_2-]_n·4nH_2O (11)、[Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12);一个二维聚合物: [Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n)。2nH_2O (13);单核钒配合物[VO(H_2O)]·2H_2O (14)、草酸根桥联双核锌配合物[Zn_2_4](ClO_4)_2·H_2O (15)、美洛西康铜配合物[Cu_2]·2DCM (16),利用元素分析、摩尔电导、红外光谱、电子光谱和单晶X-射线衍射对上述所得化合物进行了结构表征,探讨了结构影响因素,并研究了其超分子结构。

The experiment was lasted for four weeks, and all animals were sacrificed one day after the final simvastatin administration. The right tibiae were removed for the measurement of bone histomorphometry, and bone mineral density in the right femur was measured by dual-energy X-ray absorptiometry.

实验持续4周,所有大鼠在最后1次灌胃后的第2天被处死,取大鼠右侧股骨用双能X线骨密度仪测量整体和远端骨密度;取右侧胫骨近端进行骨组织形态计量学测定。

Base Station type Software versionTypes of carrier frequency board adoptedTypes of combiner adoptedWhether had obtained the network license or notIndoor type or outdoor type Whether the master port is separated from the remote-port The maximum carrier frequency capacity of single cabinet The maximum supportable sector numbers of single cabinetWhether it is dual-carrier frequency board or notMust it be paired configuration if it's dual-carrier frequency board (namely, the type of single carrier frequency station could only configure the dual-carrier frequency on hardware) The maximum achievable configuration of a single station of the single cabinetReceiver sensitivity The maximum expand capacity of a single base station (the maximum number of TRX in configuration / the number of cabinets which is required)(fill in according with the three sectors) Top box transmitted power (given separately a grade one combine and a grade two combine) The maximum output power of amplifier (voice, a single logical carrier frequency) The maximum output power of amplifier (EGPRS, a single logical carrier frequency)Whether it has tower-interfaceWhether it has built-in lightning protectionWhether it support the ultra-long cover / whether it need for software support (give simple description that how hardware and software could achieve this) The supporting condition of EGSM (it should be supported including by the carrier frequency, combiner) Dual-band carrier wave (whether it supports the mixed use of 900 M/1800M in the same cabinet) The commonality of duplicate parts Whether it can built-in transmission unitThe single cabinet size (high × width × deep) Installation method Whether it can place against the wallThe basic frame full-configured weight and the supportable number of carrier frequencyThe expansion frame full-configured weight and the supportable number of carrier frequency

基站型号软件版本号采用载频板型号采用合路器型号是否已取得入网许可室内型or室外型是否是主远端分离单机柜最大载频容量单机柜最大支持的扇区数是否是双载频板如是双载频板,是否必须成对配置(即单载频站型只能硬件配置双载频)单机柜可达到的单站最大配置接收机灵敏度单基站最大扩展能力(最大配置TRX数/需机柜数)(按3扇区填写)机顶发射功率(分别给出一级合路与两级合路)功放最大输出功率功放最大输出功率(EGPRS,单个逻辑载频)有无塔放接口有无内置避雷装置是否支持超远覆盖/是否需要软件支持(简单描述软硬件如何实现)EGSM支持情况(包括载频、合路器均应支持)双频段载波(是否支持900M/1800M在同一机柜内混合使用)备件通用性是否可以内置传输单元单机柜尺寸安装方式可否靠墙放置基本架满配重量及支持载频数扩容架满配重量及支持载频数是否支持基本架与扩容架跨扇区满配功耗满配时重量供电方式机柜进出线方式合路器损耗合路能力:几合一单扇区最大支持几载频合路到一副天线/采用几个合路器单扇区载频达到需要增加一副天线时,是否支持两级合路换以不增加天线如两级合路插损为是否支持基带跳频和合成跳频每单个合路器在从低载频数向高载频数扩容时,是否还需要增加硬件可用性指标MTBFMTTR系统中断服务时间硬件是否支持EGPRS本次报价软件版本号开始支持EGPRS的软件版本号其他特点注: 1 应分别填写出来按照本次报价要求所采用的全部BTS型号和采用的合路器型号 2 列出本报价要求的全部室外型基站与高功放单元

Atfirst,stress and displacement at the end of collinear crucks are calculated by elasticity me-chanical method,then general solution of twist force at the end of collinear cracks is givenby rotation theory,single crack and double cracks are discussed emphatically.

本文计算并讨论了忽视旋转的传统理论所不能给出的裂纹端部场与场源的相互作用,首先利用弹性力学方法计算了共线裂纹组端部的应力场及位移场,然后应用旋转理论给出共线裂纹组端部的扭转力通解,对单裂纹和双裂纹情形做了重点讨论。

Put two ends of one steel wire through two channels of one wheel of angle turner for one longer end and one shorter end. Put the shorter end through the vertical wheel of double-wheel stand top and the longer end through the horizontal wheel of the double-wheel stand top and into the vertical wheel of the single-wheel stand top.

将其中一根的两个端头分别穿过转角器一轮子的两条槽,分成一长一短,短端穿入双轮顶座的竖轮,长端经过双轮顶座的横轮,牵引穿入单轮顶座的竖轮。

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I didn't watch TV last night, because it .

昨晚我没有看电视,因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来,在北京的很多小区里,电梯液晶电视被撤了下来。

I'm running my simile to an extreme.

我比喻得过头了。