双烯合成

The results show that it only takes 8 min for the reaction, when the initiator is potassium persulfate/sodium thiosulfate which forms an oxidation-reduction initiator system; N,N-methylene diacrylamide is as cross-linker; neutralization degree is 70%, under the microwave power of 360 W.

结果表明，在360W的微波辐射功率下，采用过硫酸钾与硫代硫酸钠的氧化还原引发体系，N，N-亚甲基双丙烯酰胺为交联剂，接枝单体的中和度为70%时，只需8min就可以完成纤维素基高吸水树脂的接枝共聚合成。

Last, we studied the allylation of benzoylhydrazones with allyltrichlorosilane.

在研究过程中，发现了一个C=N双键烯丙基化的新方法，和苯甲酰肼的新的合成方法。

In order to study strcture-bioactivity relationship concerning α,β-unsaturated-γ-lactones, we further synthesized γ-benzyloxymethy-γ-butanolide XXIII and the corresponding unsaturated buteno- lido XXV Scheme 6, p.

为了研究该类化合物的构效关系，在本论文第三部分，我们进一步设计并合成了--γ-苄氧基甲基-γ-丁内酯XXIII和--γ-苄氧基甲基-γ-丁烯内酯XXV这两个内酯化合物，目的是想考察内酯的α，β-不饱和双键是否是产生细胞毒性的关键结构。

Objective To synthesize 10-O-adipic acid-[2'-methoxy-4'-(3"-keto-1"-Butenyl)-Phenoxy-]-dihydroartemisinin conjugate.

目的 合成10-O-己二酸基－［2'-甲氧基4'-（3&-酮－1&-丁烯基）－苯酯］－双氢青蒿素酯。

The trifluoroethylester silane was synthesized by modifying a PEG diacid to form the corresponding bistrifluoroethylester, followed by a reaction with 3-aminopropyltriethoxysilane.

通过用PEG二酸修饰合成三氟乙基乙烯醚硅烷，由此形成相应的双丙烯酰胺三氟乙基乙烯醚，再将其与3-APS相互作用。

A hyperbranched macromonomer (3) was synthesized with maleic anhydride,diethanolamine,o-phthalic anhydride by step polymerization,take advantage of the different activities of functional groups.

以顺丁烯二酸酐、二乙醇胺、邻苯二甲酸酐等为原料，利用官能团活性的差异，通过逐步展开的方法合成了含有双键和端羟基的聚型分子结构的超支化大单体(3)。

The main downstream products from the industrial dipentene were reviewed,such as:some kinds of polyester,fine chemical intermediates such as p-cymene,p-menthane and flavours such as carvone ,terpinyl acetate and so forth,the main characteristics and applications were also described in the paper.

综述了工业双戊烯主要的下游产品聚酯树脂、精细化工中间体如对伞花烃、对孟烷以及香料如香芹酮，乙酸松油酯等的合成方法及反应条件，介绍了相应产品的主要性质、用途。

The catalytic performance of copper-nickel oxalate catalysts prepared by concurrent coprecipitation was studied in the gas-phase reaction of p-cymene synthesis by dehydrogenation of industrial dipentene.

研究了并流共沉淀法制备的草酸铜-草酸镍催化剂在工业双戊烯脱氢合成对伞花烃气相反应中的催化性能。

The p-Isopropylbenzoic acid was synthesized by catalytic transfer dehydrogenation with 5% Pd/C using dihydrocumic acid as material and hydrogen offer, industrial dipentene as hydrogen acceptor and solvent, reacted directly under reflux condition.

采用5% Pd/C作为转移氢催化剂，原料二氢枯茗酸为氢给予剂，以工业双戊烯作为氢接受剂和溶剂，合成了对异丙基苯甲酸。

The results showed that MGM had good spherical shape and narrow size distribution,and the particles with diameters ranging from 0.13 mm to 0.28 mm were about 91 wt%.The surface hydrophilicity of Fe3O4 microcrystal was improved by formamide dispersing treatment.The gel particles made by the copolymerization of glycidyl methacrylate and N,N′-methylene bisacrylamide could encapsule Fe3O4 microcrystal to produce colloid cores,and uniform and stable MGM microspheres were formed by the conglomeration of the colloid cores.

结果表明，合成的MGM呈球形，且粒度分布较窄，粒径为0.13～0.28 mm的粒子占91%；甲酰胺分散Fe3O4，微晶表面的亲水性进一步增强，单体甲基丙烯酸缩水甘油酯和 N，N′亚甲基双丙烯酰胺交联共聚生成的胶粒能够包埋Fe3O4微晶形成胶核，胶核聚集形成均匀、稳定的MGM微球。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。