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We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

I mean to go ,but my fathernot won't alow meTo raise salary means increasing purchasing power.

我想去,但是我父亲不让我去 mean to do打算想,客观上的原因没办法去

Recently,I went to the bar,I remembered that I had promised him,Later again will not go to the bar to play, But at this time,I has no way to complate this pledge really,I can relax heartily and forgot heartily only there.Forgot these recollection does not belong to own .Let the liquor anaesthetize my thought.I do not understand so painful to love him?

这些日子,我又去酒吧了,我记得曾经答应过他,以后再也不去酒吧玩,但此时的我,真的没法完成这个承诺,只有在那里,自己才可以尽情地放松,尽情忘记,忘记那些原本就不属于自己的回忆,让酒去麻醉自己的思想,我不明白爱他真的有那么痛苦吗?

If he even see a straddle-bug start to go anywheres, he would bet you how long it would take him to get to--to wherever he was going to, and if you took him up, he would foller that straddle-bug to Mexico but what he would find out where he was bound for and how long he was on the road.

要是他看见一只屎克螂朝哪里开步走,他就跟你赌它几天才能到——不论到哪儿都行;只要你接茬,哪怕是去墨西哥,他也会跟着那只屎克螂,看看它到底去不去那儿,路上得花几天的时间。

The first thing to see, looking away over the water, was a kind of dull line -- that was the woods on t'other side; you couldn't make nothing else out; then a pale place in the sky; then more paleness spreading around; then the river softened up away off, and warn't black any more, but gray; you could see little dark spots drifting along ever so far away -- trading scows, and such things; and long black streaks -- rafts; sometimes you could hear a sweep screaking; or jumbled up voices, it was so still, and sounds come so far; and by and by you could see a streak on the water which you know by the look of the streak that there's a snag there in a swift current which breaks on it and makes that streak look that way; and you see the mist curl up off of the water, and the east reddens up, and the river, and you make out a log-cabin in the edge of the woods, away on the bank on t'other side of the river, being a woodyard, likely, and piled by them cheats so you can throw a dog through it anywheres; then the nice breeze springs up, and comes fanning you from over there, so cool and fresh and sweet to smell on account of the woods and the flowers; but sometimes not that way, because they've left dead fish laying around, gars and such, and they do get pretty rank; and next you've got the full day, and everything smiling in the sun, and the song-birds just going it!

往 水面上望去,首先看到的是灰蒙蒙的一条线——那是河对岸的树林子——别的便什么也看不清——接着是天空中有一点儿鱼肚白;然后鱼肚白多了些,逐渐朝四周散开去;接下来,远处河水的颜色淡了些,不是那么黑了,而是灰灰的了。更远处,可以看到小小的黑点子在漂过来——那是些载货的驳船之类。还有黑黑的一长条——那是木筏子。有时能听到长桨吱吱地响,或者一些杂音。四周这么寂静,声音又来自很远的远方。过了一会儿,你看到一道水纹。凭了水纹的模样,你知道那里有一块礁石,急流朝着它冲过去,流水飞溅,成了这个模样。你看到,雾气袅袅上升,离开水面,东方红了起来,河面红了起来。你可以看到对岸河边树林子边上一处原木搭成的小屋,那可能是一个木材场,在那里堆着的一堆堆木材,中间却是空的,容得狗钻来钻去,为了能叫人家上当①。然后微风轻拂,从河上一阵阵吹来,那么凉凉的,那么清新,闻起来那么甜美,这是全凭了那些树林子和那些鲜花的缘故。可有时候也并非全是如此美妙。

First of all, introduce the Fourier analysisand wavelets analysis, two methods of non-linear function approximation of the effect ...

第二章介绍了图像去噪的知识和各种去噪方法,着重介绍了阈值去噪和相关的阈值取法。

Whilst every fair-skinned, dark-haired maiden in the area attempted to persuade the village elders that she should be the one chosen for this important task, More travelled up to Sheffield to commission an expert armourer to create a suit covered with spikes of steel six inches long.

当时,当地的每一个皮肤白皙的黑发少女都试图说服村里的长老自己应该被选去完成这个任务。骑士一直旅行到Sheffield去委托一位制作盔甲的专家去制作一件表面覆盖着许多6英寸长的钢制钉子的盔甲。

I visit the travel to be able to start from Japan, I want to go to box root froth that to be well-known the world hot spring, then I must go to South Korea, then is France, when I wander about in that aspic colored field, that kind of feeling is certainly very satisfied, then I must go to England to look in front of Buckingham Palace the valiant palace guard passes on to the next shift the ceremony.

我的环游之旅会从日本开始,我想去箱根泡泡那闻名世界的温泉,然后我要去韩国,接着是法国,当我徜徉在那薰衣草花田里,那种感觉一定很惬意,然后我要去英国看白金汉宫前雄纠纠的御林军交班仪式。。。。。

He would want to be in Austin, but will be where he must.

奥斯汀是他想去的地方,但最终他会先去他必须去的地方。

Of course, this is a war you personally won't have to fight. Just like when you went AWOL while the poor were shipped to Vietnam in your place.

当然,这是一场你不会去亲身犯险的战争,就像你去AWOL的时候,代替你去越南的是那些穷人。

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歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

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