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There are temperature grads and crystalline particle concentration grads existed in oxyacetylene flame. It leads to the unequal thickness of diamond film and increases the tool cost. This paper brought forward the varying parameters method for depositing diamond thick film.

氧气-乙炔火焰的燃烧特性决定了火焰的横断面存在温度梯度和成晶粒子浓度梯度,导致金刚石厚膜的厚度不均匀,增加了厚膜刀具的制造成本。

The influence of different assembled condition such as assembly method, concentration of zirconium source and pH value on the effectiveness of assembly were evaluated via DSC-TG, FT-IR, Uv-vis and SAXRD et al. It showed that the assembly effectivness of uncalcined 3 Si/Zr_10# sample was best.c The optical characteristic, which including light-conduction in infrared band and polarity in visible band, of dip-coating film and membrane assembled zirconia after processing parameters of assembly optimized were observed via FT-IR and Uv-vis. The polarity was characterized by polarizing angle through calculation from light-transmittance, light-reflectance and fresnel coefficient. qualitative analysis showed that the polarity of Si/Zr_10 # dip-coating film assembled was best.d Adopting zirconium oxychloride as zirconium source, CTAB as template, employing different CTAB adding sequence, two mesoporous zirconia samples were prepared. The template effect of two samples was discussed. It showed that the effect of the sample which CTAB adding sequence was same as mesoporous silica film was better. The light-conduction in infrared band of these samples was also studied, which offered comparison to the polarity of zirconium dioxide assembled within mesopore.

结果显示:组装条件优化后的uncalcined 3 Si/Zr_10#厚膜样组装效果最好,其组装液对应的pH值最利于该锆源离子模板交换组装; c选用FT-IR、Uv-vis对组装条件优化后纳米氧化锆/介孔氧化硅厚膜、纳米氧化锆/介孔氧化硅薄膜包括红外导光性、可见光区内的偏光性在内的光学特性进行了分析,其中偏光性以膜层透光性、反光性及菲涅耳系数计算出的偏振角即布儒斯特角表征,定性分析显示,Si/Zr_10#ZrO_2/介孔氧化硅厚膜偏光性最好; d以氧氯化锆ZrOCl_2·8H_2O为锆源,CTAB为模板剂,采用不同的模板剂加入顺序,探索性地制备两介孔氧化锆样,分析了两介孔氧化锆样的模板效果,得出模板剂加入顺序同介孔氧化硅薄膜时介孔氧化锆样的模板效果较好,并分析了所得样品的导光性,为锆氧粒子引起的附加光学特性分析提供了参考和对比。

The lattice relaxation in the CVD diamond thick films were detected by the X-ray diffraction attachments. It is associated with self-annealing of diamond thick films in the process of long time deposition. The wearing discrepancy of diamond coated cuttings and diamond thick films brazed cuttings is well illustrated by means of lattice relaxation.

用X射线衍射仪的薄膜附件测试分析金刚石厚膜内的晶格松弛现象,发现沉积金刚石厚膜过程中存在高温自退火的作用,运用晶格松弛的观点很好地解释了金刚石薄膜涂层刀具与厚膜钎焊刀具的耐磨性能差异。

To resolve this behavior, only the surface business card printing and membership card making to set to print in ink that is not on the surface without worrying about the colour, there are three ways: the first one is a drumlike complex members'meeting, Bopp/business card printing and membership card making/PE, such a structure you need to have special line cost more per bag fee in order to achieve $ 0.10/only, the second film structure is the PE/business card printing and membership card making/PE, such a structure common packaging equipment can also be filling, but cost more, each bag shall be $/only 0.08, the third option is the-tape-PE/business card printing and membership card making/PE structure in the original film, that is, the members'meeting membrane business card printing and membership card upon completion of the making of the operation, the business card printing and membership card making surface salivate a layer of transparent with thin-film, this is our company according to actual usage of the product structure specially developed.

给彻底处置这一不隐象,只有不兵暗地制卡和会员卡制作改不败边印,油不朱不在暗地也不离供给安心掉色,办法有不一栽:第一栽是复不合奶膜布局为BOPP边/制卡和会员卡制作/PE边,这样的布局需有附带灌装摆设,不败本也较矮,每一个袋子用度给到达0.10元/只把握),第二栽膜的布局是PE/制卡和会员卡制作/PE,这样的布局别致灌装摆设也可灌装,但不败本还是较矮,每袋须0.08元/只把握,第不一栽办法是流延PE/制卡和会员卡制作/PE布局不厚膜,即在原奶膜制卡和会员卡制作完不败后,再增增一道工序,在制卡和会员卡制作背流涎一层透明的较不厚的不厚膜,这是我们公司根据客户本质搁置环境出格开不收的产物布局。

The stability of production materials are also important, films and soft and hard on business card printing membership card making ink adhesion can be expected to a certain extent, the high density of ink on filmogen is not particularly good, soft point on monlchamus filmogen passbys.

承印质料的稳定性也很重给,不厚膜的不硬不硬差制卡和会员卡制作油不朱的附着力也会有必定感化,矮密度的不厚膜质料上不朱不是不入格精良,不硬一不面的不厚膜质料上不朱较好。

The factors of temperature and humidity influenced on film thickness and order of layer were studied, in which pulling speed and pulling times were also included. It showed that the thickness of single dip-coating film reached 0.23 μm ~ 0.625 μm, and the degree of order of surface layer were still holding much higher.b Adopting calcined or uncalcined mesoporous silica membrane as matrix, nano zirconia particles were assembled through ion exchange method and ion-template exchange method.

结果表明,单次提拉膜膜厚0.23μm~0.625μm、8次提拉后表层膜仍有一定的有序性; b以自制的介孔氧化硅煅烧/未煅烧厚膜样为基体,采用离子交换法/离子模板交换法组装锆氧纳米粒子,选用DSC-TG、FT-IR、Uv-vis、SAXRD等对不同组装方法、锆源浓度、pH值等组装条件下ZrO_2/介孔氧化硅厚膜组装效果进行评价。

The above production operations to undergo a rigorous control of detection, the ink attachment fastness of general usage requirements can be achieved, but because the milk membrane business card printing and membership card making, as printed on the table, that is, the surface of the ink in the film, is vulnerable to all kinds of injury, and water, acid, machinery, more or less friction will cause ink wash after wash, moreover, milk is in the filling is completed, are generally intended to be appropriated for cold storage of 4 ° c, milk from the inside out, the film surface as a result of alternating hot and cold, dew will be generated, in transit, bags and bags into as a result of vibration between, in the hands of consumers, and some of it will be on milk heating drinking, such a procedure requires ink has both a very good resistance to freezing, resisfance, thermotolerance and crocking performance and this envirogluvtm products in production is very difficult, so far, no inks contain all the characteristics of these four.

以上出产上各道工序不纬功澈底把持的检测后,油不朱的附着牢度凡是可以到达搁置请求,但由于奶膜的制卡和会员卡制作为边印,即油不朱在不厚膜的暗地,容难受到百般保养,火、酸、板滞、磨擦或多或少城市引起油不朱的掉色,况且,牛奶在灌装完不败后,凡是都需放出4℃的冷藏室冷藏,牛奶从冷藏室拿不出来后,不厚膜暗地由于冷冷瓜代,会爆不收结露不隐象,在输送途洋,袋与袋之间由于波动爆不收磨擦,到了出产者手边,有的还需差牛奶增冷饮用,这样一个功程不离请求油不朱同时具有不一不合精良的抗冷冻、耐火性、耐冷性和耐磨擦本能机能,而这样的油不朱产物在出产洋是不一不合艰难的,到目后为止,也操纵一栽油不朱能合座敷裕以上四栽共性。

This is because when BaTiO_3 volume fraction is higher than 50%, the crystallinity of PVDF is low and the film quality deceases.

这是因为随着BT的含量的增加,PVDF不能很好结晶,复合厚膜的微观结构也出现较大孔洞,材料彻底失去弹性。

For the powder having burn out process, the densification of the films is higher under carrier gases Ar,O2,N2. The surface roughness also increases with increasing gas flux.

初始粉末经烧除后镀制之厚膜结构,以Ar,O2或N2携带气体下最为致密,且膜厚及表面形态差异并不大,可发现较为平整之膜面,但随著流量的提升,表面的粗糙度则会增大。

The dielectric and ferroelectric properties of the films and their dependence on the film microstructure were also studied.

研究了PZT厚膜的铁电、介电性能及其与制备工艺条件和膜的微结构的关系。

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