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The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应,用茚〓和1,1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物,发现可控制反应条件,使1,1'-联茚与〓反应,并高产率地得到具有新颖结构的单加成物,用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征,测得它的两个〓杂化的桥头碳的化学位移为〓ppm,证明生成的衍生物为6∶6闭式环加成,〓NMR谱中共给出38个信号,表明〓联茚衍生物分子具有〓对称性;在波长532nm,脉冲宽度8ns的激光下,〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近,由于〓联茚单加成衍生物熱稳定性好,在四氢呋喃,丙酮等极性溶剂中溶解性好,能分别均匀地掺入溶胶-凝胶中,已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能;使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究,通过等温压缩曲线测试,证明浓度为〓〓时,〓联茚衍生物能够形成单层膜。

In the pH range of 6~12, the results of the flotation tests indicate that the performance of the new combined cationic collector (CS3:CS1=3) and (CS3:CS2=2) is similar, and they are effective collectors for reverse flotation of the iron ores. The combined cationic collectors exhibited the same collectability as dodecylamine, but better selectivity than dodecylamine. By using the combined collector, the dosage of the collector decreased from 1 10-4mol/L to 1 x 10-5mol/L .

单矿物可浮性试验结果表明,在pH=6~12的范围内,新型组合药剂CS_3:CS_1=3和CS_3:CS_2=2具有相近的药剂性能,在其捕收能力与十二胺相当的前提下,不但选择性较十二胺好,而且还能显著提高药剂的协同效应,使药量从单用时的1×10~(-4)4mol/L降至1×10~(-5)mol/L,是铁矿石反浮选的高效捕收剂。

In SCD survivors, sustained monomorphic ventricular tachycardia is inducible by electrophysiologic testing in 40 to 50% and polymorphic VT in 10 to 20%; in 30 to 50%,no sustained arryhthmia is induced.

在心源性猝死生还者中, 40~50%电生理试验能诱导持续单一型室性心动过速,10~20%能诱导多型的,30~50%不能诱导持续的节律异常。

Majority of acute leukemias in infant, either acute lymphoblastic leukemia or acute myeloblastic leukemia, posses a chromosomal translocation affecting the 11q23 chromosome region which specifically inoles the mixed-lineage leukemia gene.1-3 Most pediatric leukemias with MLL rearrangement clearly hae a remarkably short latency.1,4 MLL gene rearrangement is also associated with secondary leukemias of patients preiously treated with the topoisomerase II inhibitors.4 The latency of these secondary leukemias is similarly ery short.4 Of note, the concordance rate of leukemia with MLL rearrangement in infant monozygotic twins approximates to 100%,1,4 and identical breakpoint in the MLL gene was shared in these pairs of identical twin infants with concordant ALL.1,4 Moreoer, the unique and clonotypic MLL fusion gene was detectable in neonatal blood spots for Guthrie cards from non-twined indiiduals who subsequently deeloped ALL.1,4 These obserations indicate not only that MLL fusion is generated in utero but also that MLL fusion proteins could be capable of inducing leukemic transformation with few, if any, secondary mutations.2,3,4 Greaes et al speculate that an MLL fusion protein somehow promotes rapid transition to full-blown disease in patients ia ery rapid clonal expansion, genetic instability, or inhibition of DNA damage repair.4 In general, for clonal expansion of malignancies, tumor cells often hae acquired strategies that escape immune sureillance of the hosts.5,6 Immune escape mechanisms also contribute to the failure of graft-ersus-leukemia effect after allogeneic hematopoietic stem cell transplantation.7 Therefore, leukemia cells could acquire some immune escape mechanisms during leukemogenesis.

绪论 绝大多数的婴儿白血病,不管是急性淋巴性白血病或是急性骨髓性白血病,在染色体11q23部位有染色体易位的情况;这个部位的染色体易位牵连了混合谱系白血病基因。大多数具有MLL基因重排的儿童白血病潜伏期明显短很多。MLL基因重排也和经拓扑异构酶II抑制剂治疗后的继发性白血病有关。这些继发性白血病的潜伏期类似地都非常的短。很重要的是,单卵双胞胎婴儿同时患有或同时免于MLL基因重排阳性的白血病的一致性接近100%;并且同样患有ALL的同卵双胞胎的MLL基因的断裂点是一致的。而且,这种独特的克隆特异性的MLL融合基因能够从那些得ALL的非双生个体出生时的血斑标本中检测到。这些发现表明MLL融合基因产生在胎儿还在子宫的是后,而且MLL融合蛋白能过和其他的基因突变一起诱导白血病的产生。Greaes 等推测MLL融合蛋白在某种情况下同过快速克隆增殖,遗传的不稳定性或是DNA损伤修复的抑制促使疾病迅速地全面爆发。恶性肿瘤细胞的克隆增殖通常已经获得了逃避机体免疫监视的能力。免疫逃避机制也归因于异体外周血干细胞移植后移植物抗白血病作用的失效。所以,白血病细胞在白血病的产生过程中可能获得了某些免疫逃脱机制。

The trophoblast blood flow spectrum could be easily detected with the guide of CDE.The ultrasonic findings were characterized by broad arterial flow spectrum,high diastolic component of the low resistance trophoblastic flow,RI=0.40~0.51 with single or biphasic spectrum.The salpingian ring with high blood flow indicated early and complete salpingian pregnancy.

结果:①异位妊娠包块血流信号丰富,血管连续性好,能较完整显示血管床、血管网及范围广的低流速血流信号;②脉冲多普勒取样为滋养层周围性血流频谱,其特征为:频谱增宽、单相或双相持续存在、阻力降低(RI=0.44±0.04)、舒张期血流丰富的动脉频谱;③具有鲜明丰富的滋养层周围性彩色血流频谱特征的&输卵管环&是早期输卵管妊娠的特征性表现,并提示是输卵管完整存在的标志。

They may lack some conceptual beauty but you have to agree - they are fine-tuned, visually stable, and very difficult to reproduce.

他们可能缺少一些概思性的好感,但你不能否定的是-他们是协调的,视感稳固的,很易单造的。

In the basis of comparing the developing projects on the optical interconnection networks, combining with the actual probability of realization, we proposed the scheme of free space optical crossbar interconnection network using spatial light modulator . This interconnect structure is the most powerful single level interconnect network with the characteristics of reconfiguration and non-blocking. It can achieve arbitrary point-to-point link. Even more has it the ability of broadcasting and funnelling.

在比较现有的光互连方案的基础上,结合具体的可实现性,本文提出了使用空间光调制器的自由空间光学交叉开关互连网络的方案,这种互连结构是功能最强的单级互连网络,具有可重构性和非阻塞性,不仅能实现任意点到点的连接,还具有广播和汇集的能力。

In this scheme, two kinds of watermarks are embedded respectively into vertexes coordinates and topological information of 3D mesh, which enables the model to resist against not only large scaled cropping operation but also high strong noising. During the extraction of the watermark, the original model is not necessary.

该算法分别对3D网格模型的顶点信息和拓扑信息嵌入2种不同类型的单鲁棒性水印,从而使模型既能抵抗大面积的剪切攻击,又能抗击一定强度的噪声攻击;且在水印提取时不需要原始模型信息。

When the effect ofNTP was examined after depletion of monoamines in the spinalcord by intrathecal neurotoxins, the antiallodynic and antihyperalgesiceffects were still observed after serotonergic denervation,but not after noradrenergic denervation.

鞘内给予神经毒素耗竭脊髓单胺递质后检查 NTP 的作用时,去除5羟色胺能神经支配后 NTP 的抗触觉性痛感和抗痛觉过敏作用仍然存在,但是去除去甲肾上腺素能神经支配后则消失。

It was shown that these two strains both can utilize benzoate as sole carbon source and the maximum tolerance of benzoate are 1.7% and 1.600, respectively; These two strains both can grow on benzene, toluene, xylene, phenol, benzyl alcohol of as sole carbon source. Pfluorescens PFO1 can degrade dianiline, 3,5-dinitrosalicylic acid, p- dimethylaminobenzaldehyde while P. aeruginosa ATCC27853 can utilize 3,5-dinitrosalicylic acid, p- dimethylarninobenzaldehyde.

结果表明,两种菌都能在以苯甲酸钠为唯一碳源的基础培养基上生长,并且,对苯甲酸钠的耐受性分别达到1.7%和1.6%;两种菌都能以适当浓度的苯,甲苯,二甲苯,苯酚,苯甲醇为唯一碳源生长;荧光假单胞菌能以二苯胺,对二甲氨基苯甲醛,3,5-二硝基水扬酸为唯一氮源生长;铜绿假单胞菌能以3,5-二硝基水扬酸,对二甲氨基苯甲醛为唯一氮源生长。

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Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化,但却比去年同期高8%。

However, to get a true quote, you will need to provide detailed personal and financial information.

然而,要让一个真正的引用,你需要提供详细的个人和财务信息。