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The result of SDF monosaccharide composition showed that the monosaccharidein SDF of soybean dregs is mostly rhamnose, arabinose, xylose, glucose and galactose.

实验测定的SDF单糖组分分析表明:豆渣SDF的单糖组分主要为鼠李糖、阿拉伯糖、木糖、葡萄糖和半乳糖。

Sugar alcohols such as mannitol, sorbitol, xylitol, erythritol, lactitol, maltitol, isomaltitol are applied in confectionery products, chewing gums, and mixed juices. In this research, capillary zone electrophoresis was used to build up a basic analysis model to simultaneously analyze sugar alcohols.

糖醇的种类可分为单糖醇与双糖醇,主要应用的单糖醇有甘露糖醇、山梨糖醇、木糖醇、丁四醇,而双糖醇则有乳糖醇、麦芽糖醇和异麦芽酮糖醇(isomaltitol,又称为巴糖醇,palatinitol)等。

The monosaccharides in LBP-4 identified by GC were xylose , galactose , mannose , Rhamnose , glucose and arabinose with the molar ratio of 4. 45: 1. 20: 1. 0: 0.98: 0.90: 0.85. The content of calcium, magnesium, zinc and iron in LBP-4a were 127. 9070mg·g〓, 32. 3953mg·g〓, 0.3845mg·g〓 and 0.2930mg·g〓, respectively. The content of galacturnic acid in LBP-4a was 55. 45% while the content of protein is 3. 80%. According to IR spectra, it contains -COOH group,-NH- roup,-OH group,-NH〓 group and β-D-glucose. The backbone of sugar residues chain in LBP-4a were contained 1→6 indican bond according to periodate oxidation and the results of β-elimination reaction indicated that the chain of polysaccharides and protein were connected by O-linked chemical bond. The photograph of LBP-4a got by laser scanning confocal microscope and scanning electron microscope showed that the LBP-4a combined both with each other and with itself in its crystalloid. The crystalloid was flake and anisotropic.

由LBP-4a的红外光谱图知:LBP-4a中含有-COOH、-OH和-NH〓或-NH-基团,糖链中含有β-D-吡喃葡萄糖;高碘酸氧化实验知LBP-4a糖链中不具有连二羟基和连三羟基结构的单糖残基:具有连二羟基结构的单糖残基:具有连三羟基结构的单糖残基=57.0:16.2:1,六碳糖残基的连接中含有1→6连接的糖苷键;通过β消去反应证明LBP-4a中多糖链和氨基酸间为-O-型连接;由激光扫描共聚焦显微镜和扫描电镜对LBP-4a结晶观察结果推测:LBP-4a结晶中同时存在分子间和分子内结合的现象,LBP-4a分子相互结合时,并不是无规则的相互缠绕形成无规线团结构,而是形成片层结构,并且LBP-4a结晶可能具有各向异性的性质。

Monosaccharides are classified according to (1) the number of carbon atoms present in the molecule and (2) whether they contain an aldehyde or keto group, thus a monosaccharide containing six carbon atoms is called hexose; a monosaccharide containing an aldehyde group is called aldose; and one containing a keto is called a ketose.

单糖的分类按照(1)分子中碳原子的数目(2)是否含有一个醛基或酮基,因此一个单糖含有6个碳原子叫做己糖;一个单糖含有醛基叫醛糖;含有酮基叫酮糖。

Chapter 4 Capillary Zone Electrophoresis with Amperometric Detection forComposition Analysis of LaminarinThe composition of laminarin was firstly determined by analyzing its hydrolysis monosaccharides with capillary zone electrophoresis - amperometric detection.

第四章毛细管电泳一安培检测法测定昆布中多糖成分本论文首次用毛细管电泳一安培检测法测定了昆布多糖水解单糖的成分,实现对(来源:Aa4BC9b2b论文网www.abclunwen.com)昆布多糖的测定。在选定的最佳条件下,昆布多糖水解产物岩藻糖、半乳糖、葡萄糖、甘露糖、木糖在20min内实现完全分离而且在铜电极上有着很好的电流响应。通过对昆布多糖中水解单糖成分含量的计算显示该多糖中岩藻糖、半乳糖、葡萄糖、甘露糖、木糖的摩尔比为

The Infrared Spectrum,monosaccharide composition, periodate oxidation and partial acid hydrolysis were also used to give out details of MHP structures information.

采用红外光谱法,单糖组成,部分酸水解和高碘酸氧化等相关分析方法对MHP-2中单糖的连接方式及主链、支链的单糖各键型的比例进行了研究表明虫草多糖中的单糖组成为甘露糖:葡萄糖:半乳糖三种单糖=

By means of GPC,IR,GC-MS,~(13)CNMR,~1HNMR,Methylation analysisetc,structural properties of PST-1 were identified as follows:The Mwof PST-1 was 3.44×10~6 Da and its optical rotation was _D~(20)=+0.110°(c0.1, H_2O); PST-1 constituted 8 simple sugars and the molar ratio was 2,4-Dimethoxy-Mannose:Rhamnose:Ara-binose:Xylose:Galactose:D-Galacturonic acid:Mannose:D-glucuronic acid=2%:5%:24%:9%:3%:1%:46%:10%;The chief bone of PST-1 was 1,3,6-linked-β-D-Man residue and the side chains contained Furanoid and Pyranoid residues.

结合GPC、旋光度测定、IR、GC-MS、~(13)CNMR、~1HNMR、高碘酸氧化法、Smith降解以及甲基化方法等分析测试方法,得到PST-1的单糖组成及结构表征,实验结果如下:红豆杉多糖PST-1是重均分子量为3.44×10~6 Da的支链多糖,旋光度为20D=+0.110~0(c0.1,H_2O);PST-1单糖组成为:2,4-Dimethoxy-Mannose:Rhamnose:Arabinose:Xylose:Galactose:D-Galacturonic acid:Mannose:D-glucuronic acid=2%:5%:24%:9%:3%:1%:46%:10%;PST-1的骨架结构为:具有1,3,6-连接的β-D-甘露糖残基骨架,侧链分枝包括非还原末端的呋喃型α-L-阿拉伯糖残基、吡喃型α-L-阿拉伯糖残基、β-D-木糖残基、β-D-甘露糖残基、2,4-二氧甲基-β-D-甘露糖残基和α-D-葡萄糖醛酸残基;侧链的糖残基也可能存在2,5-二氧-取代呋喃型α-L-阿拉伯糖基、3-氧-取代的β-D-木糖残基、6-氧-取代的α-D-半乳糖醛酸残基、6-氧-取代的α-D-半乳糖残基、4-氧-取代的α-D-葡萄糖醛酸残基和2-氧-取代的α-L-鼠李糖残基,同时后者也可能穿插在主链上。

Thederivatives of 5 kinds of monosaccharides Xyl, Ara, Man, Glc, Gal were detected anddetermined respectively by GC-MS. The influences of several factors, such asreductive time, reductive temperature, acetylating temperature and acetylating time,on recovery of monosaccharides were studied by orthogonal experiments. The resultsshowed that the reductive temp.

利用气相色谱—质谱联用技术检测五种常见单糖(木糖、阿拉伯糖、甘露糖、葡萄糖、半乳糖)的乙酰化产物含量,采用正交试验综合考察了还原时间、还原温度、乙酰化温度、乙酰化时间等因素对单糖回收率的影响及规律。

Monosaccharide Isomerization Simple aldoses and ketoses containing the same number of carbon atoms are isomers of each other; that is, a hexose and a hexulose both have the empirical formula (C6 H1206 )and can be interconverted by isomerization.

单糖异构化含有相同数目碳原子的单醛糖和酮糖互为同分异构体,也就是说一个已醛糖和一个已酮糖都符合经验分子式C6 H1206,并且可通过异构化作用相互转化

Results Method I of gas chromatography can't be used for determination of monosaccharide in spirulina glucoprotein, while method 2 was suitable, and 7 monosaccharides were found in ion chromatography.

结果 气相色谱法1不适于藻糖蛋白单糖分析,气相色谱法2较适合藻糖蛋白单糖分析;离子色谱法测得藻糖蛋白含7种单糖

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。