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The miscibility, molecular interaction of the two components and structure of condensed mixed momolayers were investigated in details.

对不同组分的Ru2+3[简称Ru]与花生酸在纯水亚相上的混合单分子膜的相容性、分子间相互作用以及凝聚单分子膜的结构进行了研究。

In the chiral SU(3) quark model, we use the coupling between quarks and nonet scalar meson fields and nonet pseudo-scalar meson fields to describe the medium and long range interactions, and use one gluon exchange to describe the short range interaction. In the extended chiral SU(3) quark model, besides the nonet pseudo-scalar meson fields and the nonet scalar meson fields, the coupling between vector meson fields and quarks is also considered, the short range interaction can be dominately described by vector meson exchange. We investigate the nucleon-hyperon interaction in the extended chiral SU(3) quark model and study the S-wave phase shifts of N-Λ and N-Σ systems. Comparing to the results in chiral SU(3) quark model, we find that the short-range interaction could be described either by the one-gluon exchange or vector meson exchange.

在手征SU(3)夸克模型中,用夸克与标量介子九重态和赝标介子九重态场的耦合来描述中长程相互作用,单胶子交换来描述短程相互作用,推广的手征SU(3)夸克模型是在原来手征SU(3)夸克模型的基础上进一步引入了夸克和矢量介子九重态场的耦合,主要由矢量介子交换来描述短程相互作用,在推广手征SU(3)夸克模型下研究了核子-超子相互作用过程,计算了N-Λ和N-Σ相互作用的S波散射相移,通过和手征SU(3)夸克模型的结果比较,发现N-Λ和N-Σ系统的短程相互作用既可以由单胶子交换来描述,也可以由矢量介子交换来描述。

In comparison to scalar wavelets, multiwavelets simutaneously have several advantages such as compactsupport, orthogonality symmetry and so on, which are known to be important in signal processing. Thus, multiwavelets offer the possibility of superior performance for image processing applications.

与单小波相比较,多小波同时具备诸如紧支性、正交性、对称性等诸多在信号处理中非常重要的良好性质;这决定了多小波是一种优于单小波的信号处理技术。

The results showed that the sintered dielectric was a kind of glass-ceramics. The crystals in the dielectric included Hexacelsian and Celsian. Celsian would affect the insulation properties of the dielectric seriously.

研究结果表明,烧结后的介质层是微晶玻璃,主要有六方钡长石(Ba[Al_2Si_2O_8])和单斜钡长石两种晶相,单斜钡长石的存在严重影响了介质层的绝缘性能。

With increasing monomer concentration inside the disperse phase, the monodispersity of emulsions became slightly worse and the mean diameter of emulsions gradually became smaller. Monodisperse monomer-containing emulsions were obtained when the SPG membrane pore size was larger than 1.0 μm; however, when the SPG membrane pore size was smaller than 1.0 μm, no monodisperse emulsions were obtained because of the formation and chokage of p-phthalic acid crystals in the pores of the SPG membrane.

当SPG膜孔径大于1.0 μm左右时,可得到单分散的含TDC单体乳液;而当孔径小于1.0 μm左右时,水分子更容易扩散并溶解到油水界面甚至油相内部与TDC生成对苯二甲酸,TPA积累到一定程度在油水界面上析出将膜孔堵塞,从而无法制得单分散乳液。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现;3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布;4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒;5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明:1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致;2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响;3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现; 3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布; 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒; 5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明: 1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致; 2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响; 3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。

Part II:The electrocatalytic oxidation of guanine, adenine, guanosine-5'-monophosphate and ssDNA was performed in the presence of iron bis(2,2':6',2"-terpyridine) and Fe tris(1,10-phenanthroline) complexes as a homogeneous catalysts with Fe redox couple. The electrocatalytic and electroanalytic properties of guanine with an iron bis(2,2':6',2"-terpyridine) complex was measured by the amperometry method using the rotating disk electrodes. Electropolymerization of iron tris(5-amino-1,10-phenanthroline) complex produced thin polymer films on a gold, platinum, nickel, and glassy carbon electrode.

第二部分利用iron bis(2,2':6',2&-terpyridine)和Fetris(1,10-phenanthroline)之金属错合物当作均相的催化剂对於鸟嘌呤、腺嘌呤、5'-鸟嘌呤核苷单磷酸盐(guanosine-5'-monophosphate)和单股DNA进行电催化氧化的研究。iron bis(2,2':6',2&-terpyridine)之金属错合物对於鸟嘌呤的电催化和电分析性质可利用计时安培法并使用旋转环-碟电极进行测量。rontris(5-amino-1,10-phenanthroline)之金属错合物可经由电聚合过程所形成的聚合薄膜固定在黄金、白金、镍和玻璃碳电极上。

Lastly, based on analysis on phylogentic relationships among 39 ciliates combined with their main morphologic characters, some conclusion were drawn: 1 the monophyly of the peritrichs was strongly supported, and its subclass rank in the class Oligohymenophorea is reasonable; 2 the genus Epistylis might not be monophyletic, and the peristomial area, especially the peristomial lip, might be an important phylogenetic character within the genus Epistylis; 3 the taxonomic rank of the genus Carchesium and the genus Campanella were suggested to be adjusted; 4 Opisthonecta probably diverged from peritrichs with stalks; 5 the phylogenetic tree of peritrichs was reconstructed based on the molecular information inferred from SSrRNA gene sequences and the morphology.

测定了6科8属13种缘毛类纤毛虫的SSrDNA序列,将构建的最大简约树和邻接树与形态学相结合,分析得出:1)缘毛类纤毛虫是单系的,其分类地位是隶属于纤毛门寡膜纲缘毛亚纲:2)指出累枝虫属可能不是单系的,口围区是累枝虫属中重要的系统发育特征;3)建议调整独缩虫和聚钟虫属的分类地位;4)得出后游虫可能是由有柄缘毛类进化而来的类群;5)基于缘毛类反口区结构和SSrRNA基因序列提供的信息重建了缘毛类纤毛虫的系统发育树。

By the extraction and derivation of gastrodia elata, the content of monose in gastrodia elata leaves is analyzed by capillary chromatography and five kinds of monose are determined.

通过对天麻的提取和衍生处理,采用毛细管气相色谱法分析了天麻中可溶性单糖含量,鉴定出天麻中含有5种单糖。

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But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊!不用提了。提到肉,真是糟透了。

Tristan, I have nowhere to send this letter and no reason to believe you wish to receive it.

Tristan ,我不知道把这信寄到哪里,也不知道你是否想收到它。