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At the same time, at the aspect of theory, we givea lot of results, including: performance calculating formula of FFT phase comparing,coincidence relation of calculating result and target' s real range, calculatingformula under zeroize FFT or single channel.

在相关理论上,我们提出了FFT比相的性能指标计算公式、FFT比相下测距结果与目标实际位置之间的对应关系、补零和单通道下的FFT比相结果。

The antimicrobial test and researched was done on wide distillation of different solvents on Terpenoid, polarity separation of ethanol distillable substance, thin layer chromatography of different polarities and distillation of amylase. The results showed that the active substance distilled by 95% ethanol and V methanol: toluene=3:1 had stronger antimicrobial activity on Agaricus blazei Murrill. The antimicrobial activity of ethyl acetate was stronger than wide distilling substance with ethanol, but the water part has not antimicrobial effect. Two straps of ethyl acetate phase(Rf0.57、Rf0.63)(0.1g/ml)had stronger antimicrobial activity on Agaricus blazei Murrill, the antimicrobial zone on Pseudomonas was 19.3mm. The bacteriostatic activity of chromatography strap of water phase was rather weaker, the water solution (0.5g/g) of amylase had better effect on pathogenic fungus of Agaricus blazei Murrill, its antimicrobial zone on Aspergillus niger, Citrinin, Trichoderma viride were 10.8 mm, 7.9 mm, 5.3 mm.

通过对日本凹顶藻以不同溶剂的粗提、乙醇提取物的极性分离、不同极性的薄层层析和多糖的提取,进行抗菌试验的研究,发现95%乙醇和V甲醇:甲苯为3∶1的提取的活性物质具有较强的抗姬松茸的病原细菌活性,乙酸乙酯相对病原细菌的抑菌强于乙醇的粗提物,而水相基本无抑菌效果,乙酸乙酯相的两个带(Rf0.57、Rf0.63)浓度为0.1g/ml具有较强抗姬松茸病原细菌的活性,对假单孢杆菌抑菌圈达到19.3mm,水相层析带的抑菌活性较弱,多糖的粗提物配成0.25g/g的水溶液对姬松茸病原真菌有较好的抑菌效果对黑曲霉、桔青霉和绿色木霉的抑菌圈分别达到10.8 mm、7.9 mm、5.3 mm。

Specifically, itcontains 8 chapters.In chapter 1, the formation, structures, properties and the futureprospect of liposome were thoroughly reviewed;In chapter 2, the stibility and permeability of phopholipid -eleostericacid liposome were studied together with the effect of polymerizationof eleostearic acid. This membrane system was very sensitive to 〓,the effect of 〓 was clarified to increase the aggregation/fusion ofliposomes and made the permeability of mixed liposomes much higher;In chapter 3, two polymerizable conjugated diyne bolaamphiphiles were synthesized. They could form very stable mixed liposome, andthe diyne could be polymerized by UV light in bilayer liposomes, as aresult, the stability of mixed liposome against solvent or surfactantafter polymerization were enhanced. In chapter 4, two kinds of amphiphilic amino acids were synthesized andstable liposomes were formed therefrom After the condensationpolymerization of amino acid in bilayer liposomes, stable polypeptide liposomes were obtained, which had lower phase transition temperatureand higher permeability.In chapter 5, four kinds of glycolipids were synthesized and theiraggregation behavior in water was comparied. When incorporated intophospholipid bilayer membranes, they could increase the phase transitiontemperatures and inhibit the aggregation and fusion of mixedliposomesat lower temperature.In chapter 6 and 7, three kinds of steroidal bolaamphiphiles withdifferent chain lengths were synthesized. Incorporation of steroidalmoiety to the center of lipid bilayer membrane obviously increased themobility of lipid membrane and shifted Tc to lower temperature side incomparasion with cholesterol. The bolaamphiphile which was shorter thanthe hosted lipid bilayer membrane thickness influenced the lipid packingmore obviously.

全文共分8章:第一章对脂质体的形成、结构、性质及展望进行了较为详细的文献综述;第二章研究了磷脂-桐酸脂质体的稳定性,通透能力及桐酸的聚合对这些性质的影响;磷脂-桐酸混合脂质体为一类对〓灵敏的脂质体,〓的作用首先是使脂质体集聚然后使脂质体融合,并加速内包荧光物的释放;第三章通过合成两种可聚合共轭双炔双极性双亲分子DDCA,DDOL,研究了共双炔分子在双分子层脂质体膜上的聚合及对脂质体性质的影响,聚合可以提高脂质体相对于溶剂及表面活性剂的稳定性;第四章合成了两类氨基酸为极性基团的双亲分子,它们均可以在超声下形成稳定的脂质体结构;氨基酸基团可以在脂质体上进行缩聚反应,若聚合后脂质体表面仍有足够的亲水能力,则可得到稳定的多肽型脂质体;聚合后脂质体的相变温度降低,通透能力增加;第五章合成了四种亲水基团为单糖基的双亲分子GL-l,GL-2,GL-3, GL-4,研究了它们在水中的分散情况、集合体形态与分子结构的关系;在DMPC双分子层膜中加入糖脂分子可以使脂质体的相变温度提高,阻止脂质体在低温放置时的集聚与融合;第六章-第七章合成了三种不同碳链长度的双极性含胆甾环双亲分子 CL-1,CL-2,CL-3;它们可以象胆固醇一样与磷脂混合形成稳定脂质体,胆甾环基团位于脂质体双分子层膜的中间;与胆固醇的作用相反,它们可以增加磷脂双分子层膜的流动性,降低混合脂质体的相变温度;三种分子的作用与其碳链长度和磷脂双分子层膜的厚度有关,比膜厚度短的分子影响最大。

Differential scanning calorimetry and polarizing microscope were used to study their liquid properties. Among them, nine are found to exhibit liquid crystal properties, and most of them displayed as heating monotropic liquid crystals. There are one or two mesophases and certain phase transition temperature,Δ H and temperature range of liquid crystal.

用差示扫描量热仪和偏光显微镜研究了其液晶性,发现其中九个配合物具有液晶性,多为升温单变液晶,有一至两个中介相,有确定的相转变温度、热焓和相变区间。

The metastable phase equilibrium of the quaternary system Na(superscript +)∥Cl(superscript -), CO3(superscript 2-), B4O7(superscript 2-)-H2O was studied at 273 K by isothermal evaporation method, the solubility and density of the equilibrium solution of this system were determined and the metastable equilibrium phase diagram was plotted in line with the experimental data. The phase diagram of the system consists of three univariant curves, three crystallization fields and one invariant point.

采用等温蒸发法研究简单四元体系Na∥Cl,CO3(上标 2-),B4O7(上标 2-)-H2O273K时的介稳相平衡,并测定该体系273K平衡液相中各组分的溶解度及密度,该体系的介稳相图和密度组成图显示:该四元体系在273K时的相图由3条溶解度单变量线、3个结晶区及1个共饱和点组成。

Based on the solubility data, the phase diagram of the system was plotted, which consists of three univariant curves E1E, E2E and E3E, one invariant point E and three crystallization fields: KCl, K2B4O74H2O and K2SO4 The experimental result s show that potassium chloride had the salting-out effect on potassium borate (K2B4O74H2O), and potassium sulphate (K2SO4) Meanwhile, the law of density was discussed briefly.

根据实验数据绘制了相应的相图。相图中有一个共饱点E,三条单变曲线E1E,E2E和E3E;三个结晶区平衡固相分别为:K2B4O74H2O,K2SO4和KCl。实验结果表明KCl对K2B4O74H2O和K2SO4有盐析作用,并简要讨论了密度变化规律。

The experimental results showed that the double salt Na2SO4·MgSO4·4H2O forms in the quaternary system Na+,Mg2+//SO42-,B4O72--H2O at 288K. The quaternary system has three invariant points F1,F2, and F3, seven univariant curves E1-F1,E2-F1,E4-F3,E5-F3,E3-F2,F1-F2,F2-F3, and five fields of crystallization [Na2SO4·MgSO4·4H2O,Na2B4O7·10H2O,Na2SO4·10H2O, MgSO4·7H2O,MgB4O7·9H2O].

研究结果表明:交互四元体系Na+,Mg2+//SO42-,B4O72--H2O 288K时的相平衡实验中,有复盐Na2SO4·MgSO4·4H2O生成,平衡相图中有3个共饱点,7条单变量曲线,5个结晶区,对应的平衡固相分别为Na2B4O7·10H2O,MgB4O7·9H2O,Na2SO4·10H2O, MgSO4·7H2O和Na2SO4·MgSO4·4H2O。

The former is believed to be the transformation of finer particles while the latter for coarser ones.

第二阶段相变是熟知的大颗粒单斜相到四方相的转变,它的发生伴随着大的体积收缩。

The symmetry of the antiferroelectric phase of PbZrO3 was reinvestigated by the symmetry element analysis based on the projective figures given in the related literatures.

在参考文献给出的锆酸铅的反铁电相投影图的基础上,从生群元的角度重新研究了反铁电体锆酸铅的反铁电相的对称性,发现锆酸铅反铁电相的对称群应是P2/m,属于单斜晶系。

"During a part of each oscillation, a region whose pressure is above the equilibrium pressure is formed."

平衡相可由三元相图中的单相和两相区的交界线上的两点表示。

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