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Results showed that the monomer conversion increased slightly in the presence of the crosslinking agents The size of particles decreased slowh as the amount of cmsslinking agent increased.and the size distribution of the particles broadened at a higher amount of cmsslinking agent Divinyl benzene was more effective than ethyl glycol dimethyl methacrylate to make polymer crosslinked.During alkali treatment process,void latex particles can be obtained when no DVB or less than 0.5 wt% of EGDMA was used,while muhihollow structure was generated when DVB or more than 1.0 wt% of EGDMA was introduced.The volume expansion of the particles decreased with increasing the amount of emsslinkirlg agents.

结果表明,体系中加入交联剂后,单体转化率都有不同程度的提高;随交联剂用量的增加,乳胶粒粒径略有减小,交联剂用量较高时,乳胶粒粒径分布加宽;二乙烯基苯的交联效率稍高于双甲基丙烯酸乙二醇酯;不加入交联剂及EGDMA用量低于0.5%时,处理后乳胶粒呈空腔结构,加入DVB及EGDMA用量高于1.0%时,处理后乳胶粒呈多孔结构,并且乳胶粒体积增量随交联剂用量的增加而减小。

Dibutyltin maleate,dioctyltin maleate,N-phenyl maleimide, N-(p-chlorophenyl) maleimide,N-(p-nitrophenyl) maleimide with unsaturated groups were synthesized using dibutyltin oxide,dioctyltin oxide,maleic anhydride, aniline,p-chloroaniline,p-nitroaniline as raw materials,respectively.Then dibutyltin male,ate/styrene bipolymer,dibutyltin maleate/styrene/methyl acrylate terpolymer,dibutyltin maleate/styrene/N-phenyl maleimide terpolymer ,dibutyltin maleate/styrene/N-(p-chlorophenyl) maleimide terpolymer ,dibutyltin maleate/styrene/N-(p-nitrophenyl) maleimide terpolymer ,dioctyltin maleate/styrene biopolymer,dioctyltin maleate/styrene/methyl acrylate terpolymer,dioctyltin maleate/styrene/ N-phenyl maleimide terpolymer,dioctyltin maleate/styrene/ N-(p-ehlorophenyl) maleimide terpolymer[P(DOTM/St/NC1PMI)],dioctyltin maleate/styrene/N-(p-nitrophenyl) maleimide terpolymerwere synthesized using DBTO,DOTO,PMI,N-p-ClPMI,N-p-NOPMI,styrene and methyl acrylate as monomers,respectively.

再以DBTO,DOTO,PMI,N-p-ClPMI,N-p-NOPMI,苯乙烯,丙烯酸甲酯等为单体,合成了马来酸二丁基锡/苯乙烯二元共聚物{P},马来酸二丁基锡/苯乙烯/丙烯酸甲酯三元共聚物{P},马来酸二丁基锡/苯乙烯/N-苯基马来酰亚胺三元共聚物{P(DBTM/St/NPMI)},马来酸二丁基锡/苯乙烯/N-对氯苯基马来酰亚胺三元共聚物{P(DBTM/St/NClPMI)},马来酸二丁基锡/苯乙烯/N-对硝基苯基马来酰亚胺三元共聚物{P(DBTM/St/NNOPMI)},马来酸二辛基锡/苯乙烯二元共聚物{P},马来酸二辛基锡/苯乙烯/丙烯酸甲酯三元共聚物{P},马来酸二辛基锡/苯乙烯/N-苯基马来酰亚胺三元共聚物{P(DOTM/St/NPMI)},马来酸二辛基锡/苯乙烯/N-对氯苯基马来酰亚胺三元共聚物{P(DOTM/St/NClPMI)},马来酸二辛基锡/苯乙烯/N-对硝基苯基马来酰亚胺三元共聚物{P(DOTM/St/NNOPMI)}。

According to different acidity of free Flavonoids in Resina Draconis, different acidic lavonoids were extracted with the pH gradient extraction method from ethyl ether.

根据血竭中游离黄酮存在着酸性差异,采用溶剂除杂,转溶于乙醚,再用pH梯度萃取得到不同酸性的黄酮,进而对弱酸性组分分离纯化得到2个单体化合物。

It includes the introduction of prediction method,test of groups of highway bridges by artificial neural network and importing theconception of ductibility .

文章主要内容为:简要介绍目前桥梁震害预测的方法;在桥梁群体震害预测成果的基础上应用人工神经网络进行结论验证;在单体桥梁推倒分析中引入了延性的概念,并结合实例予以分析。

I found that the major distinction for gene duplicability in protein complexity is between hetero-complexes, each of which includes at least two different types of subunits, and homo-complexes, which include monomers and complexes that consist of only subunits of one polypeptide type.

结果发现,基因可复制性在异复合体(由两种以上的次单元所构成的复合体,hetero-complexes)及同复合体(单体或是单一种次单元所构成的复合体,homo-complexes)之间存在明显的差异。

In this paper, synthetic process of PTT and cationic dyeable PTT was studied, including molar ratio, catalyst concentration, reaction time and temperature, types of antioxidants in the esterification reaction and the condensation reaction.

研究了聚对苯二甲酸丙二醇酯、阳离子染料可染PTT的合成工艺条件中各因素对酯化及缩聚反应的影响,包括单体物质的量比、催化剂浓度、反应时间和温度、抗氧剂种类等。

In order to approach the industrialization continuous production flow, the article studied production of acid dyeable polyacrylonitrile by the continuous water phase suspension polymerization using the existing laboratory instrument. The influence of third monomer and initiator content on productivity and dye uptake of PAN were investigated.

为了接近工业化的连续生产流程,利用实验室现有的仪器设备,设计了连续水相悬浮法生产酸性染料可染聚丙烯腈的实验装置,实现了聚丙烯腈的连续聚合,并研究了第三单体、引发剂用量对聚丙烯腈上染率、产率的影响。

An acid dyeable polyacrylonitrile blend fiber was prepared by blending polyacrylontrile and a copolymer syn-thesized from trihydroxy methyl-aminomethane containing basic groups and acrylonitrile raonomr via wet spinning process.

用含有碱性基团的丙烯酸氨基酯与丙烯腈单体共聚,其共聚物与聚丙烯腈共混,经湿法纺丝制备酸性染料可染PAN共混纤维。

Through comparing with commercial low molecular emulsor, the effect of DMPA content on the surface-active ability of PEPUD was researched and an available DMPA content in the synthetic fomulation of PEPUD suitable for acrylate monomer emulsification was determined.

研究了DMPA含量对可聚合自乳化聚氨酯水分散体表面活性能力的影响,通过与商用低分子乳化剂的表面活性能力进行对比,确定了其符合丙烯酸酯单体乳化要求的合成配方中DMPA的适宜含量。

APUHD was prepared with PEPUD acted as emulsor and reactive seeded emulsion in polymerization of acrylate monomer.

利用可聚合自乳化聚氨酯水分散体作为乳化剂和反应性的种子乳液与丙烯酸酯等单体共聚,其优点在于能调节聚氨酯水分散体侧链上参与共聚的双键数目,使聚氨酯和丙烯酸酯两相聚合物体系间直接化学键合增强,相容性提高,增加体系内部交联密度,合成得到具有核壳间互穿网络结构的丙烯酸聚氨酯杂合水分散体。

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