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Temperature-sensitive hydrogels P(NIPA-co-DiAB) with aromatic group as hydrophobe was were prepared by free radical micellar crosslinking copolymerization with N-isopropyl acrylamide, N,N-dially benzylamine as comonomers, N,N-methylene-bis-acrylamide as crosslinker, sodium dodecyl sulfate as surfactant and ammonium persulfatetetramethylethylenediamine as initiator system.

以N-异丙基丙烯酰胺、N,N-双烯丙基苄胺为共聚单体、N,N-亚甲基双丙烯酰胺为交联剂、十二烷基硫酸钠为表面活性剂、过硫酸铵-四甲基乙二胺为氧化还原引发体系,采用自由胶束交联共聚法合成了疏水基团为芳香基的疏水改性温敏性智能水凝胶P(NIPA-co-DiAB)。

Two novel soluble poly, poly [(3-butyrylpyrrole-2, 5-diyl) p-nitrobenzylidene] and poly [(3-butyrylpyrrole-2, 5-diyl)(3-hydroxy-4-methoxy) benzylidene], were synthesized firstly by condensation of 3-butyrylpyrrole with p-nitrobenzaldehyde and vanillin, respectively.

通过3-丁酰基吡咯单体分别与对硝基苯甲醛和香草醛的缩聚反应,成功合成了两种新型可溶性聚吡咯甲烯衍生物-策[(3-丁酰基吡咯-2,5-二)对硝基苯甲烯]和聚[(3-丁酰基吡咯-2,5-二)(3-羟基-4-甲氧基)苯甲烯]。

The major results obtained are: PCR-RFLP method is suitable for molecular identification of Shihu; 205 compounds were isolated from 10 species of Dendrobium, including 21 new compounds, and 28 compounds isolated from genus Dendrobium for the first time. Each of the extracts and compounds were screened for anticoagulant and antitumour activities separately. The results indicated that the ethyl acetate extract from Dendrobium chrysanthun has significant anticoagulant function; the antitumour function of the 4 bibenzyl components from Dendrobium chrysotoxum is stronger than that of phenanthrene, of which the erianin has significant anti-angiogenic effect both in vivo and in vitro; components with moderate or stronger antitumour activities were found in the extracts of D. thyrsiflorum, D. chrysanthun and D. trigonopus; quality standard for 5 species of Dendrobium was drawn up use active or indicative components as control.

重要研究结果有:经方法学研究,认为PCR-RFLP法适于作为石斛属药材分子标记鉴定方法;对10种石斛进行化学成分分离鉴定,共分得205个化合物,其中新化合物21个,首次从石斛属分得的28个;对提取物和各单体化合物分别作抗凝血、抗肿瘤等活性筛选,结果说明束花石斛乙酸乙酯部位有显著的抗凝血作用,鼓槌石斛的4个联苄类成分抗肿瘤作用强于菲类,联苄类毛兰素在体内外有显著抗血管生成活性,球花石斛、束花石斛及翅梗石斛均筛到中等或较强抗癌活性的成分;选择有活性或指标性成分作对照品,对5种石斛草拟了质量标准。

Because the solubility of the complex monomers is very important for polymerization, the bidentate ancillary ligand of the bicycloiridium complexes also has an effect on the luminous properties of the chelating polymer.

实验证明了在这类电磷光聚合物中配合物单元辅助配体合理的分子设计,可以提高配合物单体的溶解度,提高聚合物的分子量和发光性能。

The introduces binaphthyl bisphenol monomer on side-chain benzene ring of sulfonic group on molecular level, prepares sulfonated poly aryl ether with sulfonic group only on naphthalene ring of side chain, so that ensures chemical stability of main chain with high molecular weight, while having no influence on mechanical property thereof.

本发明从分子水平出发,将磺酸基在侧链苯环上的联萘双酚单体引入,制备仅在侧链苯环上有磺酸基的磺化聚芳醚,从而保证了高分子主链的化学稳定性,且不会影响其优异的物理机械性能。

The asymmetric polymerization of methyl methacrylate is carried out using the chiral binaphthyl crown ether macrocyclic compounds binding n-BuLi or t-BuOK as chiral initiator at -78℃.

以手性联萘冠醚为配体,络合n-BuLi,t-BuOK等有机金属化合物形成手性引发剂体系,初步探讨了甲基丙烯酸甲酯单体的聚合反应。

On the other hand, the formation of peptide and protein from amino acids is a central biosynthetic process in all living systems.

摘要在原始海洋中,生物聚合物的前生物合成包括活性单体的缩合和脱水过程。

Using levulinic acid and phenol as raw materials, hydrochloric acid as catalyst and thioglycolic acid as assistant catalyst, the synthesis technology of diphenolic acid, a new polymer material substitution for biphenol A, was investigated.

研究了以苯酚和新型平台化合物乙酰丙酸为原料,采用盐酸为催化剂、巯基乙酸为助催化剂催化合成高分子材料单体双酚酸的合成工艺。

First,from molecular aspect,a novel copolymer-PPBES has successfully been synthesized by nucelophilic substitution reaction with biphenol,4-(4-hydroxyphenyl)-phthlazin-1(2H)-one and 4,4\'-dichlorodiphenylsulfone,which has both twisted and linear molecular structures in the backbone.

本文从分子设计出发,首先选用联苯二酚与4-(4-羟基苯基)-2,3-二氮杂萘-1-酮和4,4′-二氯二苯砜为共聚单体,采用溶液亲核取代逐步缩聚合方法,合成了一系列含有杂萘联苯结构和联苯结构的新型共聚芳醚砜。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

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