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According to the heat release rate, the reaction pathway to ignition of sample alkane is analyzed.

利用新型的绝热量热仪研究了两种典型烷烃的自加热过程,采取了增大样品容器体积和加压的方法,得到了正庚烷和正十六烷的初始反应温度、大升温速率和最大升温速率对应的温度。

In the real bake-out process, it suggests that the air excess coefficient of burning should be controlled within 1 in order to avoid electrode being oxidized by high temperature fume; when the temperature is below 700 C, it rises slowly in temperature to bake out thoroughly and uniformly; when above 700 C, it speeds up in heating-up to reduce the electrode oxidation.

在实际焙烧过程中,为了减少高温烟气对电极的氧化,建议燃烧的空气过剩系数控制在1以下;700℃以前缓慢升温,以达到焙烧彻底、均匀的目的;在700℃以后,加快升温速度,以减少电极的氧化。

The critical heating rate for different body radius was predicted by comparing the gas pressure when the peak degradation rate occurred with the threshold body strength which was determined by the diametric compression test of the green body during thermal debindering.

摘 要:以聚乙烯醇和NiFe2O4/Ni型金属陶瓷压坯为对象,采用热重分析研究PVA在N2气氛中的热脱脂行为,建立PVA热脱脂速率的数学模型,在此基础上,模拟并计算PVA分解产物气体在多孔粉末压坯内的压力构建情况;结合粉末压坯脱脂强度测试结果,分析粉末压坯在脱脂过程中压坯尺寸、粘结剂含量等因素对升温速率和脱脂时间的影响,获得不同半径尺寸压坯的极限升温速率。

However,for free decay method,its range of changing frequency is very narrow and the initial states of samples are not easily repeated because of the effect of crystallization;for forced oscillation method,the measuring results are seriously affected by crystallization,which is caused by slow heating rates.

然而,自由衰减法有限的变频范围,以及由于受晶化的影响,使两次升温测量时样品的初始状态不易重复;用强迫振动法测量时,同步变频条件限制了升温速率,造成金属玻璃的晶化过程严重影响了测量结果。

Effect of sulfurization time, water content, oil as well as sulfur on spontaneous combustion of iron sulfide is investigated on the same sulfide formed from Fe2O3. It indicates that long sulfurization time, some oil, sulfur as well as good ventilation condition could accelerate oxidation and temperatures rise, but uncertain water content and poor ventilation condition lessen the spontaneous combustion tendency.

以Fe2O3的硫化产物为典型样品,研究了硫化时间、水分、油品、硫及通风条件对硫化铁氧化升温特征的影响,结果表明,硫化时间长,适量的油品和硫以及良好的通风条件能够加速硫化铁升温过程,而一定的水分及不良的通风条件则降低了硫化铁的自燃倾向性。

The invention provides a preparation method of small crystal SAPO-43 molecular sieve, which is characterized in that: the stepwise procedures are adopted to synthetize SAPO-43 molecular sieve, temperature-rising rate in different temperature phase during crystallization is controlled, so that the synthetized SAPO-43 molecular sieve has small particles, even crystal particles, short crystallization time, and reduce the amount of templates greatly, thereby reducing environmental pollution.

本发明的目的是提供一种小晶粒SAPO-43分子筛的制备方法。本发明的特点在于它是采用分阶段程序升温来快速合成小晶粒SAPO-43分子筛。通过对晶化过程中不同温度段内升温速率的控制,从而实现了合成的SAPO-43分子筛晶粒小,晶粒尺寸分布均匀,晶化时间短,且大大的降低了模板剂的用量,从而减少了对环境的污染。

Based on the method of stepwise increasing temperature in the process of polymerizing PDMDAAC initiated by APS which has been successfully studied in our research group, the optimal method of increasing temperature in the polymerization initiated by the AIBA.2HC1 was found.

以本课题组在采用APS引发DMDAAC水溶液聚合时的所用的梯度升温方式为基础,通过实验得到了适合于AIBA·2HCl引发DMDAAC水溶液聚合时的梯度升温方式中各阶段的最佳温度。

The oil yield of six types of Huadian oil shales were measured on a Fischer assay retort,and the factors which effected the results of Fischer assay of oil shale were investigated,such as heating rate,particle size,final retorting temperature and retorting persistent time.

结果表明,页岩油的产率随着挥发分含量的增大而增加,在一定范围内提高升温速率,页岩油产率增大,但升温速率过快,反而使页岩油产率降低;终温在500℃~510℃,持温时间20 min的条件下,产油率最高,继续增加干馏终温和持续时间对产油率影响不大;同时适宜的粒度可以适当提高页岩油的产率。

The mass and energy change speed of the TiB2 coating paste for aluminum electrolysis during its solidification and carbonization process was studied by the DTG and DDTA, and a reasonable heating program of solidification and carbonization was established. On this basis, the effect of heating program on the properties of TiB2 cathode coating was investigated.

摘 要:采用DTG, DDTA等热分析手段,研究了高温固化、炭化过程中,铝电解用TiB2阴极涂层糊料的质量和能量的变化速率,制定了涂层的变速固化、炭化升温制度;在此基础上,研究了升温制度对TiB2阴极涂层性能的影响。

The correlation between the phase behaviors and heating rates for PMMA/α-MSAN blend and PS/PVME blend was investigated by using SALS method within the relatively wide heating rates range.

研究发现,由这两种体系所得到的结果相似,即使在很低的升温速率下,共混体系的相分离温度与升温速率之间的关系均会明显偏离线性。

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Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

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