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XRD, 29Si, 27AI MAS NMR, the adsorption of nitrogen at low temperature,129Xe NMR, XPS, IR-TPD, NH3-TPD, the high vacuum volumetric analysis and pulse flow microreaction were used to study the difference in structure and property between the US-SSY zeolites obtained by quick and slow cooling after treating SSY zeolite with steam at high temperature.

应用X射线粉末衍射、29Si、27Al魔角旋转核磁共振、低温氮吸附、129Xe核磁共振、X射线光电子能谱、程序升温脱附和脉冲微反等多种物理、化学手段,详细考察了经高温水蒸汽处理后的超稳Y分子筛在急冷和自冷过程中产生的结构和性能差异,结果表明,冷却速率是制备分子筛必要的控制因素

Experimental results indicate that a high reaction temperature and quickly ascending temperature speed apparently increase the nucleation number of monoclinic zirconia in the precursor solution.

实验结果表明,高的反应温度和煅烧过程中快的升温速度明显增加了前驱体溶液中单斜氧化锆的形核数。

In the technical scheme of the invention, reactant, ammonia and hydrogen peroxide are ordinally added into the reaction system of catalyst containing Ti-MWW-F molecular sieve and solvent, and after stiring, temperature raising and reaction are finished, an oxime product is produced by filtering, distillation, liquor filtering and separation.

本发明的技术方案是将反应物酮或醛、氨、过氧化氢依次加入到含Ti-MWW-F分子筛的催化剂和溶剂的反应体系中,搅拌,升温,反应结束后,经过滤,蒸馏滤液,分离得到产物肟。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下:一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸;蒸馏NMP;干燥增溶剂;二、在氮气气氛下,Py与NMP混匀后加入密封的反应器中,再加入增溶剂,然后加入5-氨基-2-苯并唑,搅拌;三、在氮气气氛下,将步骤二的混合液搅拌并升温至50℃~150℃后加入脂肪族二酸,再加入TPP后缩聚;四、再倾入甲醇析出沉淀,过滤,清洗沉淀,再干燥;即得到含唑环半芳香聚酰胺。

With industrial monomer solution of dimethyldiallylammonium chloride as raw material, ammonium persulphate as initiator and Na_4EDTA as chelating agent,using the methods of adding initiator all at once,graduated increasing of temperature and stepwise initiation and polymerization,the polymerization process of preparing poly-dimethyldiallylammonium chloride was researched.

以一步法工业单体二甲基二烯丙基氯化铵为原料,以过硫酸铵为引发剂,采用一次性加入引发剂,梯度升温,分步引发水溶液聚合反应的方法,对制备聚二甲基二烯丙基氯化铵的聚合反应的工艺进行了优化研究。

In the fermentation material properties, loose 24-48 hours, days, 15 days of deodorization into fat, not only speed than the planimetric fermentation, and still more effectively prevents the fermentation of hydrogen sulphide, amine such harmful gas and bio-degradability of odorous gases, accord with environmental protection requirement, namely, and can produce good biological fertilizer.

发酵物料在这种松散物料性状下,24-48小时升温、三天除臭、15天左右成肥,不仅比深槽发酵速度快的多,还有效防止了发酵过程中硫化氢、胺气、吲哚等有害、恶臭气体的产生,即符合环保要求,又能生产上好的生物有机肥。

Hydroxypropylmethylcellulose which possesses weak polarity groups, like polyhydroxy groups and ether groups, will transform to hydrogel when temperature increases.

纤维素衍生物羟丙基甲基纤维素分子中含有大量的羟基和醚键,其水溶液在升温情况下可以发生凝胶转变,是一种新型的有机模板,本文对其作用下特别是凝胶状态下的矿化进行了探讨。

In present work, Al〓O〓/Ti Ceramics with several weight percent Ti were made by pre-sintering and pressureless sintering at flow of Ar with Al〓O〓/Ti covered powder.

但是,金属氧化物的使用可能会降低材料的机械性能,以过快的升温速度烧结又有可能导致产品不均匀受热。

A furnace equipped with a removable measuring scale in the side was applied to study on the shrinkage characteristics of semicoke/coke under gradient temperature during coking process.

利用炉侧安装了移动测量标尺的加热炉(φ150 mm×300 mm),分别以三种加热速率(1.0℃/m in、1.5℃/m in和3.0℃/m in)及两种堆密度(880 kg/m3和1 080 kg/m3)模拟工业炼焦,研究了1 500 g的炼焦用煤在焦化过程中径向收缩与焦化时间、中心温度、焦化升温速率及梯度温度的关系。

For the weakness of actual Trombe wall that slows indoor temperature rise in the morning, an improved Trombe wall with honeycomb structure was built based on the comparable hot-box.

针对现行的带 Trombe墙体太阳房早晨室内升温速度较慢的缺点,利用可对比热箱,建造了带有新型竖置透明蜂窝的改进型 Trombe墙体。

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