升温

The temperature-programmed desorption and temperature-programmed surface reaction were studied by in situ mass spectrographic analysis.

应用质谱在线技术，对CuO-ZnO-ZrO2催化甲醇水蒸汽重整反应进行程序升温脱附和程序升温表面反应研究。

Effect of sulfurization time, water content, oil as well as sulfur on spontaneous combustion of iron sulfide is investigated on the same sulfide formed from Fe2O3. It indicates that long sulfurization time, some oil, sulfur as well as good ventilation condition could accelerate oxidation and temperatures rise, but uncertain water content and poor ventilation condition lessen the spontaneous combustion tendency.

以Fe2O3的硫化产物为典型样品，研究了硫化时间、水分、油品、硫及通风条件对硫化铁氧化升温特征的影响，结果表明，硫化时间长，适量的油品和硫以及良好的通风条件能够加速硫化铁升温过程，而一定的水分及不良的通风条件则降低了硫化铁的自燃倾向性。

The invention provides a preparation method of small crystal SAPO-43 molecular sieve, which is characterized in that: the stepwise procedures are adopted to synthetize SAPO-43 molecular sieve, temperature-rising rate in different temperature phase during crystallization is controlled, so that the synthetized SAPO-43 molecular sieve has small particles, even crystal particles, short crystallization time, and reduce the amount of templates greatly, thereby reducing environmental pollution.

本发明的目的是提供一种小晶粒SAPO-43分子筛的制备方法。本发明的特点在于它是采用分阶段程序升温来快速合成小晶粒SAPO-43分子筛。通过对晶化过程中不同温度段内升温速率的控制，从而实现了合成的SAPO-43分子筛晶粒小，晶粒尺寸分布均匀，晶化时间短，且大大的降低了模板剂的用量，从而减少了对环境的污染。

By regression of experimental data, therules of the linkage between these factors, which will provide a theoretical basis for designing BBP with different scales.3 Using thermal analysis technology and dynamic thermogravimetry, the paper studies combustion kinetic characteristics of 3 types of agricultural crops at different rate of temperature rise, and thus, achieved dynamic parameters of these fuels at different rate of temperature, established dynamic model of straw combustion, which reflects the dynamic process in the fast combustion area.4 Characteristics of straw briquette combustion was experimented, focusing on the impact of straw type, temperature, air supply, and density, diameter, and weight of briquette on the combustion speed, and the following conclusions were drawn:(1) combustion of straw briquette fuel is static permeation diffusion combustion;(2) temperature has a larger impact on the speed of straw briquette combustion than air supply; the higher the combustion temperature is, the faster volatilizable component separates out, and the less steady the combustion is;(3) density of briquette fuel has impact on the speed of volatilizable component separation and therefore the combustion speed;(4) increase of diameter and weight of briquette fuel increases the average combustion speed in the initial stage, and that in the later stages is comparatively steady;(5) the proportion of volatilizable component in straw briquette fuel is high, therefore, the temperature control during combustion under the rational ventilation condition is essential to ensure its safe combustion.5 Using the above-mentioned results of experiments and theoretical analysis, and based on thought of hydraulic driven and bi-direction compression, the hydraulic system and compression parts of the HBP BBP are re-designed in terms of industrialization.

利用热分析技术，采用动态热重实验法，对我国的三大农作物秸秆在不同升温速率下的燃烧动力学特性进行了较系统的研究。得到了各原料在不同升温速率下的动力学参数；建立了秸秆燃烧的动力学模型，该模型反映了秸秆迅速燃烧区的动力学过程。 4 对秸秆成型燃料的燃烧特性进行了试验研究。着重研究了秸秆河南农业大学博士学位论文巫的种类、温度、空气供给量、成型燃料密度、直径、质量对成型燃料燃烧速度的影响并得出如下主要结论：①秸秆成型燃料的燃烧方式属于静态渗透式扩散燃烧。②秸秆成型燃料燃烧速度受温度的影响大于通风量燃烧速度的影响：燃烧温度越高，挥发分析出速度越快，燃烧平稳性愈差。③成型燃料密度影响成型燃料挥发分的析出速度，影响燃烧速度。④成型燃料直径和质量的增加，使得燃烧初期的平均燃烧速度增大，中后期的平均燃烧速度相对平稳。⑤秸秆成型燃料含挥发分比例高，因此合理配风下的控温燃烧是保证其完全燃烧的关键。 5运用已取得的试验和理论分析结果，以液压驱动、双向成型为基础，从产业化的角度对HBP型成型机进行了液压系统和成型部件的改进设计；同时采用了二级预压机构，使该成型机的生产率达到 500kg.hd；单位能耗 60kwh。上'左右，磨损件修复周期 300小时左右，基本解决了影响生物质固化技术在国内推广的技术难题。

Progress in researches on catalysts for fluidized bed oxychlorination of ethylene to make dichloroethane;2. The catalytic performance of CuCl2-KCl/MgO-Al2O3 catalysts was evaluated for the oxychlorination of ethane to produce vinyl chlorid.

采用浸渍法制备了不同含量MgO改性的γ-Al2O3，采用X射线衍射、N2物理吸附、NH3的程序升温脱附和程序升温还原等手段表征了催化剂的结构、表面酸性和氧化还原性质，并对CuCl2-KCl/MgO-Al2O3催化剂催化乙烷氧氯化制氯乙烯反应进行了活性评价。

C NMR, IR, GC MS and TG combined with some techniques including solvent extraction method, TPO and structure characterization were applied to determine the components of the deposit on the coked β zeolite catalyst after reaction for 8?000 h in pilot plant scale. It was shown that the composition of the deposit ...

用13CNMR ，IR ，GC MS ，TG等手段，并结合溶剂萃取法、TPO和结构分析等方法，确定了改性β沸石催化剂上沉积物的主要成分是多异丙基苯和四氢化萘，且主要分布在沸石孔道内；同时，快速升温后恒温烧炭的效果优于慢速升温后恒温烧炭的效果

Based on the method of stepwise increasing temperature in the process of polymerizing PDMDAAC initiated by APS which has been successfully studied in our research group, the optimal method of increasing temperature in the polymerization initiated by the AIBA.2HC1 was found.

以本课题组在采用APS引发DMDAAC水溶液聚合时的所用的梯度升温方式为基础，通过实验得到了适合于AIBA·2HCl引发DMDAAC水溶液聚合时的梯度升温方式中各阶段的最佳温度。

The oil yield of six types of Huadian oil shales were measured on a Fischer assay retort,and the factors which effected the results of Fischer assay of oil shale were investigated,such as heating rate,particle size,final retorting temperature and retorting persistent time.

结果表明，页岩油的产率随着挥发分含量的增大而增加，在一定范围内提高升温速率，页岩油产率增大，但升温速率过快，反而使页岩油产率降低；终温在500℃~510℃，持温时间20 min的条件下，产油率最高，继续增加干馏终温和持续时间对产油率影响不大；同时适宜的粒度可以适当提高页岩油的产率。

The mass and energy change speed of the TiB2 coating paste for aluminum electrolysis during its solidification and carbonization process was studied by the DTG and DDTA, and a reasonable heating program of solidification and carbonization was established. On this basis, the effect of heating program on the properties of TiB2 cathode coating was investigated.

摘 要：采用DTG， DDTA等热分析手段，研究了高温固化、炭化过程中，铝电解用TiB2阴极涂层糊料的质量和能量的变化速率，制定了涂层的变速固化、炭化升温制度；在此基础上，研究了升温制度对TiB2阴极涂层性能的影响。

The curve of expansion versus temper- rature in the temperature elevating process is depicted automatically and the coefficients of mean lin- ear expansion, instantaneous thermo-expansion, transforming temperature and softing point can be printed according to the.

本文介绍了一种■全由计算机进行设定控制的热膨胀仪，可以对温度范围、升温速率、初始条件进行设定，并由计算机完成实时数据的采集及处理，完成升温过程中温度-伸长量曲线自动描绘，并根据用户要求自动打印出各温度段的平均线膨胀系数、瞬间热膨胀转变温度及软化点等，其结构准确可靠、使用方便、自动化程度高，达到国内领先水平。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。