十四烷

The reaction of condensation-cyclization of the two prepared compounds at 100 ℃ in the presence of anhydrous potassium carbonate gave 1,4,7,10-tetrakis(p-toluenesulfonyl)-1,4,7,10-tetraazacyclododecane,with a yield of 71%.

在无水碳酸钾存在下，100℃加热使所得两种磺酰化产物缩合环化得到1，4，7，10-四-1，4，7，10-四氮杂环十二烷，产率71.0%。

Anti-knock additive tetraethyl lead,vapor pressure,cetane number and content of aromatic hydrocarbon,ethylenes,sulfur and oxides respectively in the motor fuel are more detailedly analysed in regard to their effect on motor vehicle exhaust emission.

较为详细地分析了燃油中四乙铅抗爆剂、芳烃含量、烯烃含量、硫含量、蒸气压、十六烷值及含氧化合物等对汽车排放的影响，并简述了其发展趋势。

In the fifth chapter, six compounds formed between nitrogen-containing ligands such as 2, 2'-bipyridyl, isonicotinamide and 1, 4, 8, 11-tetraazacyclotetradecane and the solution cadmium sulfonates such as 1, 5-naphthalenedisulfonate, 2, 6-naphthalenedisulfonate, 4, 4'-bipenyldisulfonate and 4, 4'-penyletherdisulfonate have been synthesized and structurally characterized. Besides, another compound has been synthesized with cadmium carbonate reacting with 1, 5-naphthalenedisulfonate acid.

第五章以2，2'-联吡啶、异烟酰胺和1，4，8，11-四氮杂环十四癸烷与含有Cd〓和1，5-萘二磺酸根离子、2，6-萘二磺酸根离子、4，4'-联苯二磺酸根离子和4，4'-苯醚二磺酸根离子的水溶液反应，合成了六个化合物，另外以1，5-萘二磺酸与碳酸镉反应合成出一个化合物。

Objective To evaluate the diagnosis value of positive 99Tcm-4,9-diaza-3,3,10,10-tetramethyldodecan-2,11-dione dioxime (HL91) imaging using receiver operating characteristic curve for distinguishing the character of pulmonary neoplasms.

目的 探讨半定量分析及接受器工作特性曲线法在99Tcm 4 ，9 二氮3，3，10 ，10 四甲基十二烷2 ，11 二酮肟(HL91)肿瘤阳性显像鉴别肺部良恶性肿块中的价值。

The value of 4,9-diaza-2, 3, 10, 10-tetramethydodecan-2, 11-dione dioxime (HL91) tagged with 99Tcm on detecting the hypoxic brain tissue surrounding the hypertensive cerebral hemorrhage nidus, which represents the penumbra is still waited for confirmation.

采用99Tcm标记的缺氧显像剂4，9-二氮-2，3，10，10-四甲基十二烷-2，11-二酮肟(HL91)检测血肿周围可逆性损伤组织来反映半暗带是否可行，有待证实。

Bis-imidazoline was prepared from triethylene tetraamine and N,N-dimethylformamide dimethyl acetal at 85℃ for 2 h with toluene as solvent, with a yield of 90.4%. The reaction of bis-imidazoline with 1,2-dibromoethane and potassium carbonate in acetonitrile provided with a monobromide salt yield of 78.7%. Hydrolysis of monobromide salt under aqueous causic solution formed 1,4,7,10-tetraazzcyclododecane in a 74.2% yield.

用甲苯作溶剂，使三乙烯四胺和N，N-二甲基甲酰胺二甲基缩醛在85℃反应2 h，得到中间体双咪唑啉，产率90.4%，在乙腈溶剂中，碳酸钾存在下，双咪唑啉和1，2-二溴乙烷进行扩环反应，得到环状中间体一溴盐，产率78.7%，一溴盐经碱性水解2 h，得到1，4，7，10-四氮杂十二烷，产率74.2%。

The macrocyclic polyamines are a kind of excellent ligands and have a substantially high binding affinity with transition metal ions. Macrocyclic polyamine metal complexes as enzyme models are widely used in chemical biology, medicine and gene therapy. 1, 4, 7, 10-tetrazacyclododecane is a representative macrocyclic polyamines compound and shows high binding affinity with transition metal ions, such as Zn, Cu and Co. Their metal complexes especially multinuclear complexes were widely used in DNA, RNA recognition.

大环多胺化合物是一类性质独特的优秀配体，具有良好的金属配位能力，其金属配合物作为人工酶模型广泛应用于核酸结构及功能研究、基因表达与调控、抗癌药物的研制等生物、化学和医学领域。1，4，7，10-四氮杂十二烷是典型的大环多胺化合物，对过渡金属离子Zn， Cu and Co有良好的配位能力，这些金属配合物特别是多核金属配合物被广泛应用于DNA识别中。

The measurement of apparent volume change is described during cure reaction of a new spiro ortho -carbonate, 3, 9, di (p-methooxybenzyl)- 1, 5, 7, 11-tetraoxspiro (5,5) undecaneand epoxy resin, and the volume expansion ratio of this new monomer is culcu-lated,and its applications are approached.

叙述了新的螺环化合物3，9-二-1，5，7，11-四氧杂螺环[5，5]十一烷与环氧树脂进行固化反应时，其表现体积变化率的侧定方法，推算了这种新单体的体积膨胀率。

A series of tri-block copolymers of styrene/tetradecyl methyl acrylate/3-methacryloxyl-propyl thimethoxyl silane was synthesized by atom transfer radical polymerization. The structures of those copolymers were characterized by means of gel permeation chromatography, infrared spectrum, and nuclear magnetic resonance (1H-NMR). Effect of tri-block copolymers on the mechanical properties of glass fiber/polypropylene composites was also investigated.

采用原子转移自由基聚合法合成了一系列新的三嵌段共聚物大分子偶联剂聚苯乙烯－b-聚甲基丙烯酸十四酯－b-聚3-甲基丙烯酰氧基丙基三甲氧基硅烷，通过凝胶渗透色谱、红外光谱和核磁共振(1H-NMR)证实了其结构，并研究了其对玻璃纤维／聚丙烯复合材料力学性能的影响。

The compound 3, 9-bis (2＇, 4＇, 6＇-tribromophoxy)-2, 4, 8, 10-traoxa -3, 9-dip- hosphospiro [5.5] undecane -3, 9-dioxide (HFR-1) was prepared with pentaeryth- ritol, phosphorus oxychloride and 2, 4, 6-tribromophenoxy soldium by esterifica- tion and condensation reaction.

以三溴苯酚钠、三氯氧磷、季戊四醇为原料，通过酯化和缩合两步反应合成了阻燃剂3，9-双(2'，4'，6'三溴苯氧基)-2，4，8，10-四氧代-3，9-二磷螺环-3，9-二氧[5.5]十一烷。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了