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十二醇

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In this paper, the catalytical esterification of palmitic acid with 1 hexadecanol by lipase immobilized by microemulsion base organo gel that consisted of bis (2 ethylhexyl)sodium sulphsuccinate/heptane/water/gelatin in apolar organic solvent was studied.

研究了以AOT二(2 乙基已基琥珀酸酯磺酸钠/正庚烷/水/明胶组成的反相微乳凝胶固定化脂肪酶,在有机溶剂中催化棕榈酸和十六醇的酯化反应。

The invention discloses an InP quantum point preparing method, comprising the steps of:(1) mixing InCl3 with trioctylphosphine oxide, and preserving heat at 90-110DEG C to prepare a solution whose In content is 0.1-0.3mol/L;(2) raising temperature to 130-180DEG C, and charging argon gas;(3) injecting PSi(CH333 into InCl3-TOPO compound in the molar ratio of 1 to 1-1 to 2;(4) when the solution color turns into transparent red or orange, raising temperature to 260-270DEG C and preserving heat;(5) lowering temperature to 90-110DEG C and injecting dodecyl amine, decyl amine or mercaptan;(6) dissolving reacting mixture in nonpolar solvent to form transparent colloidal solution, then adding in polar solution until the colloidal solution is muddy, and centrifugally separating and obtaining deposits and supernatant; and (7) centrifugally separating the supernatant, where the above steps (1)-(5) are performed.

本发明公开了一种InP量子点的制备方法,其步骤为:①将InCl 3 与三辛基氧膦混合,在90~110℃保温制得In含量为0.1~0.3mol/L的溶液;②升温到130~180℃,通入氩气;③将PSi(CH 3 3 3 注射入InCl 3 -TOPO复合物中,其摩尔比为1∶1~1∶2;④待溶液颜色变为透明的红色或橙红色,将升温260~270℃保温;⑤降温到90~110℃,注入十二胺、癸胺或硫醇;⑥将反应混合物溶于非极性溶剂,形成透明的胶体溶液,然后加入极性溶剂,直至胶体溶液出现混浊状,然后离心分离获得沉积物和上层清液;⑦取上层清液进行离心分离。上述步骤①~⑤在保护气氛下进行。

The δ-γ fishlike phase diagram is applied to the research of the phase behavior of sodium dodecyl sulfonate / alcohol/ alkane/ NaCl aqueous solution of qualernary system.

用δ-γ型"鱼状"相图研究了微乳液体系十二烷基磺酸钠/醇/烷烃/NaCl水溶液的相行为。

The formulas for these phenolic compounds are Epigallocatechin gallate is the main flavanol in dried green tea.

这些酚类化合物的分子式为:表儿茶素酸酯是干绿茶中的主要黄烷醇。语文课本三十二册。

According to experiment, polyvinyl alcohol , 12 alkyl benzene sulphur sour sodium,, single glyceride these good flaky aluminium single auxiliary of powder very too.

根据实验,聚乙烯醇、十二烷基苯磺酸钠、单甘油酯这几种也是很好的片状铝粉的单一助剂。

The experiment results showed that the optimum reaction condition were as follow: concentration of H_(2)SO_(4) was 0.5 mol/L, calcinations time were 4 h at the temperature 550℃, the molar ratio of acrylic acid to octadecyl alcohol was ...

丙烯酸十八酯的优化工艺条件为:丙烯酸与十八醇的摩尔比为1.2,固体超强酸及对苯二酚的用量分别为6%、0.8%,反应温度为120℃,反应时间为3 h。在此反应条件下,酯化收率可达97%。

The testing methods and targets were shown as below:Recorded milk weights from the 7th day postpartum to 15th day postpartum,and calculate the average day-milk yield;Milk samples were draw in 7th day and 14th day postpartum,and testing the milk fat,milk lactose,milk protein,milk Zn and the milk somatic cell counts;Blood samples were adopted at the 7th day postpartum,testing the levels of serum PRL; Blood samples adopted at the 1st day and the 12th day in oestrous cycle were used to test the levels of E_2 and P_4 in serum;In the experimental stage, registering the condition of parturition, the mean birth weight of calves,the first oestrus,the oestrus scycle postpartum and the conception rate of the first service after artificial insemination.

试验方法及所测指标如下:于产后第七天到第十四天记录日产奶量,最后计算每组平均日产奶量;每组随机抽取分娩后第七天、第十四天的奶样,测定乳糖、乳蛋白、乳脂、乳锌含量及乳体细胞数;于产后第七天,随机采取奶牛血样,测定血清中PRL含量;于发情周期的当天和第12天,随机采取血样,测定血清中雌二醇(Estradiol,E2)和孕酮(Progesterone,P)的浓度;记录奶牛的分娩情况、犊牛初生重、产后第一次发情日期、产后发情周期,并采用人工授精技术进行受精,记录第一情期受胎率,最后取平均值,作为衡量奶牛繁殖性能的指标。

The conversion of product reaches 98% under the optimal experiment condition: the molar rate of acrylic acid and tetradecyl alcohol is 1.1; the amount of p-methyl benzene sulfuric acid is 0.8%; the amount of p-benzened...

得出合成丙烯酸十四酯的最佳合成条件:丙烯酸与十四醇摩尔比为1 1,对甲苯磺酸用量为0 8%,对苯二酚用量为0 6%,反应温度为120℃,反应时间为4h。

Methods: After the sample being digested, because of ethylenediamine-hydrochloric acid, aluminium, chrome azurol S, the polyethylene glycol octyl phenyl ether together with hexadecylpyridine bromide form a steady blue quaternion system, whose absorbance and aluminium content is direct ratio within some consistence range.

样品经消化后,在乙二胺-盐酸缓冲介质存在下,铝与铬天青S和聚乙二醇辛基苯醚及溴代十六烷基吡啶形成稳定蓝色四元体系,在一定浓度范围内,其吸光度与铝含量成正比。

A novel method to prepare Au nanorings by self-reduction of HAuCl4 in the soft template composed of sodium dodecyl sulfate-PEG 20000 cluster at ambient temperature and atmosphere was reported, in which no hard template and extra reducer was needed. TEM image displays that the diameter of Au nanorings is (500±50)nm.

介绍一种由十二烷基硫酸钠与聚乙二醇(PEG 20000)组成的团簇为软模板,在室温、常压、无硬模板及无外加还原剂条件下自还原HAuCl4合成金纳米环的新方法。

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The objective is to subjugate and discourage the people, because that allows the elite to continue to rule unopposed.

其目的是压制和打击人民的积极性,因为这可以让实权派继续统治不会沦为反对派。

GOD,this is the second time you vanquished me!

天啊,这是第二次你打败了我!

So a kind of strong antagonism permeated in the relations of two countries.

所以两国这一时期的政治关系始终弥漫着一种强烈的对抗情绪。