化学

Name of appearance of the chemical composition that determined all sorts of synthesis outcome according to chemical analysis and XRD analysis data, substance, lens of report of use emissive scanning is calcic to 6 kinds of boric acid microscopical form appearance, grain size undertook token, those who discover them is microscopical form appearance, grain size has very big different.

根据化学分析和XRD分析数据确定了各种合成产物的化学组成、物相名称，用场发射扫描电镜对六种硼酸钙的显微形貌、颗粒大小进行了表征，发现它们的显微形貌、颗粒大小有很大的不同。

In this thesis, by the means of calefactive oxidation test of coal samples, the characteristics of different samples spontaneous combustion are analyzed; the infrared spectrum is assimilated to review the rule that coal function corps change in the process of coal low-temperature oxidation ; by the means of thermal analysis by differential scanning calorimeter, thermogravimeter, the kinetic function of coal low-temperature oxidation in spontaneous combustion process are analyzed , depend on the device, the mathematical model of coal spontaneous combustion is developed, the model are dealt with, Finally, the temperature field and the velocity field with velocity of the entry flow is got.

论文通过煤的低温氧化和自燃过程，实验研究了煤的低温氧化气体产物特征和变化规律，研究得出了煤的低温氧化过程中气体生成量与氧气消耗量与煤温之间的指数关系式；在煤的低温自热氧化过程中，对煤的官能团等化学结构的变化研究，揭示了煤炭低温自热氧化化学基团变化规律；采用非等温TG和DSC法研究了烟煤低温氧化动力学，得出了煤低温氧化分布活化能及煤低温氧化机理函数的变化规律；建立了煤低温氧化自热数学模型，并对该模型进行数值解算，可得煤样的温度场与速度场随入口风量变化情况。

Electrochemical oscillation of lead electrode in sulfuric acid has been explored with in-situ ellipsometry.Effects of improvement of electrodes properties are affected by increase or decrease of surface temperature of the samples badly during ion implantation. Some theories and methods on substance diffusion transfer have been applied to calorifics to obtain mathematical relation between the surface temperature on the samples and operation time during ion implantation.

掠射式椭圆偏振方法是本论文提出的一种全新的研究方法，为验证这种现场研究方法的可行性，本论文选择了几个用其它方法研究较为成熟的电化学体系并结合本论文研究的化学电源体系，以掠射式椭圆偏振技术进行研究，提出了改良镍电极、锌电极、铝电极和铜电极性能的具体措施或者理解这些电极表面性质和涉及它们的电极过程的实验依据，为使用这些电极的化学电源性能的提高奠定了基础。

ObjectiveTo review the progress in the study of chemical constituents and pharmacological effects of Canarium album for its reasonable utilization and further development.

作者：项昭保，陈海生，何从林橄榄；，，化学成分；，，药理作用摘要：目的综述橄榄的化学成分、药理作用，为橄榄资源的合理利用和深度开发提供可靠的依据。

Reaction trends of catalytic desulfurization of thiophene were determined based on the reaction energy needed, which was obtained with the AM1 calculation results of thiophene and possible carbonium ions on transition state.

采用半经验AM1计算方法，利用静态理论对噻吩在分子筛催化剂上的催化裂化脱硫机理进行了量子化学计算研究，通过对噻吩分子和可能产生的中间正碳离子的量子化学计算，得到各中间反应所需的能量，从而判断噻吩催化裂化脱硫反应的趋势，证实了氢转移反应在催化裂化脱硫中所起的作用。

The distribution of nutrient was also different for different plant components in Carex lasiocarpa .

研究生物与环境中化学因子之间的相互作用过程，主要是指化学物质在生态系统中的运移、转化及归趋与效应。

With the rapid growth in supramolecular chemistry in recent years, a great deal of effort has been devoted to the design and assembly of supramolecular compounds, for these compounds have potential applications in catalyses , molecular recognition, molecular electronics, photonic materials and so on.

近年来，超分子配合物因在催化化学、主客体-超分子化学和分子磁性材料、超导材料、非线形光学材料等方面的潜在应用价值而成为最活跃的研究领域之一。

The effective stimulating sites were indentified by defensive cardiovascular response and other components of defence reaction evoked by 3 s trains of rectangular cathodal pulses (100Hz, 0.5ms pulse duration, 70 -150μA intensity for dPAG and 150-250μA for PF) delivered from a programmed multichannel constant current stimulator. The responses included an increase in blood pressure and heart rate, pupillodilation and an increase in the rate and depth of respiration. Currents of 1Hz, intensity of 100- 150μA for dPAG and 200-250μA for PF were used to observe the effect of the stimulation of them on RVLM neurones. The deep peroneal nerve and superfacial deep peroneal nerve were carefully separated, and put on a pair of stimulating electrode respectively, Both nerves were stimulated with constant rectangular pulses of 1Hz, 0.5ms duration and 300μA current intensity to see their effects on RVLM neurones. The baro-and chemo-receptors were activated by the intravenous injection of phenylephrine or 0.208 M NaH2PO4. The degree of convergent inputs to individual RVLM neurone was studied by the stimulation of the sites mentioned above. It was found that neurones about 61.4%(27/44) and 35.3%(6/17) received convergent inputs from three and four places respectively.

过去的研究主要集中于整体水平，利用电刺激或化学刺激RVLM神经元，观察对血压、心率及交感活动的影响，并对影响心血管交感活动的神经递质进行了广泛探讨，积累了大量资料；在神经元水平，主要研究刺激脑内核团、外周神经、化学感受器及压力感受器等对RVLM神经元放电的影响和某些神经递质影响神经元活动的机制、然而，对RVLM神经元如何整合不同信息、其可能突触机制等研究得较少，本互作拟采用在体细胞内、细胞外记录电活动与微电泳，结合中枢核团及外周神经电刺激等方法，对RVLM神经元在不同状态下的整合作用规律与可能机制进行初步探讨，为进一步了解这一复杂的整合过程提供新的理论依据。

Animals after chemolysis failure to homogenate respectively,centrifugate and take the pure liquid,mcasure collagenase activity with Blanckaert method,the data handled with statistics did not show obvious difference.

组织化学检测：将实验动物组、对照组、手术组和化学溶解术失败再手术组标本的纤维环内层、中层和外层分别匀浆、离心，取上清液，按Blanckaert法测定胶原酶，所得据经统计学处理差异无显著性。

Methods: A 5ml bone marrow was extracted from the lilac of human volunteers. By Percoll fluid and density gradient centrifugation, the MSC was obtained; after the cells filled the bottom of vessel, subcultured them, when they subculture in third generation, redigested them, 500 R/min centrifugate, alter the completed medium to chemical definition medium, examined the form change and prolifration of cells by invert microscope, toluidine blue stain、immunocytochemical stain and RT-PCR to test the type Ⅱ collagen mRNA and proteoglycan.

取健康成人髂后上棘处骨髓5ml，经percoll液分离后密度梯度离心，〓／ml密度接种培养，观察原代细胞的贴壁、增殖状况，细胞长满瓶底后进行传代培养；传至第三代细胞，重新消化后以500转／分钟轻度离心5分钟，〓／ml接种，改用化学限定培养基代替完全培养基培养，倒置显微镜观察细胞生长情况及形态变化，甲苯胺蓝染色观察诱导细胞合成细胞外基质中的蛋白多糖，免疫细胞化学染色检测ECM中Ⅱ胶原的蛋白合成，RT-PCR鉴定诱导细胞Ⅱ胶原mRNA的表达。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。