化合物

In search of environmentally benign insecticides with high activity, low toxicity and low residue, a novel series of anthranilic acid esters containing N-pyridylpyrazole were designed and synthesized. All of the compounds were characterized and confirmed by IR, 1H NMR, MS and elemental analysis.

设计，合成了8个新的含N-吡啶基吡唑杂环的邻氨基苯甲酸酯类化合物，结构经FTIR， MS， 1H NMR 和元素分析确证，并且采用X-射线衍射分析方法确证了具有较好生物活性的化合物14d的结构。

The results show that total sixteen organic compounds were identified in the BSF, in which anthracene relative content is as high as 85% and following abundant components are palmitic acid, anthrone and anthraquinone with contents around 3%, whereas contents of others are less than 1%.

结果表明，在该苯可溶物中共鉴定出16种有机化合物，其中蒽的含量高达85％，其次是棕榈酸、蒽酮和蒽醌，含量各为3％左右，其他化合物的含量都小于1

We have presented some important evidences to the antiknocking mechanisms of aromatic amine through investigating the reactions of aromatic amine and peroxide on the premise of analyzing the electrochemical properties of aromatic amine. As a result, the relationship of antidetonating quality and electrochemical properties has been discussed.

本文在分析苯胺类化合物电化学性质的基础上，通过研究苯胺类化合物与过氧化氢的作用，为芳香胺抗爆机理的研究提供了重要依据，并由此探讨抗爆剂的抗爆性与电化学性质的关系。

A series of antimony mercaptide compounds which formula are Sb 〓 and Sb S (CH〓〓COOR 〓(R represents an alkyl or aryl, aralkyl, n=0～2) have been synthesized. A new synthetic method has been invented to solve the defect of abroad patent method which has complex technological conditions and singleness intermediate compounds. A new catalyst QL-1 and preactivated antimony trioxide and other means have been used to avoid neutralizing, washing, separating and other procedures of intermediate and simplifing process flow at the same time. According to this new technique, a series of antimony mercaptides and their intermediate products have been synthesized with high yield.

合成了结构为SbS(CH〓〓COOR〓及Sb〓（R为烃基或芳烷基，n=0～2）的一系列硫醇锑化合物，针对国外专利报道的合成工艺存在着工艺条件苛刻，同时需多步完成，操作复杂，而且中间体品种单一的缺陷，发明了一种一步法合成硫醇锑化合物的新工艺，采用QL-1催化剂，且将三氧化二锑预先活化，变固—液相反应为液—液相反应，同时可免除中间体的中和、洗涤、分离等工序，工艺流程简化，产品收率高，且能制得系列硫醇锑产品。

Compounds 1 and 2 were isolated from Asterina pectinifera for the first time, while compound 4 was first obtained from Asterina pectinifera of China Sea.

化合物1、2为首次从海燕中分离得到，化合物4为首次从中国海域的海燕中分离得到。

We hope that the formation of biazulene compound(201), under the coupling reaction of 1、3-position being along with electron-withdrawing group, 2-position being along with hydroxy group, and four 4、8-position being along with static energy obstacle large enough functional group of azulene compound(200), may have the chiral auxiliary effect like that of the BINOL.

希望将两个在1、3-位置上有拉电子基、2-位置上有羟基及在4、8-位置上有立体能障够大的官能基之薁类化合物(200)，进行偶合反应后所形成的双薁类化合物(201)能够像BINOL那样具有掌性辅助剂之效果。

The bay area has no substituent and has electron-withdrawing groups,such as bromine atom,cyano-group and 4-formyl phenoxy group compounds have strong absorption in 525 nm,when excitated them,they have strong yellow and salmon pink luminescence bettwen 538 and 566 nm.When introduce electron-donating substituents,such as phenoxy group,morpholinyl,piperidinyl and n-butylamino group,the absorption bathochromic shift while the electron-donating ability is improved,bettwen 536 and 692 nm have strong absorption,reach to the near-infrared region. When excitated them,only the phenoxy group compound has strong salmon pink luminescence in 572 nm,the others have no fluorescence.

其中，港湾位无取代的以及含吸电基团(—Br、—CN、对甲酰基苯氧基)化合物在525 nm左右处均有很强的吸收ε＞10~4M~(-1cm~(-1)，当光激发时，港湾位无取代、溴代和氰基取代物发出538～547 nm的强烈黄色荧光，对甲酰基苯氧基取代物则发出566 nm的强烈橙红色荧光；含供电基团(苯氧基、吗啉基、哌啶基、正丁氨基)化合物随着供电子能力的增强，吸收发生红移，在536～692 nm处均有很强的吸收ε＞10~4M~(-1cm~(-1)，达到了近红外区，当光激发时，只有苯氧基取代物发出572 nm的强烈橙红色荧光，而含氮供电基取代物均发生了荧光淬灭。

The forth part is a review about the progress of studies on the chemical constituents from Belamcanda chinensis and Iris species. Fifty-three compounds were isolated from Rhizoma Belamcandae, the rhizomes of B.

采用正、反相硅胶柱层析、凝胶柱层析、薄层制备及HPLC等各种分离方法，从三种药用植物中共分离出68个不同的化合物，其中61个的结构得得以鉴定，另外4个化合物的结构正在鉴定中，3个由于量少且有点杂质未作进一步的鉴定。

In search of safer and more effective fungicidal compounds,eight N-(4,6-disubstitued pyrimidin-2-yl)- benzamide s were designed and synthesized.

为了寻找高效、安全的杀菌活性化合物，设计并合成了8个N-(4，6-二取代嘧啶-2-基)苯甲酰胺类化合物，其化学结构经1HNMR、IR、LC/MS和元素分析确证。

Benzenoid system and coronoid system s are the natural representations of the skeletons of molecules of benzenoid hydrocarbons and coronoid hydrocarbons in the field of organic chemistry.

六角系统和冠状系统分别是有机化学领域中的苯碳氢化合物和冠状碳氢化合物的分子结构的自然体现。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。