化合物

This paper reviews the preparation and characterization of polymers containing cholic acid obtained by free radical polymerization, polymers modified with cholic acid and polycondensation of cholic acid, etc. The development of polymers containing cholic acid in the future is also forecasted. Contents

本文从自由基聚合形成的含胆酸高分子化合物、胆酸修饰的高分子化合物和胆酸聚合物等几个方面综述了含胆酸高分子化合物的制备和特性，并对胆酸在高分子材料方面的新用途作了展望。

The results showed that the addition of alcoholate increased the elution recovery of phenolic acids on resins in supercritical CO2. The infrared spectroscopy was used to study the interaction between solute and solvent molecules in supercritical fluid. The hydrogen bond between alcoholate entrainer and phenolic acid was the main factor to increase the ability of supercritical elution. The results appeared that salvianolic acids could be extracted by supercritical carbon dioxide with ethanol as entrainer.

结果表明：醇类夹带剂的加入能大大提高树脂上酚酸类化合物的超临界洗脱率；通过红外光谱技术研究了超临界流体中分子间的相互作用与超临界洗脱过程的关系，认为醇类夹带剂与酚酸类化合物的氢键作用是提高酚酸类化合物洗脱率的主要因素；以乙醇为夹带剂的超临界CO2洗脱可应用于丹参酚酸的提取。

The catalyst includes: supported Ziegler-Natta catalyst of titanium halide compound and organic electron donor compound supported with MgCl2 alcoholate carrier; aluminoxane prepared with trialkyl aluminum and water; and one kind of organic electron donor, such as organosilicon compound R2Si(OCH3)2, where R is phenyl, isopropyl, isobutyl or cyclopentyl.

该催化剂包括，a一种负载型的Ziegler-Natta催化剂，即将卤钛化合物和有机给电子体化合物负载在氯化镁醇合物载体上得到的固体催化剂，b一种通过三烷基铝与水反应而制备得到的铝氧烷和c一种有机电子给体，如有机硅化合物R 2 Si(OCH 3 ) 2 ，其中R为苯基、异丙基、异丁基或环戊基。

Over the past four decades, many dearomatization reactions have developed and applied for synthesis of alicyclic compounds con-taining six–membered carboncyclic moieties.

芳香族化合物稳定、易得，通过芳香族化合物的脱芳构化反应，制备官能化的脂肪六元碳环化合物，早以引起人们的广泛兴趣。

The invention relates to a method for making oligomeric isocyanates by reacting diisocyanates in the presence of a catalyst, wherein the catalyst comprises a saline compound prepared from an anion selected from 1,2,3- or 1,2,4-triazole, a substituted species of 1,2,3- or 1,2,4-triazole and carbocyclically and/or heterocyclically annellated species of 1,2,3- or 1,2,4-triazole and the cation selected from an alkali metal, alkaline-earth metal and/or monovalent ammonium cation and/or phosphonium cation of formula (5), wherein the E, R1, R2, R3, R4 are as defined in the descriotion.

本发明涉及一种制备低聚异氰酸酯的方法，包括二异氰酸酯在催化剂的存在下进行反应，其中所述催化剂由盐化合物组成，该盐化合物由选自1，2，3-或1，2，4-三唑、1，2，3-或1，2，4-三唑的取代系列者、1，2，4-三唑的碳环稠合系列者、1，2，3-或1，2，4-三唑的杂环稠合系列者的化合物及其混合物的阴离子和选自碱金属、碱土金属和/或通式(5)的一价铵阳离子和/或磷友衾胱拥难衾胱又票福其中E、R 1 、R 2 、R 3 和R 4 如说明书中所定义。

Means to solve the problem of insufficient contact between paper and plate surface upon printing and to improve printability have been reported in Japanese Patent Application Laid-open No. 2000-345493 in which a matte paper is produced by forming a coating layer with a pigment having a volumetric particle size distribution of more than 65% within the range of 0.4 to 4.2 μm on a base paper containing 10 parts or more by weight of mechanical pulp as a pulp for paper making and 3 to 12% by weight of paper of amorphous silica as a filler and then treating using a soft nip calender at 150° C. or higher; and in Japanese Patent No. 3093200 in which a bulky coated paper is produced by admixing a polyhydric alcohol and fatty acid ester compound or a polyhydric alcohol ester compound, said ester compound having alkylene groups having 2 to 4 carbons in less than 12 moles per mole of said ester compound to base paper for coating.

手段来解决不足的问题之间的联系的文件和钢板表面后，印刷及改善印刷适性已报道，在日本专利申请的下岗公开号2000-345493 ，当中一名磨砂纸所产生的形成层与色素有容积颗粒尺寸分布的65 ％以上的内部范围0.4至4.2 μ m的对基地文件，其中载有十个部分或以上按重量计算机械浆为纸浆造纸和第3至12 ％，按重量计算的文件白炭黑作为填料和治疗，然后用软债券发行计划的日历在150 ℃或更高；和在日本专利号3093200 ，当中一名笨重的涂布纸是由掺1多元醇与脂肪酸酯化合物或1多元醇酯复合说，酯化合物具有alkylene组有2至4活性炭在不少于12痣每摩尔说，酯化合物以原纸为涂层。

The results showed that 42 compounds were identified from perianth at 5 stages, including 18 terpenoid compounds, 7 ester compounds, 4 alcohol compounds, 1 ketone compound, 11 alkanes compounds and 1 unknown compound.

结果表明，5个时期的含笑花被片共鉴定出42种化学成分：萜类化合物18种、酯类化合物7种、醇类化合物4种、酮类化合物1种、烷烃类物质11种和未知物1种。

A series of new isoxazolines were prepared by 1,3-dipolar cycloaddition between different mono-substituted styrenes and new 1,3-dipolar compounds which were synthesized by the reaction of N-methylhydroxylamine sulfate with aromatic carbonyl compounds.

以N-甲羟胺硫酸盐和芳香族羰基化合物为主要原料合成了一系列不同的1，3-偶极化合物，并合成了四种不同的单取代苯乙烯。以该系列1，3-偶极化合物和单取代苯乙烯为主要中间体，采用1，3-偶极环加成反应合成了一系列异恶唑啉类新化合物。

In order to reveal the nature of reducibility of organic compounds and find theoretical basis for the selection of organic reductants, the electronic structure of studied organic reductants and related organic compounds has been calculated by means of HMO method、CNDO/2 method in quantum chemistry. It was discovered that the energy of the highest occupied molecular orbital of organic compounds has best correlation with their reducibility, and theoretical criterion for reducibility of organic compounds was presented.

为了揭示有机化合物还原性的本质，为有机还原剂的寻找提供理论依据，应用量子化学HMO法、CNDO/2法计算分析了研究的有机还原剂及相关有机化合物的电子结构特性，发现有机化合物的最高占据分子轨道HOMO能量与其还原性之间具有最好的相关性，据此提出了有机化合物还原性的理论判据。

The preliminary bioassay indicated that the pyridine compounds display inhibitory activities against mosquites; pyrazolopyridine compounds possessed some plant growth regulation activity; pyrazole compounds displayed some inhibitory activities against wheat rust and tobacco mosaic virus respectively.

初步的生物活性测定结果表明，吡啶类化合物对蚊子有较好的杀虫作用；吡唑并吡啶类化合物有一定的植物生长调节活性；部分吡唑类化合物对小麦锈病和烟草花叶病毒有较好的抑制效果；部分1，2，3-噻二唑类化合物对烟草花叶病毒有很好的抑制效果，与商品药剂病毒A的效果相近。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。