化

Novel sodium 2-2-(alkylaryloxy-alkylamidoethanesulfonates (m+nAr-T, m, n: carbon numbers; Ar: aromatic nucleus; T: taurine) with high purity were synthesized through bromization, esterification, Fries rearrangement, Pd-catalyzed hydrogenation, Williamson reaction, and acylation, et al, using carboxylic acid, phenol and taurine as starting materials. The structures and purities were characterized.

以羧酸、苯酚和牛磺酸为原料，通过溴代反应、酯化反应、Fries重排反应、催化氢化反应、Williamson反应以及催化酰胺化反应等过程，首次成功合成并表征了系列结构明确的高纯度N-酰基牛磺酸钠(m+nAr-T，m、n为烷基链碳数，Ar为芳环，T表示taurine)。

The synthesis of poly{2-4-[bi(4-tetrabutylphenylamino]phenylphenylenenvinylene} was beginwith 4-tetrabutylbenzoic,through acylation、Hoffmann rearrangement、bromization、idionization、Ullmann reaction、bromization、condensepolymerization.

聚{2-[4-二(4-叔丁基苯胺基苯基]苯撑乙烯}是以对叔丁基苯甲酸为原料，经酰氯化、酰胺化、Hoffmann降解、碘化、Ullmann反应、溴化、缩聚反应得到。

Potassium bromide produced in the elimination step was cleaned with steam treatment, then used to bromize tert-Butyl alcohol, producing tert-butyl bromide.

为了回收中间元素澳，用水蒸汽蒸馏方法除去脱漠化氢后生成演化钾盐中的杂质，通过添加硫酸以再生漠化钾用于叙丁醇漠化制漠代叔丁烷。

Based on the absorbance change of indicators with the concentration of hydrogen ion released from the enzyme-catalyzed reaction, a convenient colorimetry method is established for the assay of acidic phospholipase 〓 and glycogen phosphorylase b Brilliant yellow and bromothymol blue are chosen as indicators for assays of acidic phospholipase 〓 and glycogen phosphorylase b by following the absorbance changes at 495 nm and 615nm respectively The method is simple, sample-saving, sensitive and valid for a wide range of enzyme concentrations.

为了研究糖原磷酸化酶的激活动力学和酸性磷脂酶〓的复性过程，我们根据酶催化反应中释放氢离子浓度的变化引起相应的指示剂的光吸收发生变化的原理，建立了一种简捷的比色法，用于测定酸性磷脂酶〓和糖原磷酸化酶b的活性。选用亮黄和溴麝香草酚兰分别作为酸性磷脂酶〓和糖原磷酸化酶b测活的指示剂，在495 nm和615 nm处检测二者的光吸收值的变化，可以测定酶活。本方法的优点是，可在比较宽的酶浓度范围内进行活力测定，而且操作简单、节省样品、灵敏度高。

Cellulose acetate butyrate with high or low degree of butyryl substitution was synthesized in heterogeneous system(butyric acid/ acetic acid/ butyric anhydride/ sulfuric acid) using the "free solvent" method. The effect of activation time, esterification time, the molecular weight of cellulose and the content of the organic acid or anhydride on the degree of acetyl and butyryl substitution of cellulose was discussed.

在非均相体系中进行酯化反应，采用&反应性溶剂&，以硫酸作为催化剂合成出从高丁酯含量到低丁酯含量的纤维素醋酸丁酸酯，研究有机酸以及酸酐的添加量、活化时间、酯化反应时间以及原料纤维素的分子量对酯化产物纤维素醋酸丁酸酯的影响。

objectiveto study the protective and therapeutic effects of the extract of retinervus luffae fructus and carapax trionyei on con a-induced hepatic fibrosis in balb/c rats.methodsthe hepatic fibrosis in rats was first induced by intravenous injection of concanavalin a, the treatment in both protective and therapeutic stage was performed by subcutaneous injection of the extract.

目的 探讨鳖甲复方中药针剂对con a在balb/c雄性小鼠中诱导肝纤维化的预防和治疗作用。方法采用con a诱导肝纤维化，造模期间及造模成功后均用复方中药针剂干预药剂组，比较组间各项血液生化指标和肝脏组织学方面的差异，以探讨针剂对肝纤维化的预防和治疗作用。

The main steps include as follows: CO2 is led into the mother liquor of sodium meta-aluminate to carry out carbon content decomposing; the primary separation between the aluminum and the gallium is realized by primary carbonatation to filter out sodium hydroxide; secondary carbonatation is carried out on the filtrate to obtain the deposit of the complex salt of gallium and aluminum; a sodium carbonate crystal is obtained after the filtered filtrate is condensed and vaporized; the deposit of the complex salt of gallium and aluminum is dissolved in the mother liquor of sodium meta-aluminate; the processes are repeated until the proportion of gallium and aluminum in the complex salt of gallium and aluminum is larger than 1/340; then the complex salt of gallium and aluminum is added into the NaOH liquor and electrolyzed, thus obtaining the metal gallium with a purity larger than 99.9 percent which reaches the level of 3; simultaneously, the byproducts of the aluminum hydroxide and the sodium carbonate during the process of carbonatation by steps are obtained.

主要步骤包括：向铝酸钠母液中通入CO 2 进行碳分分解，一次碳酸化实现铝镓的初次分离；过滤出氢氧化钠，滤液进行二次碳酸化获得镓铝复盐沉淀，过滤后滤液经浓缩蒸发获得碳酸钠晶体，铝镓复盐沉淀溶解在偏铝酸钠母液中，重复上述过程直至铝镓复盐中的镓铝比例大于1/340，将其加入到NaOH溶液中，电解可获得纯度＞99.9％的金属镓，达到3N级水平同时在分步碳酸化的过程中获得氢氧化铝和碳酸钠副产品。

Because there are many complex factors resulting in concrete cardonated,the experimences of other peoples must be used in line with local conditions and materials other than simply when study on carbonation speed and evaluation of proof carbonification.

由于影响混凝土碳化的因素复杂多变，在研究碳化速度，评价其抗碳化性能优劣时，应因地、因材制宜，不能生套别人的经验。

To make a new interpretation of As I Lay Dying by Faulkner, and reveal the carvelesque features of the novel in terms of narration, structure and genre, in the perspective of Bakthins carnivalesque theory, the carvelesque features of the novel can be generalized in three aspectsduality, polyphony and alteration.

从狂欢化视角对《我弥留之际》做新的解读，分析其叙事、结构和体裁上呈现出的狂欢化特征，可以将《我弥留之际》的狂欢化特征归纳为复调、两重性和死生交替。

The research indicated that the main electric particles forming guiding discharge channel were the electrons released from the process of the breaking up of the negative ions. During 10 microseconds after the laser pulse, the electrode also could guide discharge effectively; and it suggested the new conception of the electrode erosion, and developed new-type running disk electrode, which could discharge for a million times in atmosphere. It also suggested methods of the texturing roller of besmearing with oil film and cathodal discharge in processing. The research of the texturing roller indicated that roughness of 14 microns and the intensified depth of over 200 microns could be got.

研究表明：形成诱导放电通道的带电粒子主要是负离子解离过程释放的电子，在激光脉冲结束后10微秒内，电极都能有效诱导放电；提出了电极损耗的新概念，并研制了新型转动圆盘电极，可在大气中完成上百万次放电，提出了加工过程中负极性放电、工件表面涂介质薄膜放电的毛化工艺方法；并用之对轧辊试件进行了毛化工艺研究，毛化粗糙度可达14微米，强化深度大于200微米。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。