加氨

Adopting quartz sand and active carbon to filtrate have achieved good results,and biological turnplate made biological filtrating and contemporary removed ammonia-nitrogen.

采用石英砂加活性炭过滤，其效果显著且经济，生物转盘进行生物过滤能同时去除氨氮，臭氧杀菌方便卫生且兼有增氧作用。

The result indicated that the reacting mixture containing dioxane 11.3mL/g HDCA which had been added ethyl chloroformate drop wise should be keep at 10℃ for 30min, then, rising to 15℃ for another 20min in the step of forming mixed anhydride ,and 1.5mol/L NaOH was used to dissolve taurine before aminolysis, and crude product was recrystalled by acetone in purifying process.

结果表明，形成混酐时，二氧六环用量为11.3ml/g HDCA，滴加氯甲酸乙酯后先在10℃反应30min，再在15℃下反应20min；用1.5mol/L的NaOH水溶液溶解牛磺酸后再进行氨解；粗产品用丙酮重结晶。

Better denitrification efficiency could be obtained with adding amylo and the removal ratios of ammonia nitrogen were at least 93%. The removal ratio of TN increased gradually with the increasing of C/N ratio. When C/N ratio was 10, the best removal ratio of TN could reach 80.81%. But when C/N ratio added on 12, the ratio removal of TN was not increased only keeping about 75%.

投加淀粉调整C/N比，系统能取得良好的脱氮效果，氨氮的去除率均在93%以上，随着C/N比的增加，TN的去除率也逐渐的增大，当C/N为10时，TN最高去除率能达到80.81%，但当C/N增大到12时，TN的去除率不再增大，只是稳定在75%左右。

More and more attention is focusing on the safty of drinking water suply. In this paper, firstly, chloramine formation and the characteristics and kinetics of monochloramine autodecomposition were studied. Secondly, considering the high concentration of ammonia and the complication of organic matters in Shanghai Huangpu River, formation characteristics and rules of disinfection byproducts were reviewed during the breakpoint chlorination process, and on the basis of grading and clssification of organisms, the control effects of chloramination on DBPs formation were studied. Finally, the formation rules of 2-monochlorophenol, 2,4-dichlorophenol and 2,4,6-trichlorophenol from phenol chlorination were investigated, and related influencing factors and kinetics were analysed.

饮用水的安全供给受到越来越多的重视，本文首先进行了氯胺形态以及一氯胺自降解特性及其动力学研究；然后结合上海黄浦江水源氨氮浓度高、有机物成分复杂的特点，研究折点加氯过程中消毒副产物的生成特性和规律，以及在将有机物分级和分类的基础上，研究氯胺消毒对不同类别有机物生成消毒副产物的控制效果；最后考察了氯化苯酚生成2-一氯酚(2-MCP)、2，4-二氯酚(2，4-DCP)及2，4，6-三氯酚(2，4，6-TCP)的规律，并进行了影响因素和动力学分析。

A compound 2-(3-hydroxyphenyl)[60] fullerene pyrrolidine was synthesized by the 1,3-dipolar cycloaddition reaction of the fullerene(C60) and azomethine ylide (prepared from glycine and 3-hydroxybenzaldehyde). The product was characterized by UV-Vis,1H-NMR ,FT-IR and MS. The reaction conditions affecting the yields of product were investigated and the optimum reaction conditions with product yield 75%(based on consumed C60) were:molar ratio of C60∶3-hydroxybenzaldehyde:glycine 1∶3∶6,reaction temperature 95℃,reaction time 18h.

利用甘氨酸和3-羟基苯甲醛与C60发生1， 3-偶极环加成反应，合成分离得到了2-(3-羟基苯基)[60]富勒烯吡咯烷，用UV-Vis、1H-NMR、FT-IR、MS等测试手段表征了产物的结构，并通过单因素方法，探讨了反应条件对产物产率的影响，得到最佳工艺条件：反应物摩尔比1∶3∶6，温度95 ℃，反应时间18 h，产物的产率可达75%（以消耗的C60计）。

A salt or ester of butyric acid .

加有一个碘原子的酪氨酸。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2，6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐，然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基，而擅转乙酰，氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂，加氯。

Methods: 60 cases of chronic severe hepatitis were divided into observe group and control group randomly, 30 cases in respectively. Control group was treated with routine approaches comprised of liver protecting, kata-ALT, detoxicating and albumin supplementing, et al, at the same time, adding colon herbs dialysis to the cases of observe group with HC-3000 therapeutic machine. At first, intermittence lavage using coloclysis solution at the depth of 50cm, 60min, then infund 100~200ml herbs colon dialysis solution constituted by rhubarb, acori graminei, semen raphani, dandelion, oyster and cornu bubali, at al, remaining 1~2h, biw, continuous 4wks. Observe the amelioration of primary symptoms, physical signs and complications in all of the cases, as well as the change of liver function, prothrombin time and the contents of blood ammonia.

60例慢性重型肝炎患者按分层随机配对分为观察组和对照组各30例，对照组给予常规护肝、降酶、退黄以及补充白蛋白等支持治疗，观察组在基础上加用HC-3000结肠途径治疗机透析治疗，每次先用结肠灌洗液间歇灌洗60min，深度50cm，然后注入由大黄、石首蒲、莱菔子、蒲会英、牡蛎、水牛角等组成的中药结肠透析液100~200mL，保留灌肠1~2h，每周2次，连续4周后观察患者主要症状、体征及并发症的改善情况，同时检测治疗前后肝功能(TBil、ALT、ALB、CHE)、凝血酶原时间和血氨(NH3)等指标。

This dissertation is mainly focused on the reactivity of methylenecyclopropanes and comprises six parts. 1 The reactions of methylenecyclopropanes with phenylsulfenyl chloride, phenylselenyl chloride and diphenyl diselenide; 2 The coupling reactions of the ring-opening products derivated from methylenecyclopropanes; 3 The palladium-catalyzed ring-enlargement of mono-aryl group substituted methylenecyclopropanes to cyclobutenes. 4 The gold-catalyzed domino ring-opening and ring-closing hydroamination of methylenecyclopropanes with sulfonamides; 5 The Lewis acid-catalyzed reactions of mono-aryl group substituted methylenecyclopropanes with diethyl ketomalonate in the presence of water; 6 The iodobenzene diacetate mediated novel 1,3-dipolar cycloaddition of methylenecyclopropanes, vinylidenecyclopropanes, and methylenecyclobutane with phthalhydrazine.

本论文主要研究了亚甲基环丙烷类化合物的一些化学反应性能，共由以下六部分组成：1、亚甲基环丙烷类化合物与苯硫氯、苯硒氯及二苯基二硒的反应；2、亚甲基环丙烷类化合物开环产物的偶联反应；3、单芳基取代的亚甲基环丙烷类化合物在钯催化剂作用下的扩环反应；4、金化合物催化磺酰胺对亚甲基环丙烷类化合物的串联开环关环氨氢化反应；5、路易斯酸催化亚甲基环丙烷类化合物与丙酮二羧酸二乙酯在有水存在下的反应；6、醋酸碘苯促进的亚甲基环丙烷类化合物、亚乙烯基环丙烷类化合物及亚甲基环丁烷类化合物与邻苯二甲酰肼的新型1，3-偶极环加成反应。

The test method is to fetch the urea of the same quality and coated material of different quality first, make coating material parcel evenly the urea particle s surface, grant them into the soil, eluviate with the distilled water every 24 hours, collect the eluviationing solution, titrate the eluviationing solution with distillation titrimetric method, that is, add alkali distillation, make the ammonia release out, absorb with boric acid solution, then titrate it with standard acid.

试验方法是称取相同质量的尿素和不同质量的包膜材料，将包膜材料均匀地包裹在尿素颗粒的表面，将包裹后的包膜肥料施入模拟试验的土壤中，每隔24个小时用蒸馏水淋溶，收集淋溶液，用蒸馏滴定法滴定淋溶液，即加碱蒸馏，使氨释放出来，用硼酸溶液吸收，而后用标准酸滴定之。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。