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Wood Vinegar is a natural material that is distilled from wood. It is compose of organic acid and hydroxybenzene , Various dosage of wood vinegars, pyrolignerous acid and guaiacol were mixed into organic manure firstly in this experiment, and then, the above said organic manure are separately added into soil. Under the analysis of the amount of the edaphon, adding 10g wood vinegar to 1kg organic manure and 30kg soil can much active the edaphon effectively in a short term and make a maximum rising extent of edaphon numbers.

木醋液是从多年生柞木中经过高温蒸馏出来的纯天然物质,其主要成分是有机酸和酚类物质,为了明确木醋液和主要成分对土壤微生物的作用,将加入不同剂量的木醋液、愈创木酚、醋酸的有机肥施入土壤,观察土壤中微生物数量的变化,结果表明:在1kg有机肥中加入10g木醋液,施入30kg土壤中,土壤微生物数量增加幅度最大,土壤微生物10天内被有效地激活;同时,当在1kg有机肥中木醋液的添加量高达50g时,对土壤微生物有一定的抑制作用。

Anthocyanidin extract in methanol showed 3 absorption peaks, at 270, 340 and 520 nm, in the UV-vis spectrum, with bathochromic and hypsochromic shift with methanol+AlCl3 and methanol+AlCl3+HCl, respectively; the ratio of the absorbance at 440 nm to that at 520 nm was 0.29. No fluorescence occurred under UV irradiance, and 5 absorption peaks occurred at 270 nm after HPLC. Five molecular ion peaks occurred on MS: 595, 381, 611, 587 and 571, respectively, and monosaccharides in the extract were identified as rhamuose and glucose on HPLC.

一品红花色素的甲醇溶液分别在270、340 和520 nm 处有 3 个吸收峰;在 440 nm 吸光度与可见光最大吸收波长 520 nm 吸光度的比值为0.29;花色素的甲醇溶液中加入AlCl3后发生红移,再加入HCl后发生蓝移;色素溶液在紫外光下无荧光;色素样品经液相色谱分离后在 270 nm检测有 5 个比较明显的吸收峰;质谱中得到 595、611、381、571 和 589 等对应的分子离子峰;花色素酸解液高效液相色谱图谱和鼠李糖、葡萄糖的出峰时间一致。

This research which extends the new product supply chain model of Bulter et al. considers issues on global logistics from a more integrated view. First of all, it solves the global logistic settings problem in new product development by means of mixed-integer linear programming. Secondly, it uses the scenario-based robust optimization to lower the risk in the supply chain design. Then it adds the reliability calculation to make up for the gap between the plan and the real operation. At last it calculates and analyzes the quantitative model on the basis of the case data.

本研究延伸Butler等人之新产品供应链模式,考量更完整之全球运筹相关议题,透过混合整数线性规划描述新产品发展时全球运筹配置问题,并利用情境为基础的稳健最佳化以取得低风险的供应链配置,此外加入可靠度的影响,以弥补供应链规划与实际操作的差距,并加入缺货之惩罚成本,最后以范例资料进行计算与分析此数量模式,经由模式计算结果发现本研究规划之结果,相较於原Butler等人之模式有较低的缺货的发生可能性,且所求得之配置整体可靠度皆有所提升。

First,the content of surfactant should be more than 18 percent and the content of anion surfactant should be kept in proper proportion to the content of nonionic surfactant. Second,the content of zinc naphthenate should be kept in directly proportional to the content of other surfactant. Third,the content of rosin shouldnt too higher and the content of oleic acid should be kept in directly proportional to the content of rosin. Fourth,the content of water should be kept in a low level (less than 8%);otherwise emulsifier oil will delaminate. In addition,the requisite content of sodium heavy alkyl benzene sulfonate is higher than petroleum sulfonate.

试验表明在以松香、重烷磺酸钠、石油磺酸钠为主要乳化剂时,要获得优良的乳化液,需满足以下几个条件:(1)需在乳化油配方中加入适量的乳化剂,且其中阴离子乳化剂总量与非离子乳化剂总量的应保持适当的比例;(2)乳化油中环烷酸锌的量与其它乳化剂总量要保持正比关系;(3)乳化油中松香的量不易过大,且油酸的加入量应与松香量成正比;(4)乳化油中水分含量不易过高(一般不能大于8%),过高时稳定性不好,易分层。

The reason may be that complex formed by rhodium and halide was difficult to produce the catalytic active species. Therefore halide ion was the poison for the rhodium catalyst in hydroformylation of olefins in ionic liquid. The effect of double long chain cationic surfactant (DCMAB, dicetyl dimethylammonium bromide) on selective hydrogenation of cinnmaldehyde catalyzed with RuCl3·x H2O/TPPTS was studied.

进一步的研究表明在使用有良好反应活性的两种催化剂HRh3 、Rh_2进行催化反应时,向体系中加入含有卤离子的化合物时将使反应活性大大降低,而且随着卤化物加入量的增加,催化剂的活性迅速下降,这是卤离子可能和金属铑作用使它难于生成催化活性物种,进一步证明卤素离子是引起催化剂活性下降的极其重要的因素。

Wood Vinegar is a natural material that is distilled from wood. It is compose of organic acid and hydroxybenzene , Various dosage of wood vinegars, pyrolignerous acid and guaiacol were mixed into organic manure firstly in this experiment, and then, the above said organic manure are separately added into soil. Under the analysis of the amount of the edaphon, adding 10g wood vinegar to 1kg organic manure and 30kg soil can much active the edaphon effectively in a short term and make a maximum rising extent of edaphon numbers.

木醋液是从多年生柞木中经过高温蒸馏出来的纯天然物质,其主要成分是有机酸和酚类物质,为了明确木醋液和主要成分对土壤微生物的作用,将加入不同剂量的木醋液、愈创木酚、醋酸的有机肥施入土壤,观察土壤中微生物数量的变化,结果表明:在1kg有机肥中加入10g木醋液,施入30kg土壤中,土壤微生物数量增加幅度最大,土壤微生物10d内被有效地激活;同时,当在1kg有机肥中木醋液的添加量高达50g时,对土壤微生物有一定的抑制作用。

Firstly,two novel rare earth complexes(CH_2=CHO)Ln~Ⅲ[2,6-_2PhNSiMe _3]_2Li_3Ln=Y(2,Yb(3)containing arylamido and enolate mixed ligands have been synthesized by treatment of 2 equiv of of 2,6-~iPr_2PhNHSiMe_3 with exces n-BuLi at -78℃in THF for 12h,followed by reaction with 1 equiv of LnCl_3at 80℃for 24h in one-pot.All the two compounds were characterized by spectroscopic methods,elemental analyses,and a single-crystal X-ray diffraction study.

首先,-78℃下,在两当量的2,6-~iPr_2PhNHSiMe_3(1)THF溶液中加入过量的n-BuLi,反应12小时,再加入一当量的LnCl_380℃下,反应24小时,一锅法合成了含胺基、乙烯醇基混合配体的新型稀土金属配合物(CH_2=CHO)Ln~Ⅲ[2,6-_2PhNSiMe_3]_2Li_3Ln=Y(2、Yb(3),上述化合物结构经单晶X-ray衍射、光谱和元素分析表征,表明我们得到的是一类新型的三价稀土配合物。

Circular dichroism spectroscopy measurements also reveal that the ordered structure content of α-helical and β-structure of ovalbumin decrease, and the unfolded random structure is enhanced with increasing pressure; While the existence of dextran sulphate to the native ovalbumin, there are no apparent change on the secondary structure of ovalbumin; It seems same to glycinin.

圆二色性光谱分析表明,经超高压处理后,鸡蛋清蛋白分子中规则的二级结构减少,而部分规则的二级结构和无规卷曲含量增加。加入硫酸右旋糖苷的鸡蛋清蛋白溶液经超高压处理后其二级结构中各部分的含量变化不大:对于大豆豆球蛋白,加入硫酸右旋糖苷后,大豆豆球蛋白分子经超高压处理后其有序结构的减少及无规卷曲的增加都相对减缓。

We upgrated the Visual Motion Priming model proposed by Pantle, that means to insert a blank frame between priming and target. The goal is to explore the mechanism of visual motion priming in the brain. Method: Undergraduates on campus participated the experiments as paid volunter with normal or corelected normal version.

因此本实验对Pantle的视觉运动启动实验模式进行了改进,由特定运动方向的启动刺激引导靶刺激,在启动刺激与靶刺激之间加入一个空白阻断图片,从而打断启动——靶刺激的正常启动序列,目的是观察加入空白阻断图片,对于运动启动现象的影响以及对不同的视觉运动序列运动方向的影响。

The high sulfur coal from Jiexiu in Shanxi is used in this experiment and the influence of removing pyritic sulfur by adding different pyrites depressors on the process of agglomeration was explored in this study,The experiment result shows that adding pyrites depressors on the process of oil agglomeration can improve the sulfur-removing rate.

油团聚是以脱除煤中灰分为主的团聚技术,脱硫的效率很低,采用山西介休的高硫煤,探索在油团聚过程中加入不同的黄铁矿抑制剂(巯基乙酸、重铬酸钾、高锰酸钾)对脱除煤中黄铁矿硫的影响。结果表明加入黄铁矿抑制剂对脱硫效率有一定程度的影响

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