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Analysis of K and Na in nepheline were curried out with higher precision and repeatability by means of adding fluohydric acid during sample melting to remove SiO2 ,adjusting the ratio of K and Na in the solution to reduce the mutual interference of the two elements, and adding cesium chloride to eliminate ionization interference.

摘要本方法用于测定霞石中的钾、钠,主要通过在溶样时加入氢氟酸除去二氧化矽,调整溶液中钾、钠的含量,消除互相之间的干扰,加入氯化铯消除电离因素的干扰,提高了分析结果的准确性和重现性,使测定结果更接近化学分析值。

Analysis f K and Na in nepheline were curried out with higher precision and repeatability by means of adding fluohydric acid during sample melting to remove SiO2, adjusting the ratio of K and Na in the solution to reduce the mutual interference of the two elements, and adding cesium chloride to eliminate ionization interference.

摘要本方法用于测定霞石中的钾、钠,主要通过在溶样时加入氢氟酸除去二氧化矽,调整溶液中钾、钠的含量,消除互相之间的干扰,加入氯化铯消除电离因素的干扰,提高了分析结果的准确性和重现性,使测定结果更接近化学分析值。

The results indicated that HDPCs'proliferation was inhibited significantly when they were cultured in DMEM with 50、100μg/mlLPS. Low-dose of Chinese nutgall water extracts( 1.25、2.5、5μg/ml) resisted the inhibitory effect of LPS to HDPCs'proliferation significantly .From the third day , the proliferation activity of HDPCs incubated with 2.5μg/ml Chinese nutgall water extract and LPS increased signicificantly in a time-dependent manner.

结果显示,培养液中加入浓度为50μg/ml、100μg/ml的LPS时,HDPCs的增殖活性受到明显抑制,加入低浓度(1.25μg/ml、2.5μg/ml、5μg/ml)五倍子水提取物能明显拮抗100μg/ml的LPS对HDPCs增殖的抑制作用,2.5μg/ml五倍子水提取物拮抗100μg/ml的LPS对HDPCs增殖抑制作用第3天开始明显增加,并呈时间依赖性。

The room temperature modulus and high temperature modulus of cured samples with low content of onium salt initiator have little change before and after the addition of co-initiator.

碘锚盐引发剂含量较低时,加入共引发剂的体系的常温及高温模量与未加体系相比没有明显变化;碘锚盐引发剂含量较高时,加入共引发剂的体系的常温模量比未加体系有所上升,而高温模量则变化不大。

Results showed that green firm callus and rooting were obtained with treatments of NAA 0.5-3.0mg/L, in which the NAA 0.5mg/L treatment appeared the optimal rooting result of 90%. White loose callus was obtained with treatment of 2,4-D0.1-3.0 mg/L.Callus can not be induced by adding BA solely at 0.5-3.0mg/L. There appeared bud redifferentiation only when appropriate concentration of combined BA,NAA and 2,4-D were applied.

结果表明:单独加入NAA0.5~3.0mg/L可诱导出绿色致密的愈伤组织,并再生出根,其中NAA0.5mg/L处理生根率最高,达90%;单独加入2,4-D0.1-3.0mg/L可诱导出白色疏松的愈伤组织;单独使用BA0.5—3.0mg/L不能诱导出愈伤组织;BA与NAA或2,4-D只有在适当的质量浓度范围内配合使用才能分化出芽,芽分化率最高的处理为BA3.0mg/L+NAA0.5mg/L,分化率为30%。

The effect on the mechanical and electrical properties of the flame retardant agents especially the metal chelates was studied.

对阻燃剂的加入,尤其是金属配合物的加入对材料的力学性能和电性能的影响进行了研究。

According to the result of experiments, the author point out that the high strength and high collapsibility resin coated sands used in producing the aluminum alloy castings should be:① using rounded or near rounded sand;② using ordinary PF resin;③ using some strengthening and toughening agents;④ using satiable collapse agents.

作者通过大量的试验研究得出以下结论:用于生产铝合金铸件的高强度、易溃散覆膜砂应:①选择粒形圆整的原砂;②选用普通热塑性酚醛树脂;③加入一定量的增塑类添加剂;④加入适宜的溃散剂。

It was admitted as the 24th state in 82. Under Spanish control from 7'2 to 800, the area passed to the United States through the Louisiana Purchase of 803. Organized as a territory in 82, Missouri's application for admission as a slaveholding state in 87 sparked a bitter controversy over the question of extending slavery into new territories. The Missouri Compromise of 820 provided for the admission of Maine as a free state and Missouri as a slave state in the following year.

于82年被接受为第二十四个州。7'2年到800年,此地区处于西班牙的控制下,美国于803年在路易斯安那购买行动中获得这一地域。82年成为一个地区。87年密苏里申请以蓄奴州身份加入联邦导致了关于是否将奴隶制扩大到新地区的争论。820年的密苏里协议为次年作为自由州的缅因州和作为蓄奴州的密苏里州加入联邦铺平了道路。

After the solution was kept in the dark for five minutes,chloroform was added into it to adsorb selenium formed by previous reaction,then iodine separated out was determined by sodium hyposulfite titration using starch as the indicator,at last the content of selenium dioxide in the sample was foun.

在溶有二氧化硒的0.4~0.5mol/L盐酸介质中,加入过量的碘化钾,于暗处放置5min后,加入三氧甲烷吸附反应生成的硒,以淀粉为指示剂,用硫代硫酸钠标准溶液滴定析出的碘,测得二氧化硒的含量。

The anode catalyst for direct methanol fuel cell is Pt-W-Sn/C, and it is prepared through dispersing carbon black in distilled water, adding H2PtCl6, tungstate and stannate, stirring to make the metal salt and H2PtCl6 adsorbed fully; dropping reductant to reduce and deposite until complete reaction; washing with distilled water, filtering and drying to obtain black C carried sanitary Pt-W-Sn catalyst. The catalyst has excellent methanol catalyzing activity and low cost, and its use can lower the cost of direct methanol fuel cell greatly and raise the performance/cost ratio of the cell.

一种直接甲醇燃料电池阳极催化剂是Pt-W-Sn/C;其制备方法是将碳黑分散在蒸馏水中,然后加入H2PtCl6、钨酸盐和锡盐,搅拌使得金属盐与H2PtCl6被充分吸附;逐滴加入还原剂使之还原沉积,待反应完全后,用蒸馏水洗涤,过滤,然后于干燥箱中干燥,便得到黑色的C负载Pt-W-Sn三元催化剂;该催化剂具有很好的甲醇催化活性,价格低廉,可以大大降低直接甲醇燃料电池的成本,提高电池的性能价格比和市场竞争能力。

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