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The results indicate that the optimized sulfonylation reaction time is 4 h, the materiel rate of chlorosulfonic acid and 2-chloroimidazo[1,2-α]pyridine is 1.2 : 1, with ethylamine the yield increasing from 15.4% to above 70%; the optimized ammonolysis reaction time is 3 h and the reaction temperature is 27℃, with the acetonitrile yield increasing from 60.1% to above 79.6%.

实验结果表明,磺酰化反应的最佳反应时间为4 h,氯磺酸与2-氯咪唑并[1,-α]吡啶的用量比为1.2:1,加入三乙胺可将收率由15.4%提高到70%以上;氨解反应的最佳反应时间为3 h,反应温度为27 ℃,加入乙腈可将收率由60.1%提高到79.6%;方案经改进后,总反应时间缩短3 h,收率提高了5.5%。

Shake recipe with ice, strain over ice and top with soda water. Like most sours, fizzes and Collinses, many add either some raw egg white (which creates a nice foamy head on the cocktail when shaken) or some bitters such as Angostura or orange bitters, to taste. Egg white is said to be essential for a Fizz, but optional for a Sour or Collins.

按配方加冰摇合,滤入冰块倒苏打水,象许多酸酒,菲士和科林斯一样,不仅加入生鸡蛋清(这样在摇合的时候会出现达的泡沫),还加入安哥拉斯或橘子苦精增加口感,加蛋清在菲士里是很重要的,但是酸酒和科林斯则不同。

The method of orthogonal experiment was used to investigate the effect of parameter of boronizing process on the thickness of the boride layer.

运用正交实验法来确定渗硼工艺的参数(渗硼温度、渗硼时间、稀土加入量和铬加入量)对渗硼层厚度的影响,从而确定合理的渗硼工艺。

The steps for preparing insecticide include: first shaking flask for fermentation, adding amidon, soya bean cake powder, cotton cake powder, protease leather, yeast powder, maize milk, magnesium sulfate heptahydrate, monobasic potassium phosphate, dibasic potassium phosphate, calcium carbonate alpha-amylase and make-up water by ratio in culture medium with 100 unit volumes; secondarily filling 100ml culture mediums in triangular bottle, then seeding BTH-13 after disinfection and culturing them until the brood-cell pulls off under finite temperature; third adopting the selected culture medium and fermenting them in full-automatic fermentation tank, acidifying the fermentation liquor after the fermentation, adding the emulsifier, and directly performing spray-drying after the compression of the fermentation liquor to prepare the wettable powder.

制备杀虫剂的步骤是:首先是摇瓶发酵,在100单位体积的培养基中,按比例加入淀粉、豆饼粉、棉饼子粉、蛋白胨、酵母粉、玉米浆、七水硫酸镁、磷酸二氢钾、磷酸氢二钾、碳酸钙、及α-淀粉酶,补充水;其次是在三角瓶中装100ml培养基,灭菌后接种BTH-13,在一定温度培养至芽孢脱落;第三是采用筛选出来的培养基,在全自动发酵罐中进行发酵,发酵结束后发酵液酸化,加入乳化剂,酵液浓缩后直接喷雾干燥制备可湿性粉剂。

Using the solid boronization cut-and-try method determined the boronization craft the parameter (boronization temperature, boronization time, rare earth join quantity and chromium join quantity) to the boronization level thickness influence, thus determines the reasonable boronization craft route.

运用固体渗硼实验法来确定渗硼工艺的参数(渗硼温度、渗硼时间、稀土加入量和铬加入量)对渗硼层厚度的影响,从而确定合理的渗硼工艺路线。

Of the other members of his team, Laufer went to France after the war and joined SNCASO, where he worked on the jet-propelled Djinn, and Stepan went to England, where he joined Fairey and also does work connected with jet-propelled rotary wings.

对他的团队的其他成员,劳费尔前往法国在战后加入SNCASO,他在喷气推进灯灵工作,并斯捷潘到英国,在那里他加入了费尔雷,也没有与工作有关的喷气推进旋转翼。

When his editor, John Farrar, joined Stanley Rinehart to form a new publishing house, Brinig went with them.

当他的编辑约翰法勒加入斯坦利莱因哈特组建的一个新的出版社,布里尼格也加入了他们。

The experiment system of caustic soda in the process of Glauber's salt key point is the inclusion of sodium bicarbonate, sodium bicarbonate accession greatly improved the conversion rate of caustic soda.

本实验在芒硝制烧碱过程中的关键点是加入了碳酸氢钠,碳酸氢钠的加入大大提高了烧碱的转化率。

Gwendolyn Hatcher, former inspector general of the city Department of Cultural Affairs, told a federal jury that an outraged Myerson stormed into her office with three of her top aides in tow.

前市文化局调查主任哈彻告诉联邦陪审团说:怒气冲冲的迈尔森带领着她的三个高级幕僚闯入她的办公室。请在后台加入相关信息,比如加入广告。

Up to the present, we have not be so close to world pulses jumpiness and such deep feel the global competition and various culture. The Dec 11th 2001, the protocol of China be a member of WTO took in effect, China became to be the one hundred and fourty third member of WTO in due form.

时至今日,我们从来没有与世界脉搏的跳动如此地接近,从来没有如此深切地感受到全球化的竞争和各种各样的文化。2001年12月11日,中国加入世贸组织议定书生效,中国正式加入世界贸易组织,成为第143个成员。

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By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候,里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色,卵在发育96h后卵基本全部孵化。

There was a conflict between plebs and patricians in ancient Rome in 494BC.

在公元前494年,罗马发生了一次平民反对贵族的斗争。