加入甲醇的

It indicates that the yield of DMC is improved by adding dimethyl ether that consumes product water by hydrolysis.

在甲醇氧化羰化体系中加入少量二甲醚可以提高DMC的产率，并且对二甲醚的加入量影响进行了考察。

The method is realized by that polyether ether ketone is added into concentrated sulfuric acid to carry out sulfonation reaction, thereby obtaining sulfonated polyether ether ketone, then the sulfonated polyether ether ketone is dissolved in organic solvent, N, N (1)-Carbonyldiimidazole is added to stir for one to three hours, coupling agent is mixed for stirring the reaction for 1.5 to 4 hours, then inorganic crosslinking agent is mixed to react under the temperature of 50 to 80 DEG C. Proton conductors are mixed to continue getting the mixed solution of the sulfonated polyether ether ketone or the inorganic crosslinking agent or proton conductors under the temperature. Finally the proton exchange membrane for a direct methanol fuel cell is obtained by that the mixed solution of the sulfonated polyether ether ketone or the inorganic crosslinking agent or proton conductors is/are processed through membrane forming, drying and exuviation.

该方法首先将聚醚醚酮加入浓硫酸中进行磺化反应得到磺化聚醚醚酮；然后将磺化聚醚醚酮溶于有机溶剂中，加入N，N′-羰基二咪唑搅拌1～3小时后加入偶联剂搅拌反应1.5～4小时，再加入无机交联剂在50～80℃下反应，然后加入质子导体继续在此温度下反应得到磺化聚醚醚酮/无机交联剂/质子导体的混合溶液；最后将磺化聚醚醚酮/无机交联剂/质子导体的混合物溶液成膜，干燥，脱膜即得到所述的直接甲醇燃料电池用质子交换膜。

40 Drops of your favorite essential oil or essential oil blend keeping the safety data of the chosen essential oil in mind 1.5 ounces of distilled water and 1.5 ounces of high-proof alcohol (vodka is suitable, rubbing alcohol is not) or 3 ounces of distilled water.

加入1.5盎斯的蒸馏水及1.5盎斯的高纯度酒精（伏特加是一个满适合的选择，注意不要用工业用酒精－甲醇）或者就只加入3盎斯的蒸馏水。

The ammonia was evaporated under decreasing pressure, and the precipitate was filtered off and the liquid was poured into hot saturated picric acid solution to get picrate with a yield of 85.0%. The optimum process starting from imidazole-4,5-dicarboxylic acid was: imidazole-4,5-dicarboxylic acid in acetic anhydride was refluxed to get imidazole-4-carboxylic acid, and the product was esterification in ethanol with a catalyzer of concentrated sulfuric acid to get ethyl imidazole-4-carboxylate, at last the compound above was reduced by LiAlH4 in ether at room temperature to get the target compound, the total yield of this route was 49.6%.

以4，5-二羧酸咪唑为原料的较佳工艺：1 脱羧反应：4，5-二羧酸咪唑40g，醋酐1200ml，回流10h，过滤并将滤液浓缩至干，所得固体加至50%的乙醇溶液回流，过滤并将滤液自然冷却过夜，过滤得固体；2 酯化反应：4(5)-羧酸咪唑50g，乙醇1000ml和浓硫酸60ml，加热回流2h，5%浓度NaOH溶液调节至pH＝8，减压浓缩至干，加入少量水回流，自然冷却过夜并过滤得固体；3 还原反应：LiAlH410g，乙醚300ml和4(5)-羧酸咪唑乙酯28g，常温反应1.5h，小心滴加25ml水后过滤，滤渣溶于300ml甲醇中并过滤，收集所得乙醚和甲醇滤液浓缩至干，将所得固体溶于300ml乙醇中加热回流，后将溶液浓缩至约30ml，冷却并过滤得固体，该路线总收率为49.6%。

Ache with tristearin, sodium or nitrify cotton is coagulating agent, adopt the legal system of two steps Bei technology, in 65 ℃ respond , shell mellow wine: tristearin acid: the best proportion of the sodium of sodium hydroxide is 91: 6.5: 1, compound with two methods solid shell mellow wine, at the same time join stabilizing agent , eliminate smoke dose , restrain volatilizer and fireworks modifier etc., is as hydration alumina eliminate smoke dose, raise the integral performance of solid shell pure fuel.

以硬脂酸钠或硝化棉为凝固剂，采用两步法制备工艺，在65℃时进行反应，甲醇：硬脂酸：氢氧化钠钠的最佳比例为91：6.5：1，用两种方法配制出的固体甲醇，同时加入稳定剂、消烟剂、抑制挥发剂、焰火改性剂等，如水合氧化铝作为消烟剂，来提高固体甲醇燃料的综合性能。

A method for the separation and determination of Pueraria lobata isoflavonoid extract by reversed-phase high performance liquid chromatography was proposed.

采用反相高效液相色谱法，在C1 8柱上以甲醇水为流动相进行梯度洗脱，在 0～ 1 0min内将葛根黄酮提取物进行分离，并在 2 5 0nm检测，采用标准加入法对实际样品中的葛根素含量进行了分析。

With the extraction efficiency of rotenone and total substance obtained as estimated index, the technology conditions of extracting rotenone from the leaves of Tephrosia vogelii were investigated by SFE-HPLC method.

采用超临界流体萃取反相高效液相色谱法，以鱼藤酮萃取率和萃取产物总得率为评价指标，研究提出非洲山毛豆 Tephrosia vogelii Hook.f中鱼藤酮的超临界流体萃取较优工艺条件为：萃取物料粒径30目，静态萃取20min，萃取温度45℃，压力27.58MPa，流体总流量30mL/g，萃取前向萃取池中加入3mL甲醇作夹带剂。

A direct method to prepare nanometre catalyst of positive electrode for methyl alcohol fuel battery is to add strong oxidant to a mixed solution of manganese nitrate and some other metal nitrate, to coat them on the graphite electrode to have catalyst precursor produced, then to prepare the non-platinum nanometre catalyst of metal ion-doped manganese dioxide with carbon as a carrier by thermolytic reaction of the in-situ precursor. The prepared catalyst has the advantages of high electrical catalytic activity of methyl alcohol, high performance to protect against CO poison and low price, and it can lower the battery manufacturing cost effectively as well as can raise the entire electrical property of the battery so that the price performance and the market competitive edge of the battery are enchnaced effectively.

一种直接甲醇燃料电池阳极纳米催化剂的制备方法是在硝酸锰和其它金属硝酸盐的混合溶液中加入强氧化剂，涂抹于石墨电极上制成催化剂先驱体，通过先驱体在原位的热分解反应来制备以碳为载体的金属离子掺杂二氧化锰非铂纳米催化剂；制得的催化剂具有高的甲醇电催化活性、高的抗CO毒化性能以及低廉的价格等优点，可以有效地降低电池的制造成本，提高电池的整体电性能，从而有效地提高直接甲醇燃料电池的性能价格比及市场竞争能力。

Times. Benzyl alcohol could enhance Lip production as veratryl alcohol. At its optimal concentration of 5. 0mM, Lip activity was almost twice higher than that without addition of benzyl alcohol.

用藜芦醇的类似物苯甲醇可以代替藜芦醇作诱导剂强化木素过氧化物酶的合成，加入最佳浓度5.0mM的苯甲醇可以提高木素过氧化物酶的活力近一倍。

Samples were saponified with 20 g/L sodium hydroxide. The sexual hormones were then extracted with dichloromethane-acetic acetate (40∶1, v/v) under acidic conditions (pH 3, adjusted with 1 mol/L HCl ). An XTerraTMRP18 column was employed and a mixture of water-methanol-acetonitrile (50∶32∶18, v/v) was used as mobile phase. The seven sexual hormones were detected at 230 nm. The average spiked recoveries for the seven sexual hormones ranged from 75.6% to 97.8% with relative standard deviations of 1.9% to 7.2%. The linear ranges of determination were from 5 to 50 mg/L with correlation coefficients of 0.9999, and the limits of detection were from 3.7 to 12 ng.

先在试样中加入20 g/L氢氧化钠溶液与油脂进行皂化反应，然后用二氯甲烷-乙酸乙酯(体积比为40∶1)混合液在酸性条件下(pH 3)萃取，选择XTerraTMRP18色谱柱，以水-甲醇-乙腈(体积比为50∶32∶18)混合液为流动相，在波长230 nm处检测。7种性激素分离良好并排除了样品中杂质峰的干扰，低、高浓度平均回收率范围为75.6%~97.8%；相对标准偏差为1.9%~7.2%；检出限为3.7~12 ng。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。