加入甲醇的

The number of atomic and sub-surface oxygen species may decrease with the addition of iodine.

碘的加入可使原子氧和次表层氧物种种类更单一，更有利于甲醇的氧化脱氢反应。

A steel bar is washed and dried, and then put into a glass pipe which is sealed to obtain stirring magneton; a mixed solvent of Gamma-methacrylate oxide propyl trimethoxy silane and methanol is prepared and added with an organic base to obtain a pre-bonding solvent; the stirring magneton is immerged into the pre-bounding solvent, and the outer surface of the glass pipe of the stirring magneton is bonded with a layer of silane substance with alkenyl; a reactive monomer mixture and a pore-forming agent mixed solvent are evenly mixed and then added into a container, the stirring magneton after the pre-bounding is put into the container which is sealed and then put into a water bath; after reaction, the container is removed, the stirring magneton coated with a polymer is taken out and put into a extractor and extracted by using a solvent; or the stir bar is immersed into the solvent till no impurity can be checked in the solvent, thereby obtaining the product.

将铁条清洗干燥，放入玻璃管内，密封得搅拌磁子；配制γ-甲基丙烯酸氧丙基三甲氧基硅烷与甲醇的混合溶液，加入有机碱得预键合溶液，将搅拌磁子浸入预键合溶液，在搅拌磁子的玻璃管外壁键合一层带烯基的硅烷化物质；将反应单体混合剂和致孔剂混合溶液混匀后倒入容器中，将预键合后的搅拌磁子放入容器，密封后置于水浴中，反应后除去容器，取出涂有聚合物的搅拌磁子，置于提取器中，以溶剂提取，或将搅拌棒置于溶剂中浸泡至溶剂中无杂质检出，得产物。

High concentration of SO〓 did not interfere the determination of NO〓 because SO〓 was eluted later than NO〓. The effects of the concentration of sodium borate and CTAB on separation were also examined.

由于加入甲醇后，SO〓在NO〓后出峰，有利于河水中高浓度SO〓存在下，少量NO〓的测定，同时也考察了硼砂和CTAB的浓度对分离的影响。

The anode catalyst for direct methanol fuel cell is Pt-W-Sn/C, and it is prepared through dispersing carbon black in distilled water, adding H2PtCl6, tungstate and stannate, stirring to make the metal salt and H2PtCl6 adsorbed fully; dropping reductant to reduce and deposite until complete reaction; washing with distilled water, filtering and drying to obtain black C carried sanitary Pt-W-Sn catalyst. The catalyst has excellent methanol catalyzing activity and low cost, and its use can lower the cost of direct methanol fuel cell greatly and raise the performance/cost ratio of the cell.

一种直接甲醇燃料电池阳极催化剂是Pt-W-Sn/C；其制备方法是将碳黑分散在蒸馏水中，然后加入H2PtCl6、钨酸盐和锡盐，搅拌使得金属盐与H2PtCl6被充分吸附；逐滴加入还原剂使之还原沉积，待反应完全后，用蒸馏水洗涤，过滤，然后于干燥箱中干燥，便得到黑色的C负载Pt-W-Sn三元催化剂；该催化剂具有很好的甲醇催化活性，价格低廉，可以大大降低直接甲醇燃料电池的成本，提高电池的性能价格比和市场竞争能力。

In the residual titration, excess Reagent is added to the test specimen, sufficient time is allowed for the reaction to reach completion, and the unconsumed Reagent is titrated with a standard solution of water in a solvent such as methanol.

在回滴定法，过量的卡尔试剂加入到待测样品中，给与足够的时间去达到反应完全，未消耗的卡尔试剂用溶于溶剂例如甲醇的标准水溶液去滴定。

Anthocyanidin extract in methanol showed 3 absorption peaks, at 270, 340 and 520 nm, in the UV-vis spectrum, with bathochromic and hypsochromic shift with methanol+AlCl3 and methanol+AlCl3+HCl, respectively; the ratio of the absorbance at 440 nm to that at 520 nm was 0.29. No fluorescence occurred under UV irradiance, and 5 absorption peaks occurred at 270 nm after HPLC. Five molecular ion peaks occurred on MS: 595, 381, 611, 587 and 571, respectively, and monosaccharides in the extract were identified as rhamuose and glucose on HPLC.

一品红花色素的甲醇溶液分别在270、340 和520 nm 处有 3 个吸收峰；在 440 nm 吸光度与可见光最大吸收波长 520 nm 吸光度的比值为0.29；花色素的甲醇溶液中加入AlCl3后发生红移，再加入HCl后发生蓝移；色素溶液在紫外光下无荧光；色素样品经液相色谱分离后在 270 nm检测有 5 个比较明显的吸收峰；质谱中得到 595、611、381、571 和 589 等对应的分子离子峰；花色素酸解液高效液相色谱图谱和鼠李糖、葡萄糖的出峰时间一致。

Under the same conditions, the electrocatalytic ability of the electrode was higher than that of the pure Pt electrode.

结果表明Pt-Ru微粒电极对甲醇的电氧化显示出催化作用， Ru的加入提高了电极的抗中毒能力。

Glyoxylic acid was prepared by reaction of sodium hydroxide surplus with methyl dichloroacetate in methanol solution via neutralization of filtrate with 50 percentage sulfuric acid to pH 2～3 and hydrolyzation after separation of salts.

二氯乙酸甲酯和过量的氢氧化钠在甲醇溶液中反应，滤出氯化钠后，直接加入适量的 5 0 %的硫酸调 pH值为 2～ 3，滤出硫酸钠，蒸馏回收甲醇，水解、浓缩，得到不含乙二醛的 4 0 %乙醛酸溶液。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下：一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸；蒸馏NMP；干燥增溶剂；二、在氮气气氛下，Py与NMP混匀后加入密封的反应器中，再加入增溶剂，然后加入5-氨基-2-苯并唑，搅拌；三、在氮气气氛下，将步骤二的混合液搅拌并升温至50℃～150℃后加入脂肪族二酸，再加入TPP后缩聚；四、再倾入甲醇析出沉淀，过滤，清洗沉淀，再干燥；即得到含唑环半芳香聚酰胺。

The oxidation of benzyl alcohol produces benzoic acid and benzaldehyde selectively with the amounts of hydrogen peroxide varying.

苯甲醇氧化时，随过氧化氢加入量的不同，可以选择性地给出苯甲醛和苯甲酸。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。