前驱

Alumina sols of different content were prepared by using Al3 as precusor, water as solvent, nitric acid as peptizer, ethylacetoacetate and polyvinylpyrrolidone as modified menstruum. We used dip-coating method and spin-coating method prepared of alumina films on the plane glass and used dip-coating method and rising liquid method inside the wall of the fiber.

以仲丁醇铝为前驱物、水为溶剂、硝酸为胶溶剂、同时加入乙酰乙酸乙酯和聚乙烯吡咯烷酮作为改性剂制备了不同浓度的氧化铝溶胶用提拉法和旋覆法在平板玻璃上镀膜，同时用提拉法和液面上升法在石英毛细管内壁上镀膜。

The aim of this thesis is to prepare rutile TiO2 nanorods under the hydrothermal condition and to investigate the correlation between the preparation parameters and the photocatalytic activity of as-prepared TiO2 samples. The initial sols for TiO2 were prepared by the hydrolysis and condensation of Ti precursor, titanium n-butoxide 〔Ti4, TNB〕 in DI-water with hydrogen chloride as a peptizer.

中文摘要本研究的主要目的是制备以水热法制备金红石相二氧化钛奈米棒并探讨其制备条件与光催化活性的相关性，以四丁基氧化钛为前驱物，在盐酸的催化下，经由水热处理来合成金红石相的二氧化钛奈米粒，并藉由XRD鉴定其结晶相，TEM来观察其外观形貌及其颗粒大小，氮气吸附法来分析其比表面积。

The invention relates to a fabric nanometer following cleaning agent for obtaining TiO2/ZnO composite hydrosol, and relative production and cleaning method, wherein it uses butyl titanate and zinc acetate as predecessor, uses glacial acetic acid as catalyst and peptizer, uses water as solvent, uses absolute ethyl alcohol as the solvent of butyl titanate, and uses ethanolamine as deposit agent and supplies OH-, to be hydrolysed and polycondensated to form TiO2/ZnO composite hydrosol. And its components and mass percents are: butyl titanate at 1-15%; zinc diethyl at 1-12%; absolute ethyl alcohol at 1-20%; glacial acetic acid at 5-15%; and aminoethyl alcohol at 0.1-5%, and the left is water. The invention has lower cost and simple process.

本发明涉及一种可以得到TiO 2 /ZnO复合水溶胶的纺织品纳米后整理试剂及其制备工艺及对织物的整理方法，以钛酸丁酯和乙酸锌为前驱物，冰乙酸为催化剂和胶溶剂，水为溶剂，无水乙醇为钛酸丁酯的溶剂，乙醇胺为沉淀剂并提供OH -，经过水解、缩聚反应形成的TiO 2 /ZnO纳米溶胶整理剂，其组分和重量百分比含量如下：钛酸丁酯占1～15％；二水乙酸锌占1～12％；无水乙醇占1％～20％；冰乙酸占5％～15％；乙醇胺占0.1％～5％；水余量，具有耐洗性、无毒、无刺激、成本低廉、制作工艺简单可靠的优点，可实现对对织物的抗紫外、抗菌、抗静电功能整理。

Factors influencing TiO_2-PILC photocatalystic properties were discussed, including the ratio of CH3COOH and Ti, the temperature and aging time of pillaring agents, pH value of reaction solution, the temperature of calcined, etc.

以钛酸四丁酯为前驱物，冰醋酸为鳌合剂，重点考察了[CH3COOH]/比、柱化剂制备温度和陈化时间、催化剂煅烧温度等对TiO_2柱撑蒙脱土结构的影响。

The results indicate that the pillaring process and crystal growing of anatase can be more easily realized by increasing the acid-base ratio of pillaring agents, raising the pillaring temperature and adding proper quantities of alkali. The calcination of Ti-pillared precursor brings the growth of TiO2 grain, at the same time the layer distance is declined. In order to obtain ideal products, the right pillaring conditions are: the acid-base ratio of pillaring agents of 13, pillaring temperature of 65 ℃ and the volume of alkali (2 mol/L) in pillaring liquid of 6 mL.

结果表明：在一定范围内增大柱撑剂酸碱比、提高柱撑温度以及加入适量碱，有利于插层复合反应的进行和锐钛晶型的生长；柱撑前驱物焙烧后TiO2晶粒长大，同时焙烧引起的脱水导致膨润土层间距的下降；为获得较理想的产物，合适的柱化条件为：柱撑剂酸碱比 n n (HNO3)为13、柱撑温度65 ℃和柱撑液加碱量为(2 mol/L NaOH) 6 mL。

The essence of higher heating temperature for oxalate precursor is pockety La(superscript 3+) and Zr(superscript 4+).

草酸盐前驱体中镧和锆两种成分局部的分布不均匀是造成其处理温度比氨水法要高的直接原因。

Based on the technique from micrometer particle dispersion, superfine particle dispersion behavior and its effect on polymere.

结合微米分散技术基础，对超微颗粒在聚合物固体中分散及其结晶研究的进展深入探讨，揭示了聚合物基-纳米复合材料的颗粒分散经过纳米前驱物中间阶段，再进行聚合复合与熔体复合，得到颗粒均匀的分散体系。

Through replacing copper Tri-fluoroacetate by copper α-methacrylic in Metal Organic Deposition process, the total amount of fluorine in YBCO precursor solution was reduced by about 50%. As a result, the calcination period for YBCO precurse film was dramatically reduced.

在金属有机盐沉积法制备YBCO薄膜的工艺中，采用无F的α甲基丙烯酸铜取代原来的三氟乙酸铜，可以降低前驱溶液中大约50%的氟含量。

It is worth noting that some things that you may think are triggers, may have been a craving in the prodromal phase.

值得注意的是，有些东西你可能会认为是触发，可能已成为渴求，在前驱阶段。

Objective To probe the prodromal symptoms in schizophrenia.

目的 调查与分析精神分裂症患者的前驱症状。

I will endeavour to find you some assistance.

我尽力帮你找人帮忙。

At first I only know bruck is the idol of American younglings, afterwards I returned back to Taiwan ,even in Beijing last year ,I saw her poster everywhere, I was so surprised at her charm.

起初我只晓得布鲁克雷德丝是美国少男少女崇拜的偶像，后来回台湾，甚至去年在北京，居然也四处看见她的海报，才惊讶她的魅力之大。