制备

The preparation methods of ultrafine alkaline earth aluminate and its properties were reviewed in this paper.

对超细碱土铝酸盐长余辉发光材料的制备方法及其制备后产品的性能做一综述，分别介绍了燃烧法、溶胶-凝胶法和水热法在制备超细碱土铝酸盐长余辉发光材料中的应用。

Molybdenum-glycol complexes synthesized with different alkylene glycols and Mo/alcohol ratios have different acidity and catalytic activity. For the topic reaction, the catalytic activity of Mo-1, 2-ethandiol or Mo-1, 2-propanediol is higher than that of Mo-butanediol.

结果表明，用不同的二醇和不同醇／钼比制备的钼醇催化剂具有不同的催化性能和酸性，用乙二醇和丙二醇制备的催化剂，催化性能优于丁二醇制备的催化剂。

Quinclorac and allyl alcohol as raw materials, 3, 7-dichloro-8-quinolinoxylic acid allyl ester was obtained when catalyst is oil of vitriol or super solid acid SO〓/TiO〓. Using both catalysts, organic synthesis technology process was made respectively, and the ester was analyzed and characterized by IR spectrum and NMR spectrum Through experiment, both preparing conditions were optimized and discussed respectively.

以TiO〓为载体负载SO〓制备出固体超强酸催化剂，确定了SO〓/TiO〓催化剂制备的技术路线，以丙酸正丁酯为探针实验，考察了新型固体酸催化剂SO〓/TiO〓的催化活性及制备条件对催化活性的影响，对影响其催化效果的工艺条件进行了优化，并探讨了影响的规律性。

The result shows that the activator which was made up of organic acid and organic amine complex satisfied the prospective demand.

结果表明：采用有机酸和有机胺复配制备的活性物质满足预期要求；复配溶剂满足沸点、黏度和极性基团三大原则；所制备的免清洗焊剂多项性能满足规范要求，达到了免清洗的要求，解决了助焊性与腐蚀性的矛盾；所制备的焊膏焊接性能良好，无腐蚀，固体残留量低，存储寿命较长。

The mechanical property testing shows that the seamless PLLA tubes perform excellent radial strength,which indicates that the mechanical properties of biodegradable stents made of these tubes was supposed to be excellent.PLLA and its composites were first used in preparing seamless tubes as antecedency of laser-cut biodegradable coronary stents in china.Finite element analyses of the biodegradable coronary stent model indicate the explorative design basically meets the requirement of reasonable and applicable stents.There is not such kind of research yet in domestic.Optimum laser-cuttting parameters of CO2 laser was cauculated based on experiential formula,within it,biodegradable coronary stents,especially those with complex structure would be manufacutured from seamless tubes quickly by laser microprocessing with high consistency to the design model.The processing efficiency of the CO2 laser demonstrated in experiential formula by us will play an important guiding role in manufacturing biodegradable stents by laser-processing.Our stents that ascribed to laser-cutted,slotted tube stent are proved to be biodegradable, self-expandable and good biocompatible,basically reach the international level on the aspest of manufacturing procedures and design.

研究结果表明：壳聚糖改性材料综合性能优于纯PLLA，更适合于作为可降解冠脉支架的原材料；自主设计的探索性自膨胀管状闭环型可降解冠脉支架的性能符合冠脉设计要求，设计、验证生物可降解冠脉支架模型的研究在国内还未见报道；制备的改性PLLA无缝管的力学性能优越，可通过激光切割获得冠脉支架，这是国内首次采用聚乳酸材料来制备通过激光加工出可降解冠脉支架的无缝管；二氧化碳激光器加工精度能达到加工要求，加工出来的血管支架名义设计与实测值误差小，实现了冠脉支架、尤其是带有复杂外观设计冠脉支架的快速化、规范化加工，对二氧化碳激光器加工聚乳酸材料的效果研究在国内外属于首创，获得的经验公式对日后的深入研究有重要的指导意义；制备的支架为激光切割管状闭环型冠脉支架，支架外观设计、支架加工手段、支架的性能都基本接近国际水平，支架样品符合设计的理念，可以实现自膨胀功能。

Thinking of presenting problems, this research mainly studied some solid base catalysts which own higher catalysis ability and longer lifetime. Then, the phase diagram and equilibrium data of oil-alcohol-biodiesel-glycerol multiphase system were measured because the biodiesel producing process lacks of thermodynamic data.Based on a double-membranes theory and the thermodynamic data, a kinetic model was proposed. In addition, a mult-step extraction process was proposed to dispose the jatropha curcas l oil with high acid value in order to decrease the acid value. Then, a new technology of biodiesel producing using solid base as a catalyst was developed. The study objects and results are as follows.

本研究针对负载型固体碱催化剂活性组分易流失、使用寿命短的缺点，制备了高效、稳定的固体碱催化剂；针对生物柴油制备体系热力学数据缺乏的问题，测定了大豆油-醇-生物柴油-甘油体系的相图和平衡特性，在此基础上基于双膜理论，建立了固体碱制备生物柴油的动力学模型；同时针对酸价较高的麻疯果油，提出了先用甲醇或乙醇多级萃取降低酸价，再用固体碱催化制备的新工艺。

Two new methods about preparation of nano-inorganic coated polymer microsphere have been found. The research mainly focused on controlled precipitation of inorganic precurdors onto the polymer microspheres, technique of preparation and size distribution of transition metal oxides and sulfides emulsion particles, nano-paticles''surface modification and the HLB values adjustment, emulsification of oil-soluble monomer in inorganic colloid and emulsion stability, emulsion polymerization that inorganic particles act as medi-phase, the preparation of inorganic nano-particle/polymer hybrid microspheres, preparation of hybrid materials in inverse emulsion, inverse emulsion polymerization of acrylamide and its phase behavior. Inorganic nano-particles we studied concerning TiO2、SiO2、Fe3O4、ZnO、ZnS、Ag and black carbon. Also we studied the morphology and capability of the hybrid materials.

主要内容有：无机物在高分子乳胶模板体系的界面定位沉积研究；过渡金属氧化物、硫化物纳米胶体粒子的制备工艺与胶粒尺寸分布研究；纳米粒子的表面修饰及其亲水亲油平衡值的调制；油溶性单体在无机胶体中的乳化行为与乳液稳定性研究；以无机纳米粒子做中介相的乳液聚合与无机纳米粒子/高分子复合微球制备研究；反相体系中杂化材料的制备；丙烯酰胺水溶液反相乳液聚合、相行为与稳定性；丙烯酰胺反相体系中无机粒子的制备研究；涉及到TiO2、SiO2、Fe3O4、ZnO、ZnS、Ag、碳黑等纳米无机物，系统考察了相关材料的形态与性能，为其应用开发奠定了基础。

The differences of the micro structure and properities of the bulk sinters, between the fabrication methed of powder metallurgy and reactive synthesis for silver tin oxide composite, are studied in prensent thesis. With the increase of the tin oxide content in silver matix, the electric conductivity of the composite tended to decreace. While in the same tin oxide content, the electric conductivty of the composite fabricated by reactive synthesisis better than that by powder metallurgy. One of the reasons is that the regular net structure existing in former composite.

研究了两种方法即粉末冶金法和反应合成法制备的银氧化锡复合材料烧结坯在组织上的区别和性能上的差异，两种方法制备的银氧化锡复合材料，随着氧化锡含量的升高，材料导电性均呈下降趋势，而相同成分的材料，反应合成法制备的银氧化锡复合材料的烧结坯的导电性要优于粉末冶金法，有规则的网络状组织结构是反应合成法制备的烧结坯导电性好的原因之一。

Through the methods of sol-gel, hydrothermal reaction and forced hydrolysis, iron oxide particles with cubic, spherical, spindle and acicular shape were prepared with adding different regulators of crystal growth, such as NaH2PO4, HEDP. And through the methods of complexing-precipitate and precipitate, copper oxide and power blue were prepared respectively.

通过水热法、溶胶-凝胶法分别制备出了纳米球形和立方形Fe_2O_3；采用强迫水解法，通过添加晶型控制剂NaH_2PO_4、HEDP分别制备出了纳米纺缍形和针形Fe_2O_3，通过络合沉淀法制备出纳米球形CuO，通过沉淀法制备出纳米Co_2O_3。

Pneumophila serogroup 5 antibody to develop two immuo-colloidal gold tests respectively. Main works listed below as:1、Preparation and identification of polysaccharide antigen of L. pneumophila Bacteria of LP1 ~ 7,9 and 10 were cultured on yeast agar buffer activated carbon for three to five days at 37℃, 5%CO2. Protein-free polysaccharide antigens were obtained after harvest in cells, extraction, deproteinization, dialysis and other steps. Their immunogenicities were verified by ultraviolet spectrophotometer full-wavelength scanning and Western blotting.2、Preparation and identification of rabbit anti-LP1 antibodies and rabbit anti-LP5 antibody Rabbit anti-LP1 and anti-LP5 antibodies were purified after rabbits were immuned with antigens isolated as described above. The purities of both antibodies were above 80% and the titer of blood serum 1:32 tested by double antibody sandwich assay.3、Development of colloidal gold immunochromatographic assay kit The size of colloidal gold particles in the kit was 25nm. The optimal concentrations for antibodies were 30μg/ml and the sensitized concentrations of NC membrane were 5 mg/ml.

主要研究工作从以下几个方面进行：1、LP1~7、9和10型多糖抗原的制备与鉴定将LP1~7、9和10型菌株分别接种在缓冲活性炭酵母琼脂培养基上，37℃、5%CO2的条件下培养，3~5天后洗下菌苔，经抽提、除蛋白、透析等步骤后得到基本无蛋白的LP多糖抗原，经紫外分光光度仪全波长扫描及Western blotting验证其抗原良好。2、兔抗LP1抗体和兔抗LP5抗体的制备与鉴定分别用LP1、LP5型多糖抗原免疫家兔，采用琼脂糖双向扩散试验检测，两种抗体血清效价均为1：32；饱和硫酸铵法提取抗体，SDS-PAGE检定其抗体纯度均达到80%以上。3、胶体金免疫层析检测试剂的初步研制采用柠檬酸三钠还原法制备约25nm大小的胶体金颗粒；分别制备兔抗LP1抗体、兔抗LP5抗体的金标探针，两种抗体的最适标记量均为30μg/ml；选择适当孔径的微孔滤膜为载体包被两种抗体，NC膜包被浓度均为5mg/ml。

Plunder melds and run with this jewel!

掠夺melds和运行与此宝石！

My dream is to be a crazy growing tree and extend at the edge between the city and the forest.

此刻，也许正是在通往天国的路上，我体验着这白色的晕旋。