制备

Several methods for the preparation of mesoporous carbons are reviewed in this paper.

综述了中孔炭材料的制备方法，详细介绍了近年来新兴的模板法制备中孔炭材料在国际上的研究进展，并评述了中孔炭材料制备方法的优缺点。

According to the present situation of Hebei province, chitin was extracted from waste crab shells of Qing Huangdao, and then chitosan was prepared. On the base of those, a series of chitin/chitosan derivatives were synthesized and characterized. Finally,~then they were applied in fruit preservative, flocculation and cosmetics. The main results ~re summerized as follows:(1) Chitosans with low, middle and high viscosity have been prepared from chitin, which was extracted from waste material of crab shells produc ed in Qing HuangDao.

并对针对河北省的资源情况，从秦皇岛蟹壳废料中提取甲壳素，制备壳聚糖，在此基础上制备了一系列甲壳素/壳聚糖的衍生物，对其结构与性能进行深入的研究，并开发其在食品保鲜、污水处理、化妆品等方面的应用，具体分述如下：（1）以所提取的甲壳素为原料，在浓碱溶液中通过正交实验法对壳聚糖的制取条件进行优化，确立制备低、中、高三种粘度壳聚糖的最佳条件。

Two types of haptens, the earboxylated propyl amino derivative of the acid moiety (HCA1) that is the hydrolyzed product of cyhalothrin, and the carboxylated ethyl carbonyl derivative of the alcohol moiety (HCB2) were synthesized, and conjugated with the carrier proteins bovine serum albumin and ovalbumin respectively by the active ester method and the mixed anhydride method. The polyclonal antibodies were obtained after immuning to the New Zealand rabbits.

通过对氯氟氰菊酯分子结构中的酸部分接4-氨基丁酸(HCA1)和醇部分接丁二酸酐(HCB2)，合成两种不同的半抗原，并通过碳二亚胺法将HCA1和HCB2分别与牛血清蛋白偶联制备了人工抗原HCA1-BSA和HCB2-BSA，通过活泼酯法将HCA1、HCAS和HCB2分别与卵清蛋白偶联制备包被抗原，两种人工抗原通过免疫新西兰大白兔来制备相应的多克隆抗体。

In this paper,the SMO-type lithium ion sieve was the main research object,the manganates and lithium salts were taken as the main raw materials.Two LISs with high uptake capacity,better selectivity and stable structure were successfully prepared by hydrothermal method and coprecipitation method based on the discussion of correlation between Li+ uptake performance and the preparation conditions of LIS precursors.The effects of preparation conditions on Li+ uptake were also investigated.

本文以SMO型锂离子筛为研究对象，以锰盐和锂盐为主要原料，在采用固相法探讨离子筛前驱体制备条件与离子筛提锂性能关系的基础上，分别采用水热法、共沉淀法为主要合成方法，成功制备了具有高提锂容量、选择性好及结构稳定的两种锂离子筛材料，并研究了合成条件对材料制备及提锂性能的影响。

The sixth, there were no significantly differences between colchicine groupsand vinblastine groups on the metaphases, in the experiment of prepare mouse4-cell embryo stage single blastomere chromosome specimen by using optimumparameters; and there were significantly differences between colchicine groupsand vinblastine groups on the metaphases (P＜0.05), in the experiment of preparemouse 8-cell embryo stage single blastomere chromosome specimen by usingoptimum parameters.The end, the preparation quality of mouse 4-and 8-cell embryo stage singleblastomere specimen were 2.5, 2.7, 2.4, 1.9, respectively.

低渗液选用0.45％氯化钠时，低渗效果优于选用0.5％柠檬酸钠和0.35％氯化钾的。6、在利用最佳参数制备小鼠4-细胞期胚胎单卵裂球染色体标本时，经统计分析，两种阻断剂的作用效果差异不显著；而在制备小鼠8-细胞期胚胎单卵裂球染色体时阻断剂选用长春花碱的效果优于秋水仙素的(P＜0.05)。7、秋水仙素组和长春花碱组小鼠4、8-细胞胚胎单卵裂球染色体标本制备质量分别为：2.5、2.7、2.4、1.9。

In this work, nanostructure samples of La1-xCaxMnO3（x=0.2、0.3、0.4、0.5）were prepared by hydrothermal-precipitation method . The structural characterization of the powder samples were done by X-ray diffraction. XRD patterns showed that all the samples ate single perovskite-type phase withoutother impurity or secondary phase. The shape and size of samples were performed on Scanning Electron Microscopy. SEM photographs investigated that temperature of hydrothermal effects the phase of samples and alkalinity of the reaction mixture by ΔTad-T curve measurement device at low magnetic fielded

本论文采用水热共沉淀退火法制备了La1-xCaxMnO3（x=0.2、0.3、0.4、0.5）系纳米结构，用X射线衍射仪确定产物为单相钙钛矿结构，无任何杂峰及第二相；用扫描电子显微镜与透射电子显微镜分析了产物的大小和形貌，发现水热温度对产物的形成起决定作用，随着温度的升高，产物由薄膜状向丝状转变，而溶液的碱度可控制产物的形貌和大小，当碱度为6.35mol/L，水热温度为240 C时，La0.6Ca0.4MnO3的主要形貌为纳米丝并有少量纳米颗粒，纳米丝平均直径为40nm；最后测量了粉末样品在低磁场（1.4T）下的磁热效应，发现水热共沉淀退火法制备样品的最大绝热温度明显高于球磨法制备样品的最大绝热温变。

The mainly conclusions in our research are as flowing: tungsten trioxide powders with 100 nm primary particle are obtained by spray drying,calcination and wet milling process, and an average size of quadric particle composed of agglomerated particles is 0.64 μm; tungtsen powders with 39 nm grain size and 60 -100 nm primary particle are produced directly from previous tungsten trioxide using one step reduction in hydrogen at 700℃, and an average size of quadric particle of tungsten powder is 2.91 μm; tungsten trioxide and copper tungstate compound powders with 100 nm - 200 nm primary particle are produced using ammonia metatungsten and copper nitrate as raw materials by spray drying,calcination and wet milling process;the compound powders are transformed completely into tungsten and copper compound powders by reduction in hydrogen at 700℃,in which tungsten grain size is 59 nm and copper grain size is 51 nm; primary particle size of compound powders is 80 - 120 nm,and an average size of agglomerated quadric particle is 1.86 μm; tungsten nitride powders with 35 nm grain size are prepared from tungsten trioxide powders by nitrogen treatment thoroughly in pure ammonia at 650℃, and an average size of agglomerated quadric particle is 0.64 μm in normal temperature.

研究结果表明：采用喷雾干燥—焙烧—球磨工艺可以制备出粒度约为100nm的WO_3粉体，它们在团聚后形成的二次颗粒平均粒度为0.64μm；采用一步直接氢还原方法可在700℃下从上述WO_3粉体制备出晶粒尺寸为39nm的、一次颗粒粒度为60-100nm的W粉体，其二次颗粒的平均粒度为2.91μm；以偏钨酸铵、硝酸铜为原料，采用喷雾干燥—焙烧—球磨工艺可制备出一次粒度为100-200nm的WO_3和CuWO_4混合粉体；采用氢还原工艺可在700℃下将这种粉体完全转变为W、Cu复合粉体，其中W的平均晶粒粒尺寸为59nm，Cu的平均晶粒尺寸为51nm；复合粉体的一次颗粒尺寸为80-120nm，在常温下团聚后形成的二次平均粒度为1.86μm；采用纯氨氮化工艺可以在650℃下由WO_3粉体制得WN，其晶粒尺度为35nm，在常温下团聚后的二次平均粒度为6.4μm。

A process for preparing superthin film of polyaniline, which can be used for chemical sensors, electrochromic device, luminous device, chemical modifying electrode and polymer FETs, uses intrinsic polyaniline solution and polymer acid as raw materials, which take part in doping reaction to prepare said film.

本发明公开了一种掺杂诱导沉积聚苯胺自组装超薄膜的制备方法，属超薄膜制备技术领域。它采用本征聚苯胺溶液及聚合物酸为原料，基于本征聚苯胺与聚合物酸的掺杂反应制备聚苯胺超薄膜。

In order to study the influence of preparation techniques on stability of different morphological silver colloid s, stable silver colloid s were produced by the reduction of AgNO3 with the protection of polyvinylpyrroli-done using KBH4 and N2H4 ----------- H2O as reductants.

为了研究制备工艺条件对不同形貌银胶体稳定性的影响，在超声场作用下，以AgNO3为前驱物，聚乙烯吡咯烷酮为保护剂，KBH4和N2H4·H2O分别为还原剂，制备了稳定的银胶体，并利用透射电镜和分光光度技术对制备的银胶体进行了表征。

The results show that: the tensile strength, flexural strength and flexural modulus increase by about 10.4%, 62.1% and 122.3% respectively when the mass fraction of the aluminum powder increases from 0 to 50%, while elongation at break and impact strength decrease by about 65.0 and 74.4% respectively; the tensile strength, elongation at break and impact strength all increase with decreasing the particle sizes of the aluminum powders.b Nylon-12 coated metal powders for the indirect SLS process were prepared by the dissolution precipitation process. The coated powders have only 1.0 wt% nylon-12, and their SLS green parts have sufficient strength for features as small as 1.0 mm to be built and post-processed and high dimensional accuracy. The green parts were subjected to the post processing processes including binder decomposition and infiltration of epoxy resin, and then the metal/polymer composite parts with relatively high strength and accuracy were formed.At present, micron-scale inorganic fillers have been widely used to reinforce nylon SLS parts.

将该法制备的尼龙12覆膜金属粉末用于以下两个方面：a使用铝粉增强尼龙12的SLS成形件，通过溶剂沉淀法制备尼龙12覆膜铝复合粉末，研究了铝粉含量及粒径对SLS成形件性能的影响，结果表明：铝粉分散均匀，并与基体有良好的界面粘接；当铝粉含量从0增加到50wt％时，成形件的拉伸强度、弯曲强度、弯曲模量分别提高10.4％、62.1％和122.3％，冲击强度和断裂伸长率下降65.0％和74.4％，耐热性及尺寸精度也得到提高；断裂伸长率、冲击强度及拉伸强度均随着铝粉粒径的减小而增大。b使用溶剂沉淀法制备了间接法SLS用尼龙12覆膜金属粉末，该覆膜粉末中聚合物粘接剂的含量仅为1.0 wt％，其SLS初始形坯具有较高的精度以及足够满足后处理要求的强度，最小精细结构的尺寸达1.0 mm。

James, son of Zebedee, and John the brother of James, whom he named Boanerges, that is, sons of thunder

载伯德的儿子雅各伯和雅各伯的弟弟若望，并为他们起名叫"波纳尔革"，就是"雷霆之子"

The southern Hungarian university city of Szeged will host part of the project, amounting to 40 percent of the total investment, which will mostly be paid for through Hungary's EU structural funds.

位于塞格德南部的匈牙利大学将负责部分项目，总计占总投入资金的40%。大部分资金将由匈牙利的欧盟结构基金会支付。