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The chloroform layer and the aqueous layer were separated by multiple column chromatography including macroporous resin, silica gel and polyamide column and preparative HPLC. The compounds obtained were identified by mass spectra and NMR data.

大青叶乙醇提取物,用氯仿萃取后得到氯仿层和水层,各层再分别采用硅胶柱、大孔树脂柱、聚酰胺柱、制备液相、葡聚糖凝胶柱层析及重结晶等分离手段进行分离、纯化,并应用化学性质和质谱、波谱法(1H-NMR、13C-NMR、HMBC)鉴定其化学结构。

Glucose, formic acid and levulinic acid were not detected in the liquors of acid hydrolysis and the concentration of xylose and arabinose was high, while the acetic acid was low. The mixture of monosaccharides and fatty acid was efficiently separated and the whole process of separation was finished within 23 minutes.

通过对样品的分析表明,麦糟水解液中不含有葡萄糖、甲酸及乙酰丙酸,木糖和阿拉伯糖的质量浓度比较高,乙酸的质量浓度比较低,单糖及脂肪酸的混合液得到很好的分离分离过程在23min内完成。

For an arbitrary system of steady-flow and constant volume reactors, the concept of theattainable region is extended by the consideration of the recycle material from separation.

本文从化工过程系统综合优化的角度出发,以定态、等容反应过程为研究对象,在可得区内考虑分离回收的循环物流,通过几何方法分析总收率等值线与可得区的关系,导出了通用的反应-分离循环系统的最佳工艺条件方程。

Based on major and trace elements and isotope geochemical data, it is inferred that Sandouding suite is formed by magma melting of Late Archeozoic continent tholeiite source, and its geochemical variation is controlled by hornblende fractional crystallization. Besides fractional crystallization, the geochemical variation of Huanglingmiao suite is related to the mixing between dacitic magma and felsic magma. Dalaoling suite is probably derived from early Precambrian volcanics.

根据岩石化学和同位素组成推断,三斗坪岩套的源岩主要是晚太古代大陆拉斑玄武岩,母岩浆相当于英安质,岩套内的成分变化主要受角闪石分离结晶作用控制;黄陵庙岩套除受分离结晶作用影响外,成分变化主要与英安质母岩浆和某种长英质岩浆的混合有关;大老岭岩套的源岩亦为早前寒武纪火山岩。

Based on the Reynolds stress model CFD numerical simulation method, the experimental study of the inflow field and separation feature of nine forms of entrance structures of the oil-water separation hydrocyclone including vortex curved entrance and Archimedes spiral entrance is carried out and four kinds of ideal optimized entrance structures are obtained.

采用雷诺应力模型CFD数值模拟方法,对涡线形曲面入口、阿基米德螺旋线形入口等9种油水旋流分离器入口结构形式的内流场和分离特性进行了试验研究,得出比较理想的4种优化入口结构形式。

According to this, a new structure-the oil-water cyclone separator with the spatial Archimedes spiral cord imported flow channel and conduction current spiral-is proposed.

研究表明,采出液在进口处的相互流动干扰对油水分离效果有重要影响,据此提出一种新型结构-带有空间阿基米德螺旋线进口流道和导流螺旋的油水旋流分离器。

The test results have shown that the combined depressants are distinctively effective to depress arsenopyrite and activate galena,stibnite and chalcopyrite to certain extent.

在此基础上,选择了湖南省瑶岗仙钨矿精选工段含砷高达26%的硫化矿为对象,进行天然矿石的铜-砷分离试验,获得了极好的分离效果。

The fragment size can be amplified by 295 bp through the primer, in order to prevent false positive from appearing, a pair of internal control primers C34 is designed through the invention according to a bull autosome 3 reported sequence, the fragment size is amplified by 208bp, dual PCR amplification is performed to single bull sperm through the two pairs of primers, and then the final evaluation is performed to the sperm separation purity according to the statistical analysis to the detection result.

本发明提供了一种检测X、Y精子分离纯度的引物,该引物是针对牛Y染色体上性别决定基因Sry通过PCR错配技术设计而成,通过该引物可扩增片段大小为295bp,为了防止假阳性出现,本发明根据牛3号常染色体报道序列设计了一对内标引物C34,扩增片段大小为208bp,通过上述两对引物对单个牛精子进行双重PCR扩增,然后根据对检测结果的统计分析,对分离精子纯度做出最终评价。

A new method to separate azeotropic mixtures was proposed in the paper, that is, vacuum volatilization separation process. It is undertaken in vacuum and the temperature must be controlled under the azeotropic point to avoid forming of azeotrope.

该过程在真空下操作,控制系统温度低于共沸点,使两组分在分离过程中不形成共沸物,而依靠组分间挥发速度及扩散速度的差异,来突破共沸限制,达到分离目的。

In the end, the extractive distillation method was applied to separate and purify the binary azeotrope mixture, methanol-dimethyl carbonate. The isoamyl acetate was used as extractant and the two tower system was introduced to continuous extractive distillation operation. The results show a better separation effect.

最后采用萃取精馏的方法,对甲醇-碳酸二甲酯的二元共沸混合物进行了分离提纯研究,以毒性较低的乙酸异戊酯为萃取剂,采用两塔连续萃取精馏操作,结果表明,分离效果比较理想。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。