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The main product was 4-oxo-β-ionone with a yield of 50.2% and a purity over 98.5% under O2 pressure(1MPa) at 75℃ with additive pyridine over catalyst CuL^2 in 10h.

以CuL^2作催化剂,当反应时间为10h、反应温度为75℃、催化剂用量为1.6%、O2气压力为1MPa、添加摩尔分数为30%吡啶时,4-氧代-β-紫罗兰酮的收率为50.2%,纯度超过98.5%。

However, it is limited for IQ result to tell us.

但是,IQ分数所能告诉我们的是有限的。

This paper quantitatively analyzed the distribution of graphite in inoculated gray iron by image analysis.

作者利用图像分析技术,定量分析了灰铸铁孕育处理后石墨相的分布情况,发现石墨相体积分数与灰铸铁综合性能有较为一致的关系,确定了孕育处理时使用孕育剂的最佳方案。

Results The tiopronin in situ gel of 0.2 % sodium hyaluronate had proper gelating temperature and certain sustained releasing ability, Papp and retention time of which was 15.43 cm·s-1 and 130 min respectively, irritancy and stability were up to standard of ophthalmic preparation.

结果 含有质量分数0.2 %透明质酸钠的硫普罗宁原位凝胶具有适宜的胶凝温度和一定的缓释作用,其角膜表观透过系数为15.43 cm·s-1,角膜前滞留时间为130 min;刺激性、稳定性符合眼用制剂要求。

On the basis of color imaging system, an automated photoelasticity in white light for determining isochromatics and isoclinics is presented It includes two techniques One is automation of the ordering of color isochromatics based on BP neural network The other is whole field digital determining of isoclinic angles by five step color phase shifting Many limitations and drawbacks, which affect the precision of measurement, were more eliminated and improved The validity of experimental results was ...

以彩色信息图象处理技术为基础,围绕光弹性实验数据自动采集这个主题,提出用BP神经网络自动确定等色线分数级条纹及其级数的颜色插值法,以及全场数字化确定等倾角的五步彩色相移法。典型实验表明,上述方法在提高光弹性数据采集自动化程度和减少各种误差因素影响等方面均有所改善;进而提高三维光弹性薄切片应力分析结果的精度,促进实验应力分析的工程应用,扩大光弹性法的应用范围。

The osmotic coefficients and saturated vapor pressures have been calculated at the different temperatures .The experimental values of the osmotic coefficients for the Li_2SO_4-H_2O system were consistent with the values in the references. The results revealed the rules of the changing in osmotic coefficients and saturated vapor pressures with ion strengths and the molality fractions of Li_2B_4O_7 at different temperatures. The isopiestic equilibrium molalities were correlated by using the modified and the extended Zdanovskii rules for non-ideal mixtures, and obey well the Zdanovskii rules. The ion interaction parameters of Pitzer model have been determined by using the two methods for Li_2SO_4-Li_2B_4O_7-H_2O at 298.15K system.

本文计算了不同温度下该纯盐体系和混合盐体系的渗透系数和饱和蒸汽压,并将298.15K下的纯盐溶液渗透系数的实验值与文献值进行比较,取得了相一致的结果;揭示了不同温度下渗透系数和饱和蒸汽压随离子强度及Li_2B_4O_7质量摩尔浓度分数yb的变化规律;本文用Zdanovskii规则修正式和扩展式关联了298.15K下该混合盐体系的等压平衡浓度之间的关系,计算结果表明用这两个方程可以描述该体系在全浓度范围内的等压平衡浓度间的关系。

Standard thermodynamic functions of transfer of naphthalene from water to H 2O isopropyl alcohol mixtures have been determined.

研究了萘从水到H2O-异丙醇混合溶剂中的迁移变化,表明萘的迁移随异丙醇摩尔分数x的增加呈复杂的下降趋势。

This project also obtained several limit theorems for some important dependent random variables and stochastic processes, such as the Strassen law of the iterated logarithm for negatively dependent random variables, strong limit theorems for mixing random vectors in Banach spaces, sample path properties for two-parameter fractional Wiener processes, and so on.

随机环境中的随机变量与随机过程的研究在国内外相当活跃,本项目主要研究它们的极限性质,着重研究了随机风景中随机变量与随机过程的极限性质,主要取得了以下几个结果:首先对简单对称的Kesten-Spitzer随机游动在低阶矩的条件下给出了强逼近,大大减弱了前人要求任意阶矩的条件,然后对独立风景中的一般随机变量给出了强逼近的一般性结果,由此导出在风景和随机变量都只具有低阶矩的条件下的独立但不同分布、混合相依变量的强逼近,在只有弱高于二阶矩的条件下得到了重相对数律和弱收敛;给出了连续时间参数的Brown风景中Brown运动和稳定风景中稳定过程的滞后增量和连续模等精确样本轨道性质;同时给出了一些重要的相依随机变量和过程的若干极限定理,如负相关随机变量的Strassen重对数律、抽象空间上混合相依变量的一些强极限定理成立的充分必要条件、两参数分数Wiener过程的样本轨道性质等。

So,the method for testing the content of wax in jadeite jade is quite important.

因此,测定翡翠中蜡的质量分数成为了其鉴定的重点。

Methods TLC-scanning method was adopted for the determination of Ber and Jat in HLD. Ber Jat was made artificially according to the result of the TLC-scanning.

方法采用薄层扫描法测定HLD中Ber和Jat的质量分数,并根据其比值配制模拟方。

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Do you know, i need you to come back

你知道吗,我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。