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In this thesis, multi-wall carbon nanotubeswas worked as a modified agent. The working electrode was a glassy carbon electrode or graphite electrode. A saturated calomel electrode and a platinum electrode were used as the reference and the auxiliary electrode respectively. Some pharmaceutics'electro-chemical behavior has been studied with great details. The main researches were summarized as follows: The acid-treated CNT was successfully dispersed into the DMF by using ultrasound technology.

本论文以多壁碳纳米管为修饰剂,以玻碳电极和石墨电极为工作电极,铂丝电极为对电极,饱和甘汞电极为参比电极,研究了几种药物的电化学行为及其检测方法,取得了以下研究结果:以N,N-二甲基甲酰胺为分散介质,将酸化后的MWNT超声分散于DMF中,获得分散液。

The Scheutjens - Fleer model on monodisperse polymer adsorption was extended to the situation of polydisperse polymer adsorption by the method of seeking the extremum of the partition function constructed for the system.

采用构作配分函数而后求极值的方法,将Scheutjens-Fleer模型推广到多分散高分子吸附情形,并采用适当的计算方法,解决了长期以来人们难以解决的多分散高分子模型计算上的困难,研究了固液界面区域多分散高分子的微观吸附行为、多分散指数对吸附层性质的影响以及各种微观构象的链段大小的几率分布。

With the treatment of silicone coupling on the surface of nano-Al2O3 particles and the action of mechanical decentralization and ultrasonic wave, the particles were dispersed in the matrix of epoxy resin.

采用对纳米颗粒表面进行硅烷偶联处理和机械分散与超声波振动分散相结合的方法,实现了氧化铝纳米粒子在环氧树脂中的分散。

Firstly, the mechanism of the preparation of superfine quartz powder with ball mill is studied in this article, based on nature of quartz material, Griffiths strength theory and the crush theory of planetary ball mill. The problem of granulation during the process of the preparation of superfine quartz powder is studied minutely. And proposed increasing dispersant and disperser medium to restrain granulation, and dispersing use ultrasonic after milled.

首先,本文结合石英材料的基本物性,以格里菲斯强度理论和行星式球磨机的粉碎原理为基础,研究了球磨法制备超细石英粉体的机理,同时对粉石英制备过程中的团聚问题及其控制作了细致的研究,提出粉磨过程中增加分散剂和分散介质来抑制团聚,粉磨后采用超声法进行分散,并确定了最佳分散剂、分散介质的用量和最佳超声分散时间。

The dispersion mechanism of the dispersants was analyzed by testing the Zeta potential of the dispersion phase in the dispersion medium. It was shown that Ⅰ and Ⅱ raised obviously the absolute values of surface Zeta potential of titania particles, and NK-1 formed good solvate layers of the particles so that the nano-titania particles were stably dispersed in the water solns.

通过测定分散相在分散递质中的Zeta电位,分析了分散剂的分散机理,说明六偏磷酸钠和硅酸钠可显著提高整理液中二氧化钛颗粒表面Zeta电位的绝对值,NK-1在纳米二氧化钛颗粒表面形成良好的溶剂化层,使纳米二氧化钛颗粒在水溶液中获得优良的分散稳定性。

In chapter three, various theories and experience on the dispersion of nano-powders proposed by former researchers were generalized and reviewed. Technical standards and experimental process for determining technological parameters were suggested for the dispersion of nano-scaled metal oxides in aqueous medium according to their surface wettability, surface charge, the dependence of surface charge on pH and the compatibility of surfactants with pH and pH adjusting agents. Based on these suggested standards and experimental method, highly stable and dispersive aqueous suspensoid of nm-ZnO, nm-TiO〓, nm-Co〓O〓 and nm-MnO powders were prepared successfully and surface modification on these nano-powders was also achieved.

本文第三章通过大量的文献调研,归纳总结了前人在纳米粒子分散技术方面的理论和经验,并在此基础上根据纳米氧化物粉体的表面润湿性、表面电性及其与分散介质pH值的关系、表面活性剂及其与pH调节剂的配伍关系设计了纳米氧化物水分散体系的工艺规范以及确定工艺参数的通用实验步骤,成功地制备了纳米氧化锌、纳米二氧化钛、纳米氧化钴和纳米氧化锰的高稳定分散悬浮液并实现了干粉体的表面改性,为纳米材料在氧化锌压敏电阻中的应用创造了第二个前提条件。

Based on this result, a new technology is suggested, that is by regulating the effective sulphonating contents of 1-amino-anthraquinone, adjusting the concentration of sulfuric acid to hydrolyze 1-amino-anthraquinone disulfonic acid conversing to 1-amino-anthraquinone -2-sulfonic acid, and briminating the hydrolyzed product in 100% sulfuric acid, 87% yield of Bromamino-acid was achieved, 10% higher than the conventional method prepared by "oleum method".

此新工艺,溴氨酸在产物中含量可达87%,比常规的发烟硫酸法生产溴氨酸提高了10%,质量和收率都接近或达到溶剂法生产的水平。 1,5-二硝基蒽醌和1,8-二硝基蒽醌是生产分散蓝56、分散蓝73等一系列分散染料重要中间体。

The ultra-fine disperse black ECO was prepared from traditional disperse black ECO by ball milling, reprecipitation and pressure homogenization. The effects of ratio of dyes and milling media, milling time, ratio of dyes and organic assistants, etc on were investigated.

将普通分散染料黑ECO各组分按比例混合后加入复合分散剂及有机助剂,用球磨机高度分散后滴加到复合分散剂的水溶液中,最后经高压均质机均质后得到超细分散染料黑ECO液体染料。

Different dyeing processes were carried out on polyester-cotton blended fabrics with separated disperse and direct dye ing,and same bath alkaline dyeing with disperse/ direct dye s respectively.

对涤棉混纺织物分别采用分散染料、直接染料染色,以及分散和直接染料碱性同浴染色,测试染色织物的最大吸收波长λm ax和K/S值等指标,以确定涤棉混纺织物用分散和直接染料碱性同浴染色工艺。

The results showed that functional nanometer ITO powders of 30-50nm size with dispersion performance can be prepared. The condition is that indium salt concentration is 88mmol/L, SnO2/In2O3 =5.3wt%, reaction solution PH value is 8, The precursor are thermally reduced at 450 ℃ under hydrogen gas ,at the sametime adding 6at.% KC1 salt to indium tin salts. Thus, satisfactory and stable dispersion of ITO particles in aqueous solution is obtained only through simple mechanical force.

KCl、反应铟盐浓度88mmol/L,掺杂比SnO_2/In_2O_3≈5.3wt%,维持PH值为8的反应条件下制备前驱体,前驱粉体在450℃,氢气气氛煅烧的条件下可生成功能性的具有很好分散性能的ITO粉末,粒径大小为30—50nm,此制备得到的粉体通过简单的机械分散可直接稳定的分散于水、醇介质,若通过分散剂处理后的分散体系可以稳定存在两个月以上。

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