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The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂,甲醇为溶剂的回流提取法来提取植物多酚,用显色反应检识酚羟基;采用紫外分光光度法对多酚粗体物进行总多酚含量的测定;选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌,采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验,并测定其最低抑菌浓度;采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析,根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

In order to detect product\'s quality and to adjust the synthetic conditions, UV and RP- HPLC methods for the determination of the target product were established according to the components of products in the electrosynthesis course, by which target product were able to be simply, fast and accurately determined without separation in advance. And satisfactory results were obtained when they were applied to the determined of the product\'s content.

本研究为检验产品质量,调整合成工艺条件,根据电合成过程中生成物的组成情况,首先建立了无需进行分离就能够简单、快速、准确测定目标产物的紫外分光光度法和反相高效液相色谱法,并将其应用于产品含量的测定,获得令人满意的实验结果。

In 0.015 mol/L NaOH medium, AuCl4(superscript -)reacted with hexadecyl trimethyl ammonium bromide, forming water soluble CTMAB-AuCl4 complex that exhibited a weak absorption peak at 400 nm. In the presence of hydrazine, the reaction produced orange-red nanogold particle and exhibited a surface plasma resonance absorption peak at 520 nm.

在0.015mol/LNaOH介质中,氯金酸根离子AuCl(上标-下标 4与阳离子表面活性剂十六烷基三甲基溴化铵反应生成水溶性的CTMAB-AuCl4缔合物,在400nm处产生一个很弱的吸收峰,当有肼存在时,反应生成橙红色的金纳米粒子,在520nm处出现一个表面等离子体共振吸收峰,从而可实现废水中微量肼的分光光度测定。

These are main problems of eutrophication.In this paper we selected alga that suits to grow under different concentration of nutrition, after selecting seed, domesticating, culturing alga purely in the lab, we gained Hydrodictyon reticulatum and microalga, most of which are Miorocystis and chlorella.

本文选取在不同营养水平条件下适合生长的藻类物种,在实验室进行选种、驯化和纯化培养,得到水网藻和微藻(主要为微囊藻Miorocystis、小球藻chlorella);以实验室培养的生长速度快、生产能力高的水网藻为原料,制备一系列环境友好性光敏物质——叶绿素及其衍生物,运用光敏氧化分光光度法测定活性氧(O_2~-,H_2O_2,·OH,和~1O_2),根据其光敏产生活性氧效率,进行光敏物质的筛选;选用叶绿素铜及其钠盐,以微藻为实验控制对象,以Cu~(2+)作培养对照,在相同光照、营养条件下进行控藻实验。

Analysis on main points for determination of chlorine dioxide by iodometric method ;2. The experiment results show: To measure sulfide in wastewater by iodometric method may have errors because the interferent can not be removed.

用碘量法测定废水中的硫化物,可能因无法消除干扰而使测定结果存在较大误差;对于同一废水样品,当碘量法和亚甲基蓝分光光度法的测定结果存在显著性差异时,可用Pb2半定量法进行判定;对于某些化纤企业的废水,用氢氧化钾-乙醇溶液洗涤沉淀,可消除碘量法测定的干扰。

Surface waxes of the pericarp were observed by scanning electron microscopy; the structure and composition of cell wall were studied using light microscopy, transmission electron microscopy and Fourier transform infrared microspectroscopy respectively; the changes of calcium in the cell wall were determined by atomic absorption and the integrity of cell membrane by conductivity meter respectively.

本论文采用扫描电子显微镜研究果实表皮蜡层的变化,用光学显微镜、透射电子显微镜和傅里叶变换红外光谱仪研究果实细胞壁结构和成分的变化,用原子吸收分光光度计测定细胞壁钙离子的变化,用电导率仪检测果实细胞的完整性。同时测定了果实酚类物质含量、多酚氧化酶(EC 1.10.3.1)活性、过氧化物酶(EC 1.11.1.7)活性,并分析了果实硬度、糖和酸含量等品质指标。

The chemical analysis of N, P and K in organic fertilizer is presented: sample is decomposed by sulfuric acid-hydrogen peroxide and prepared to be a solution. N can be determined by NC-2 model quick N analysis set, P by chinoline molybdic acid method and K by tetraphenylboron potassium, needless of spectral photometer and flame photometer, the method is available when the content of N, P or K is over 0.1% with desired accuracy and precision.

介绍用化学分析方法测定有机肥料氮、磷、钾的含量,即样品经硫酸-过氧化氢消化后,制备待测溶液,分取待测溶液用NC-2型快速定氮仪测定氮,用磷钼酸喹啉重量法测定磷,用四苯硼酸钾重量法测定钾,不需使用分光光度计和火焰光度计,适宜一般复混肥料厂采用,对含氮、磷、钾分别达0.1%以上的样品均可用本法测定,方法的准确度和精密度能满足生产的要求。

The molecular structure was clarified by IR, which revealed the existence of ether bonds. The content of tartaric acid and unreacted maleic acid were detected by spectrophotometer. The effect of some factors on the yield of ESA and scale inhibition efficiency of PESA was investigated.

利用红外光谱表征了该产物结构,表明分子链中含有醚键;利用紫外-可见分光光度法测得体系内副产物酒石酸和未反应的马来酸的含量,并系统地研究了各因素对中间产物环氧琥珀酸钠的产率和最终产物聚环氧琥珀酸钠阻垢性能的影响。

The nutritional components of the whole dry pitaya flower were analyzed by ICP-MS,spectrophotometric method,chemical analysis method and gravimetric method.

采用ICP-MS、分光光度法、化学分析法和重量法对火龙果全花的营养成分进行了分析,结果表明,每100 g火龙果花干制品中水分、蛋白质、粗纤维、粗脂肪、总糖、灰分的含量分别为:7.12、11.80、10.01、1.15、23.61、7.43 g;火龙果花中钾的含量相当高,为13 772.07 mg/kg;镁、钙和磷元素的含量丰富,分别达到:1 788.34、1 745.44、307.90 mg/kg;铁、锰、锌等必需微量元素也较丰富。

Methods Spectrophotometry was used to study the activity of PLAP in the presence and absence of L Leu. PLAP relative activity was calculated according to the absorbance variation.

方法应用分光光度法分别测定有L-Leu和无L-Leu存在下的酶活力,根据其活力变化求出酶的相对活力;用双倒数作图法,确定L-Leu对PLAP的抑制类型并求出其抑制常数;同时也观察了pH对抑制作用的影响。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。