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分光光度测定法

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A method for the determination of high-content of copper in copper materials by flame atomic absorption spectrophotometry using sub-sensitive spectral line at 249.20 nm is reported in this paper.

中文摘要:利用铜的原子吸收光谱次灵敏线249.20 nm,并适当偏转燃烧器角度,原子吸收分光光度法测定含铜物料中的高含量铜。

To determine Chromium in drinking water with flow injection analysis method and spectrophotography respectively and find out the statistical significance between the two methods.

目的 运用流动注射分析法及二苯碳酰二肼分光光度法对生活饮用水中六价铬进行测定,比较它们结果差异是否存在有统计学意义。

Methods Flow Injection Analysis Method and spectrophotography were applied to detect Chromium content in drinking water; hygienic statistics was used to test the different value means and total means; analysis and comparison were made on the detection result.

对20份水分别用流动注射仪分析法和二苯碳酰二肼分光光度法测定其六价铬的含量。运用卫生统计学,检验配对设计中的差值均数与总体均数,对2种方法的检测结果进行分析比较。

METHODS Compare the assaying content of Inosine by using titrimetric method of periodic acid with spectrophotometric method.

用高碘酸滴定法测定肌苷的含量并与紫外分光光度法作对比。

The ability of magnesium trisilicate to adsorb tetracycline and its relation to pHof the medium have been investigated UV-spectrophotometrically.

本文应用紫外分光光度法研究了体外三硅酸镁吸附四环素的能力及其与介质 pH 的关系;并应用尿药法研究了三硅酸镁及其在表面活性剂和枸橼酸的存在下对四环素吸收的影响;测定了三种不同处方的四环素混悬剂的相对生物利用度并进行了有关参数的统计比较。

The results showed that Kaidimycin was chemically neutral, macrocylic polylactones, stable and liable to dissolve into water and pyridine, slight to dissolve into methanol, ethanol and N-butanol, difficult to dissolve into ethyl acetate, acetone, benzene and chloroform. Chemical reaction of functional group of Kaidimycin showed that it had glycoside, amino acid and aldehyde, no reducing sugar, polypeptide and phenol.

凯地菌素属中等极性的、中性抗生素,极性纸层析结果与多烯类抗生素的纸层析结果相似:易溶于水、吡啶,微溶于甲醇、乙醇、正丁醇,不溶于乙酸乙酯、丙酮、苯、三氯化碳;对高温、光照和紫外处理有很好的稳定性;官能团反应试验结果发现,凯地菌素可能含有糖苷键、氨基酸伯氨基和醛基,不含有还原糖、多肽和酚基,高锰酸钾、浓硫酸反应与多烯大环内酯类抗生素的特性相似;并且依据纯品,采用生物法和分光光度法对摇床发酵液进行了效价的测定。

This paper determined the content of urinary MTs and cadmium in different crowd by RLS method using alizarin red and graphite furnace atomic absorption spetrophotometry respectively.

用本文建立的茜素红共振光散射法和石墨炉原子吸收分光光度法分别测定了不同环境人群尿中MTs和Cd的含量。

Methods The pyrogllol auto-oxidation was adopted to produce superoxide anion O(superscript - subscript 2; the system H2O2/Fe(superscript 2+) was used to produce hydroxy radical through Fenton reaction; and spectrophotometry was used to detect the clearing functions of drugs with different concentrations against O(superscript - subscript 2) and OH.

采用邻苯三酚自氧化法产生超氧阴离子自由基O(上标-下标 2,采用H2O2/Fe(上标 2+)体系通过Fenton反应产生羟自由基,用分光光度法分别测定不同浓度的药物对O(上标-下标 2)是和OH的清除作用。

Methods L9(34) orthogonal test was conducted to evaluate the effects of ethanol concentration, ethanol consumption, extraction duration, and extraction time on the extraction by using the content of four kinds of sanchinosides and the content of the total flavonoids in axillary choerospondias fruit that were included in the recipe of Danxinshu capsules. HPLC and ultraviolet spectrophotometry were used in the assay of cumarin.

分别采用高效液相色谱法和紫外分光光度法测定方中三七的3种皂苷的总含量及广枣的总黄酮的含量,以两者含量的综合评分为指标,采用正交实验考察乙醇浓度、乙醇用量、提取时间、提取次数4个因素对提取效果的影响。

Sodium arsenite group and sodium arsenate group were made by 300 mg/L per day of sodium arsenite and sodium arsenate respectively. The mice were sacrificed after 10 months for liver function and pathologic examination. The expression of MMp-8, TIMP-2, Col-Ⅰ、Col-Ⅲ mRNA were detected with real time flourescence quantitative PCR. The result was controlled with 18s.

亚砷酸钠组和砷酸钠组给予普通饲料和砷溶液。10个月后处死小鼠,血清进行肝功能检测;苏木素-伊红染色部分肝组织;Trizol-酚-氯仿一步法提取小鼠肝组织总RNA,紫外分光光度法测定总RNA浓度及纯度,实时荧光定量PCR法测肝组织中MMP-8、MMP-2、Col-Ⅰ、Col-Ⅲ mRNA的表达,以18S基因作为质控。

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