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分光光度法

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METHODS:Aminopyrine and antipyrine in Antongding injection were determined by radial basis fuction neural network UV spectrophotometry,barbitial was determined with absorbance substraction technique.

采用径向基函数紫外分光光度法同时测定安痛定注射液中的氨基比林和安替比林,并结合吸光度减技术测定巴比妥。

The drying process of chrome liquor was studied. The structure and property of chrome complex reducing by alcohol were analysed and tokened by many present well-rounded separation and analysis methods such as IR, UV-Vis Spectrum, IEC and pH potentiometry. Application tests of chrome tanning agents were conducted and tanning methods of tanning at high pH were studied. A systematic study was conducted on high alkalinity chrome tanning agents application in leather making process and possibility of clean chrome tanning was discussed.

本文系统地研究了多种小分子醇与重铬酸盐之间的氧化-还原反应,对反应过程进行了认真的剖析;对铬鞣液的干燥过程进行了研究;用红外光谱法、紫外及可见分光光度法、离子色谱法以及pH电位滴定法等多种比较成熟的现代分离分析方法相结合,对醇还原铬配合物的结构与性能进行了分析与表征;对铬鞣剂的鞣革性能进行了应用实验,研究了醇铬鞣剂在高pH值下的鞣制方法,并就高碱度铬鞣剂在制革过程中的应用进行了系统研究,探讨了用其实施清洁化铬鞣的可能性。

The drying process of chrome liquor was studied. The structure andproperty of chrome complex reducing by alcohol were analysed and tokened by manypresent well-rounded separation and analysis methods such as IR, UV-Vis Spectrum,IEC and pH potentiometry. Application tests of chrome tanning agents wereconducted and tanning methods of tanning at high pH were studied. A systematic studywas conducted on high alkalinity chrome tanning agents application in leather makingprocess and possibility of clean chrome tanning was discussed.

本文系统地研究了多种小分子醇与重铬酸盐之间的氧化-还原反应,对反应过程进行了认真的剖析;对铬鞣液的干燥过程进行了研究;用红外光谱法、紫外及可见分光光度法、离子色谱法以及pH电位滴定法等多种比较成熟的现代分离分析方法相结合,对醇还原铬配合物的结构与性能进行了分析与表征;对铬鞣剂的鞣革性能进行了应用实验,研究了醇铬鞣剂在高pH值下的鞣制方法,并就高碱度铬鞣剂在制革过程中的应用进行了系统研究,探讨了用其实施清洁化铬鞣的可能性。

The level of PGE was assayed by spectrophotometer; Meanwhile, 3H-TdR incorporation method was used to detect ConA- and LPS- induced splenocytes proliferation and the production of interleukin-1 and IL-2. The content of antibodies to CII was determined by ELISA method. Pathological examination of articulus tissue was observed by Hematoxylin-eosin stain.

检测小鼠足爪肿胀度并对炎症进行评分;测定胸腺指数和脾脏指数;~3H-TdR参入法检测胸腺、脾淋巴细胞增殖反应;~3H-TdR参入法测定白细胞介素-1(interleukin-1,IL-1)和IL-2水平;ELISA法测定小鼠血清中抗CⅡ抗体含量;分光光度法检测足爪局部产生的前列腺素水平;HE染色法对关节组织作病理检查。

The comparison analysis of nitrate nitrogen determination is conducted with the same standard solution and natural water samples by two methods of spectrophotometric method with phenol disulfonic acid and ultraviolet spectrophotometer.

采用同一标准液和天然水样用酚二磺酸光度法和紫外分光光度法测定硝酸盐氮,进行比对分析,同时调查云南省内用此两种方法密码样考核的情况。

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂,甲醇为溶剂的回流提取法来提取植物多酚,用显色反应检识酚羟基;采用紫外分光光度法对多酚粗体物进行总多酚含量的测定;选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌,采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验,并测定其最低抑菌浓度;采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析,根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

Analysis on main points for determination of chlorine dioxide by iodometric method ;2. The experiment results show: To measure sulfide in wastewater by iodometric method may have errors because the interferent can not be removed.

用碘量法测定废水中的硫化物,可能因无法消除干扰而使测定结果存在较大误差;对于同一废水样品,当碘量法和亚甲基蓝分光光度法的测定结果存在显著性差异时,可用Pb2半定量法进行判定;对于某些化纤企业的废水,用氢氧化钾-乙醇溶液洗涤沉淀,可消除碘量法测定的干扰。

The CFb in blank control group was added with IMDM containing 10% FBS and those in Ang Ⅱcontrol group with Ang Ⅱ.The CFb in the 3 test groups were induced with Ang II,then added with Tau at dosages of 40,80 and 160 mmol/L respectively. Determine the proliferation of CFb by MTT method, the collagen content by oxyproline kit, the transforming growth factor- TGF-β1 (TGF TGF-β1) content by ELISA, the cell cycle by flow cytometer, the CFb NO content by nitrate reductase method, the iNOS activity by spectrophotometry, and the expression of iNOS protein by IFA.

胰酶消化法分离培养新生大鼠CFb,用Ang Ⅱ诱导促进其增殖,采用MTT法检测细胞增殖;羟脯氨酸试剂盒检测胶原含量;ELISA法测定转化生长因子β1(TGF-β1)蛋白的含量;流式细胞仪检测细胞周期;硝酸还原酶法、分光光度法和免疫荧光法检测CFb NO含量、一氧化氮合酶活性和iNOS蛋白的表达。

The recent development of the analysis of trace arsenic is reviewed,including spectrophotography,atomic-absorption spectrometry,atomic-fluorescence spectrometry and electro-chemical determination.

综述了近年来痕量砷的测定方法,主要包括分光光度法、原子吸收光谱法、原子荧光法、电化学方法、X-射线荧光法、电感耦合等离子体质谱法等,并展望了联用技术在砷形态的分离和测定的应用前景

Methods Cancer tissues of 68 carcinoma ventriculi patients and side tissues of the control group were collected; Se、Zn、Cu、Fe、Cd were determined with atomic absorption spectrophotometry and fluorophotometry.

收集68例胃癌患者癌组织及癌旁组织,用原子吸收分光光度法和荧光光度法测定Se、Zn、Cu、Fe、Cd。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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