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Third, sodium sulfoxylate formaldehyde is a kind of bleaching powder used in industry, which is prohibited from adding to food. In this part, we take it as an object to study, by using ion chromatography instrument which is equipped with autech DS-PLUS?

本章利用荧光光度法和紫外吸收分光光度法研究了核酸对环丙沙星-Tb~(3+)体系的荧光增强效应及其影响因素,探讨了其作用机理,提出了环丙沙星-Tb~(3+)配合物与核酸的作用模型,并建立了DNA的选择性测定方法,并将其运用于合成样与血清中DNA含量的测定。

One method of preparation new membrane materials was presented with putting multi-wall carbon nanotube and carboxylic multi-wall carbon nanotube in collodion solution.

分别将碳纳米管和羧基化碳纳米管均匀分散在火棉胶溶液中,采用流涎法制备出碳纳米管复合膜;并用分光光度法对样液、滤液中的间苯二酚和茜素红的吸光度进行了对比测定,以考察膜的吸附性能。

One method of preparation new membrane materials was presented with putting multi-wall carbon nanotube and carboxylic multi-wall carbon nanotube in collodion solution. Carbon nanotubes complex filtering membranes can be obtained by salivate method. Resorcin and alizarin red can be percolated using new membrane individually.

分别将碳纳米管和羟基化碳纳米管均匀分散在火棉胶溶液中,采用流涎法制备出碳纳米管复合膜;并用分光光度法对样液、滤液中的间苯二酚和茜素红的吸光度进行了对比测定,以考察膜的吸附性能。

We first studied the interaction mechanism of Erythrosin B with proteins by spectrophotometry and fluorospectrophotometry, calculated their binding number, binding constants and binding site, and estimated their binding type.

分光光度法和荧光光度法结合,首次研究了四碘荧光素与蛋白质的作用机理,计算了结合数、结合常数和结合位置,判断出结合类型。

A spectral-correction-integral- photometry method and its application in the measurement of the luminous flux of blue LEDs are introduced.

介绍了一种光谱校正积分光度法及其在蓝光LED光通量测量中的应用,对测量中的各种不确定因素作了理论分析,并与单纯的分光光度法和积分光度法的不确定度作了比较,证明该方法可实现极高的测量精度。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小,进行综合分析,确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量,测定条件:加入100ml浓度为8.0±0.1%的氢氧化钠,在恒温水浴中煮沸回流6h;采用溶剂萃取法测定JOB-1C中TATB的含量,选择TATB饱和的二甲基甲酰胺为萃取溶剂,用G4坩埚式过虑器进行萃取分离;采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量,通过实验确定了多波长组合:λ=267nm,275nm,283nm,291nm,299nm;朗波—比耳定律的适用范围为PNP浓度:0.005~0.025mg/ml,HMX浓度:0.06~0.30mg/ml;在测定波长下,对PNP、HMX标准溶液的吸光度—浓度进行线性回归,由回归曲线的斜率得出PNP、HMX的吸收系数;根据朗波—比耳定律和吸光度加和性原理,在测定波长下,对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归,回归曲线的斜率即为混合溶液中PNP的浓度。

In order to provide some scientific data for judging biological toxicity and bioavailability caused by heavy metals in sediments in Guilin, China, for the first time, the authors sampled sediments in different water areas in Guilin, and determined AVS by P-Amino dimethyl aniline dihydro chloride photometry through a set of acidification-ventilation-absorption AVS reaction unit, determined copper, lead, zinc, cadmium and nickel with tomic absorption spectrophotometry, mercury and arsenium with atomic fluorescence, and cipangopaludina cathayensis was selected as the tested species for bioavailability experiment.

首次以桂林水系沉积物为研究对象,通过酸化-吹气-吸收装置,用对氨基二甲基苯胺光度法测定沉积物中AVS含量,用原子吸收分光光度法测定SEM和间隙水中Cu、Pb、Zn、Cd、Ni含量,用原子荧光法测定Hg、As含量。

A novel method for determination of benzoyl peroxide with spectrophotometry was developed. Inclusion ratio of β cyclodextrin to dibenzoy peroxide and benzoic acid is obtained with spectrophotometry.The mechanism of the inclusion was studied,too. The results showed that β-CD react with dibenzoyl peroxide to form a 1:1 or 2:1 host-guest complex, with the apparent formation constants of 5.0× 10~2and 2.5× 10~4 , respectively.β-CD reacts with benzoic acid to form a 1:1 host-guest complex with the apparent formation constant of 6.9 × 10~2 after the dibenzoyl peroxide was reduced by hydroxyl ammonium chloride.

建立了用β环糊精测定过氧化苯甲酰的分光光度法,并测定了β环糊精与过氧化苯甲酰和苯甲酸的包结比,随着β-CD浓度的增大,可与BPO分别形成1:1或2:1的包容络合物,包结常数分别为5.0×10~2和2.5×10~4,与苯甲酸形成1:1的包容络合物,包结常数为6.9×10~2;由于包结物的吸光度值比过氧化苯甲酰的吸光度值大大增加,建立了一种当β-CD存在下,在水溶液中测定过氧化苯甲酰的方法。

The comparison analysis of nitrate nitrogen determination is conducted with the same standard solution and natural water samples by two methods of spectrophotometric method with phenol disulfonic acid and ultraviolet spectrophotometer.

测定水中硝酸盐氮含量有多种方法,主要包括酚二磺酸光度法、锅柱还原法、戴氏合金还原法、离子色谱法、紫外分光光度法和电极法等。

Methods After the sample of Fenneropenaeus chinensis, Litopenaeus vannamei, Liza haematocheila, Acanthogobius hasta, Mactra veneriformis, Aloidis laevis, Ostrea denselamellosa and Fenneropenaeus chinensis was digested with concentrated hydrochloric acid, the lead content in marine products was measured by fluorimetric method and the results were compared with dithizone spectrophotometry.

采用湿式消解法对中国对虾、南美白对虾、梭鱼、矛尾刺虾虎鱼、四角蛤蜊、光滑兰蛤、密鳞牡蛎、中国对虾样品进行处理,采用浓盐酸作溶剂,荧光分光光度法直接检测铅含量,并与双硫腙光度法的测定结果进行比较。

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