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凝胶剂

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Transmission Electron Microscope and other properties testing results show that the complex emulsifier system is the crucial influence factor of the polymerization process and the properties of products. It may influence the coagulum content and reaction rate of the polymerization process, the performance, particle diameter,viscosity, electrolyte stability and storage stability of the emulsion products and the contact angle of the film.The initiator mainly influences the coagulum content and reaction rate.The acrylic monomers mainly influence the solid content, Minimum Film Formation Temperature of the emulsion and the Glass Transition Temperature of the film.The organic silicone monomer mainly influences the water absorption of the film.The reaction temperature mainly influences the reaction rate and conversion.The stirring intensity mainly influences the coagulum content of the polymerization process.

透射电镜等性能测试结果显示:复合乳化剂体系是硅丙共聚乳液的聚合过程及产品性能的主要影响因素,它可以对聚合过程的凝胶率、反应速率以及乳液的外观、粒径、粘度、耐电解质稳定性及贮存稳定性,还有乳液涂膜的接触角等造成不同程度的影响;引发剂主要影响反应速率和凝胶率;丙烯酸酯单体主要影响到乳液的固含量、最低成膜温度以及涂膜的玻璃化转变温度,有机硅单体主要影响涂膜的吸水率等;聚合反应温度主要影响乳液的反应速率和转化率等;搅拌强度主要是影响到聚合过程的凝胶率。

The comparative tests of the rheological properties between Alcalase induced soy coagulum and Magnesium Chloride/Calcium Chloride induced soy coagulum shows that the former one has higher hardness,lower strength,and 10 times higher adhesiveness of the latter one.

对Alcalase与盐类凝固剂氯化镁和氯化钙凝固豆乳的主要流变学性质比较发现,Alcalase凝固豆乳的硬度比盐类凝固剂大,凝胶强度比盐类凝固剂低,粘附性比盐类凝固剂高10倍以上,使凝胶较粘,乳清不易排出。

A new method using gel permeation chromatographic cleanup followed by high performance liquid chromatography-tandem mass spectrometry has been established for quantitative determination of Maleic hydrazide,Prowl and butralin residues in tobacco.

建立了用凝胶渗透色谱净化-液相色谱-串联质谱分析烟草中3种抑芽剂残留的方法。卷烟中的待测抑芽剂组分用V∶V=1∶1超声提取后通过凝胶渗透色谱净化;凝胶色谱柱为Biobeads S-X3玻璃柱(50 g,400 mm×25 mm),流动相为V∶V=1∶1溶液,流速5 mL/min;收集第10~25 min流出的液体用液相色谱色谱-三重四极杆串联质谱仪测定。

Chitosan had been modified by polyacrylate sodium, glularaldehyde, and NaBH4, respectively, which afforded three kinds modified chitosan: polyacrylate sodium modified chitosan (CIS- PA4) chitosan bead and pentamethylene diamido crosslinked chitosan bead (CTSB- G- Hy). The adsorption properties of CTS-CTSB and CTSB-G-Hy were studied by L25(56) orthogonal experimental design. They show high adsorption activities for Pb2+ in solution. The highest removal efficiency of Pb2+ for CTS-PA4, CTSB and CTSB-G-Hy is 94%, 96% and 93%, respectively. The results showed the adsorption property of CTSB is the highest. The CTSB- G- Hy has good mechanical property, acid-resistance and alkali-resistance.

第二部分壳聚糖的改性及其对水溶液中铅离子的吸附性能研究以壳聚糖为原料制备了三种改性吸附剂——聚丙烯酸钠改性壳聚糖(CTS——PA_4)、珠状壳聚糖凝胶树脂和戊二氨交联珠状壳聚糖凝胶树脂,着重考察了CTSB—G—Hy的制备条件,并考察了三种吸附剂吸附6.3mg/L铅离子水溶液中铅的最佳使用条件,结果表明对CTS—PA_4而言当pb~(2+)溶液的pH在4~6.5之间,吸附剂用量为5g/L,吸附时间为1h时pb~(2+)去除率高于94%,CTS—PA_4可在酸性条件下使用,在碱性条件下依然有效但处理效果较差;CTSB对pb~(2+)具有很好的吸附能力吸附剂用量为5g/L,吸附时间为1h时处理效果极佳,pb~(2+)去除率高于96%;CTSB—G—Hy对pb~(2+)具有一定的吸附能力,吸附剂用量为3g/L,吸附时间为1.5h时处理效果最佳,Pb~(2+)去除率高于93%,而且CTSB—G—Hy的机械强度高,耐酸碱性强,可在较宽的pH范围内使用。

The effects of dosage of main components and reaction temperature on the gelling time and gel strength were examined.

由速溶纳米硅粉、缓凝剂、胶凝剂为主要组分制备了耐高温低成本调剖剂,考察了其主要组分用量及反应温度对调剖剂成胶时间和凝胶强度的影响。

In the study of modern preparations of TCM PVA,as film material of membrane and pellicles,is very promising owing to its easy forming and excellent toughness.

PVA作为巴布膏剂和凝胶剂的高分子基质,既能承载药物,又能改善制剂的使用和工艺性能,是一种优良的药物载体。

Diigel is a quick-drying gel that is odorless when dry, and is aailable in conenient, indiidual-use packets.

Diigel是一种快速干燥的凝胶剂,在干后无味,方便的单次用量包装。

Objective To observe the effect of Doxycycline slow-release on periodontitis therapy.

目的 观察多西环素缓释凝胶剂治疗牙周炎的临床疗效。

RESULTS: 20% and 70% ethanol greatly improved the percutaneous permeation of tetracaine ...

含 70 %乙醇的丁卡因凝胶剂具有较强的透皮作用和局麻效果

Research from the stability of the polymer gel system,this paper carried out the foll...

从研究聚合物凝胶体系稳定性出发本文主要开展了以下工作;(1)从聚合物类型(PHPAM、AP-P4和KYPAM-2)、分子量、水解度方面研究了聚合物凝胶体系的成胶性能,实验结果表明,KYPAM-2在60℃、80℃下与乙酸铬交联剂、70℃和90℃下与有机酚醛交联剂形成的凝胶体系30天粘度保留率85%—94%,而AP-P4聚合物在相同条件下形成的凝胶体系30天粘度保留率80%—90%;中、低水解度(15-25%)聚合物形成的凝胶稳定性较好(30天粘度保留率9036-94%)。

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