凝胶

(1) to deliver the Levonorgestrel (0.ml/kg,5mg/m) and Mifepristone gelatum (0.1ml/kg,5mg/ml) per cutem to the rat respectively and measure the serum concentration of levonorgestrel、mifepristone、estradiol and progesterone at different time by the means of HPLC, radioimmunoassay,chemical separation and atomic absorption spectrophotome.

大鼠皮肤涂抹米非司酮凝胶(0.1ml/kg，5mg/ml)和左炔诺孕酮凝胶(0.1ml/kg，1mg/ml)后的不同时间，利用高效液相色谱法、放射免疫分析法、化学分离与原子吸收分光光度法，测量血清中米非司酮浓度、左炔诺孕酮凝胶以及血清雌二醇、孕酮浓度。

The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

The analysis shows that the molecule chain coupling is the common feature of the two systems.

结果表明：一定条件下聚合物凝胶和疏水缔造合聚合物溶液具有相似的溶液结构和流动特性；胶态分散凝胶在多孔介质中的流动存在转变压力，2组流动实验中疏水缔合聚合物溶液也表现出类似的转变压力，分析认为聚合物凝胶分子链间的联结是化学交联，而疏水缔合聚合物为物理缔合，类似的分子链间联结方式是两种体系有相似流动特性的内在原因。

Result show:the solution,extracted from rat rail tendons,consist mainly of type I collagen;No growth of bacteria in 37℃ thermostatic culture box for 72 hours;Absorbing the height of ultraviolet-spectrophotometry is 230 nm by using flicker photometer examination;Amino acid in type I collagen consist of aminoacetic acid(40 per cent) and proline(14.3 per cent);Under microscope:collagen gel netted constraction consist of original collagen fibril that had been fairly well-distributed and had a quite regular striate lines ;The collagen solution prepared collagen gel matrixes in 37℃ thermostasis for culture cells and also prepared collagen solid film by washing collagen gel with a phosphate solution for plasty surgery materials.

结果：提取液主要为Ⅰ型胶原蛋白；72小时37℃恒温培养箱内培养无细菌生长；紫外分光光度计测定，吸收高峰为230nm；氨基酸成分主要为甘氨酸：占40%，脯氨酸：14.3%。显微镜下见：相互交织的胶原原纤维结构组成的网状结构；纤维均匀，有规则横纹。胶原蛋白液在37℃恒温下，可制成凝胶，用于培养细胞；用磷酸液冲洗胶原蛋白凝胶可成固体片状，制成胶原膜，用作医用材料。

The results showed that the solubility of lotus starch was low, the turgidity was closed to sweet potato starch, accordingly was a restrictive swelling starch. A lower transparency (10.4%) was researched in the lotus-seed starch pastes, condensation speed was faster, but it decreased at acidic or alkaline condition. Stronger freeze-thaw stability and lower gel strength was researched in it. It can be from the Brabender viscosity that the lotus-seed starch has a higher gelatinization temperature (77.1℃), better thermostability, stronger retrogradation, weaker cold viscosity stability.

试验结果表明：莲子淀粉的溶解度较低，膨润力接近甘薯淀粉，属限制型膨胀淀粉；莲子淀粉糊的透明度较低（10.4%），凝沉速度较快，在酸性或碱性条件下凝沉速度减缓；其凝胶具有较强的冻融稳定性和较低的凝胶强度；布拉班德粘度曲线显示，莲子淀粉的糊化温度较高达77.1℃，热稳定性好，凝沉性强，冷粘度稳定性差。

The steps were as follows: Acquiring superant from the culture medium by centrifugation, discarding waste residue by filtration, concentrating by hollow-fiber membrane, treating with salting-out, dialyzing the product of salting-out, treating the dialysate by vaccum freeze dryer, dissolving solid , using the method of gel filtration chromatography with Sephadex G-100/G-75, and proof-test by filter-paper chromatography ,then preparation by thin-layer chromatography was carried out.

建立了分离纯化该物质的有效途径：发酵液离心除菌→抽滤除杂→中空纤维过滤浓缩→盐析→透析→真空冷冻干燥→溶解→交联葡聚糖凝胶Sephadex G-100凝胶分离→交联葡聚糖凝胶Sephadex G-75凝胶分离→纸层析检验→薄层层析制备。

It was considered that the control of the PRD fluid performance and the dosage of flow pattern adjusting agent PF-VIS were the key of the technique. The viscosity of PRD spudding fluid increased rapidly with the decrease of shearing rate, it indicated that it had good sand carrying ability. The spudding fluid was good capacity of high temperature stability under the low shearing rate, its viscosity was much higher than that of traditional drilling fluid, it was beneficial for cutting carrying in big deviated wells and preventing the formation of cutting bed.

认为要控制好PRD弱凝胶钻开液的性能，流型调节剂PF-VIS的加量是关键；PRD弱凝胶钻开液的粘度随着剪切速率的降低而急剧上升，显示了其优良的井壁携砂带砂性能；PRD弱凝胶钻开液体系具有较好的高温稳定性；PRD弱凝胶钻开液体系在低剪切速率的高粘度，大大高于传统聚合物钻井液，有利于在大斜度井携带岩屑以及防止岩屑床的形成。

The main components in soy protein isolate are 7S and 11S globulins. Studiesof papain on 7S, 11S and mixture of the two proteins suggested that 11S is themain component in SPI to form coagulation. 7S coagulation required higher papainaddition than 11S coagulation, while 11S gel's elastic modular was higher than7S gel. The elasticity of mixture depended on the proportion of 11S. Two proteinases were separated from papain by SP-sepharose cation-exchangechromatography.

首先分离出大豆蛋白中的主要组分7S和11S蛋白，将木瓜蛋白酶分别作用于两种蛋白的溶液和不同7S/11S比例的蛋白溶液，结果表明11S蛋白是大豆蛋白中形成酶促凝胶的主要组分；7S蛋白形成凝胶所用的酶浓度高于11S蛋白所用的酶浓度，但11S蛋白形成的凝胶的弹性强度却远高于7S蛋白；在两种蛋白的混合溶液中11S蛋白的比例对凝胶的弹性强度起决定作用。

In this paper, the materials for experiments of montmorillonite are prepared by Xinjiang smectite, In the country, Smectite as raw mineral materials, is done to sublimate to the content of montmorillonite more than 95% up through the experiment, concentrate performance is improved, and met the requirement of medical auxiliary materials; And then adopt the activator , glue to congeal the pharmaceutical and congeal the gummed test and prepare inorganic mineral gel, gel viscidity reaches above 40mPa·s.

本课题试验选用国内蒙皂石储量最大的新疆蒙皂石作为矿物原料，通过加入分散剂高速分散方法来进行提纯处理，使其蒙脱石含量提高到了95%以上，精矿性能得到改善，达到了药用辅料的要求；再采用活化剂、胶凝剂凝胶化试验制备无机矿物凝胶，凝胶粘度达到40mPa·s以上。

Research from the stability of the polymer gel system,this paper carried out the foll...

从研究聚合物凝胶体系稳定性出发本文主要开展了以下工作；(1)从聚合物类型(PHPAM、AP-P4和KYPAM-2)、分子量、水解度方面研究了聚合物凝胶体系的成胶性能，实验结果表明，KYPAM-2在60℃、80℃下与乙酸铬交联剂、70℃和90℃下与有机酚醛交联剂形成的凝胶体系30天粘度保留率85%—94%，而AP-P4聚合物在相同条件下形成的凝胶体系30天粘度保留率80%—90%；中、低水解度(15-25%)聚合物形成的凝胶稳定性较好(30天粘度保留率9036-94%)。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。