凝缩

The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

Finally, in view of the malpractice of traditional pour point depressant, we developed new condensed suspension PPD.

最后，针对传统的降凝剂应用工艺的弊端，开展了新型缩悬浮体降凝剂的研制。

The relationship between the ratio of Ca to Si with shrinkage value was needed to be studied further.The strength of M-AAS was comparatively high, but the flexural strength was regressed in the long term. The compressive and flexural strengthes of 3 days were able to surpass 8MPa and 78MPa, respectively, and compressive strength of 90 days were all around 100MPa, but compared to flexural strength of 28 days, the flexural strength of 90 days was regressed by 19.0%. The high strength property of M-AAS associated with its hydration products and Interfacial Transition Zoo. The main hydration products of M-AAS were microcline and CSH, no calcium hydroxide was found. The coexistence of microcline and CSH worked as micro-aggregate by each other, and no weak ITZ, both resulted in its high strength. The regression of its strength was related to its high shrinkage property, because the crazing caused by shrinkage would decrease the strength, especially the flexural strength.

M-AAS强度较高，但长期抗折强度倒缩。3天抗折和抗压强度分别可超过8MPa和78MPa，90天抗压强度在100MPa左右，但90天抗折强度比28天抗折强度相比低19.0％。M-AAS的高强特性与其水化产物和界面过渡区有关，M-AAS的水化产物主要为微斜长石和CSH凝胶，没有氢氧化钙，微斜长石与CSH凝胶相互填充和配合共同起到强度的作用，M-AAS砂浆中几乎没有发现界面过渡薄弱区。M-AAS的强度倒缩现象与其收缩值较大有关，收缩会引起M-AAS硬化体内部出现微裂缝，使强度下降。

The chemical activating mechanism of UA is that CG can stimulate pozzolanicity more effective than gypsum because of higher solubility and looser crystal structure; but CG has poor property on retardation setting, and this shortage can be solved by mixing with gypsum; CS can offer alkali activity, which can depolymerize silica and aluminum glass, and benefit for other activity methods and overcome the disadvantage of HF on setting time; Sodium sulfate improves early strength greatly but loses the final strength. NF can improve both early and final strengths.

联合激发技术的化学激发机理是，煅烧石膏溶解度高及晶体结构松弛，比天然石膏的活性激发效率高，但降低石膏的缓凝作用，与天然石膏混合既可提高活性又能保持缓凝作用；干法电石渣提供碱激发，促进高钙灰中硅、铝玻璃体解聚，并克服高钙灰对凝结时间的不利影响；硫酸钠虽然早强作用明显，但使后期强度倒缩，NF使各龄期活性都得到提高；磨细的物理激发使高钙灰大颗粒中的CaO和富集碳组分被磨细、分散，活性增加而危害性降低。

Multiple factors participated in the process of secondary brain edema and nerve injuries,such as the hydrostatic pressure during formation of the hematoma and clot retraction, activation of blood coagulation cascade, generation of thrombin,erythrocytolysis and the toxicity of hemoglobin, the activation of the complement system, space-occupying effects, rupture of the blood-brain barrier,secondary ischemia around the hematoma, inflammatory reaction of the neurons around hematoma and cell apoptosis.

脑出血后继发水肿及神经损害有多种因素参与，血肿形成过程中的流体静力压和血凝块的回缩、凝血瀑布的激活、凝血酶的产生、红细胞溶解和血红蛋白的毒性、补体的激活、占位效应、血脑屏障的破坏、血肿周围继发缺血、血肿周围组织神经细胞炎症反应及细胞凋亡等。

In this paper, we designed and synthesized a molecule of compound 1, 2-(benzooxazol-2-yl)-5-4-(3-(benzothiazol-2-yl) phenylamino-6--1,3,5-triazin-2-ylaminophenol, which can only assembled into an organogel upon a short irradiation with ultrasound in toluene-methanol mixed solvent. DSC, XRD and IR were used to detect the properties and mechanisms of the organogel.

本论文中，我们设计合成了一个有机小分子化合物1，4-氨基（2-羟基苯基）苯并噁唑3-氨基苯基苯并噻唑二辛基胺缩三聚氯嗪，研究发现，在甲苯/甲醇=1：2的混合溶剂中，只有利用超声才能使之形成凝胶，加热冷却的方法不能形成凝胶，而形成针状结晶。

Fine chemicals to add auxiliary Series: lubricating oil pour point depressant, calcium zinc magnesium methacrylate, methyl acrylic acid lauryl ester, tetradecane methacrylate ester, methacrylic acid octadecyl ester, a acid ethylene glycol, diethylene glycol methacrylic acid ester, glycidyl methacrylate, the second reduction of three ethylene glycol dimethyl acrylate, acrylic acid lauryl ester, tetradecyl acrylate, octadecyl acrylate, acrylic acid ethylene glycol, diethylene glycol acrylate esters, glycidyl, two shrink three acrylate such as ethylene glycol.

精细化工添加助剂系列：润滑油降凝剂，甲基丙烯酸钙锌镁，甲基丙烯酸月桂酯，甲基丙烯酸十四烷酯，甲基丙烯酸十八烷基酯，甲基丙烯酸乙二醇，甲基丙烯酸二乙二醇酯，甲基丙烯酸缩水甘油酯，二缩三乙二醇二甲基丙烯酸酯，丙烯酸月桂酯，丙烯酸十四酯，丙烯酸十八酯，丙烯酸乙二醇，丙烯酸二乙二醇酯，丙烯酸缩水甘油酯，二缩三乙二醇丙烯酸酯等。

Poly silica hybrids were prepared through polymerization, condensation and sol gel processes of the mixture of methyl methacrylate, poly and a small amount of coupling agent methacryloxylpropyl trimethoxy siliane in tetrahydrofuran.

采用溶胶-凝胶技术，以硅酸钠为原料制备聚硅酸/四氢呋喃溶胶，再与甲基丙烯酸甲酯及少许偶联剂甲基丙烯酰氧丙基三甲氧基硅烷(MPTMS 混合，经聚合、缩合和溶胶-凝胶过程制备了有机/无机两相间有— C—Si—O—键的杂化材料——聚甲基丙烯酸甲酯/二氧化硅(PMMA/Si O2 )。

Folk art's heritage and dissemination from the family to the public and its function from God and the pursuit of self-entertainment become fashionable of experience and economic interests,or even the expression of cultural connotation it also condensed into a symbol of cultural symbols,and these changes Dongba are in the post-modern art in the context of modern encountered by the results,and has shown a mass culture characteristics.

民间艺术的传承与传播由族内转向大众，其功能也由祭神与自娱变为追求时尚化体验和Economic经济利益；甚至它所表达的文化内涵也凝缩成民族文化的象征符号，而这些变化都是东巴艺术在后dangdai现代语境中所遭遇的现代性结果，并呈现出大众文化的特色。

The logic behind this phenomenon is that chromosome condensation prevents the activity of RNA polymerases.

对这一点的解释一直是：染色体凝缩限制了RNA聚合酶的活性，但对芽殖酵母所做的一项研究表明，事实并不是这样的。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了