冰醋酸

Results:All dosage groups of Tou-Yu-Tong Pills could release chronic nerve injury caused by formaldehyde solution; remarkedly inhibit the pain of mice in the formalin test and prolong the latencies of paw-licking. It could significantly diminish pain caused by glacial acetic acid ,reduce the number of the writhing in mice.To the model of migraine ,Tou-Yu-Tong Pills can improve the content of 5-HT in brain tissue of mice ,and ruduce 5-HTAA.

结果 头愈痛丸对福尔马林致小鼠慢性神经性疼痛反应，能明显减少动物舔后足的时间，改善其伤害性疼痛行为反应；对冰醋酸致小鼠扭体反应，能显著延长扭体的潜伏期，减少扭体反应的次数；对小鼠偏头痛模型，能显著升高小鼠脑内5-HT的含量，且降低5-HIAA的趋势。

Two solvent systems which were MeOH -50% MeOH and 95% alcohol - water were studied by the content of salvianolic acid B and salviol ⅡA and the icon of Salvia miltiorrhiza Bge..

采用C18柱，乙腈-0.35%冰醋酸溶液梯度程序洗脱，以丹参酮ⅡA和丹酚酸B含量为指标并结合图谱，综合考察甲醇-50%甲醇、95%乙醇-水两套溶剂系统提取丹参药材的效果。

The bromine value of petroleum products was determined by potential titration in mixed solvents of glacial acetic acid,trichloromethane,methanoland sulfuric acid,this method was compared with indicator titration,the experimental results show the method relative standard deviation is smaller.

以冰醋酸、三氯甲烷、甲醇和1：5的硫酸(体积比为714：134：134：18)作为滴定溶剂，采用电位滴定法测定石油产品的溴值，并与指示剂滴定法进行对比。

ConclusionThese results suggest that WYPE has the preventive and therapeutic effects on gastric ulcer.

此外，该药对小鼠胃肠运动功能有很强的促进作用；能抑制冰醋酸引起小鼠扭体反应。

Under the optimum conditions, the lactobacillus bulgaricus microcapsule was madeby single agglomerate, and precipitated the wall with located in rapeseed oil with 50%ammonium sulfate solution; The preliminary micro-emulsion filtrated, then drawsome microcapsule from the micro-emulsion and progressing the second emul-sification, injecting a mixture with 3% CAP and 1.5% gelatin into the micro-emulsion,and keep the stirring speed 200r/min for 5 minutes, adjusting pH as 3.0 with aceticacid, then desiccating with the spray drier after 30 minutes. At last, got the prodtictof microcapsule powder.

通过最佳乳化条件制备的乳液，采用单凝聚法制备保加利亚乳酸杆菌微胶囊，用50％硫酸铵溶液，使菜籽油中的壁材CAP析出，形成初步的微胶囊，过滤，取上层微胶囊油液，缓慢注入3％CAP和1.5％明胶混合液中，进行第二次乳化，在200r／min的搅拌速度下乳化5min，用冰醋酸调节乳液的pH值至3.0，固化30min，取乳液置于喷雾干燥机中进行喷雾干燥。

Methods by using a broad pH range column(Gemini NX C18,4.6mm×150mm,5μm),basic mobile phase which was[H_2O-ammonia-glacial acetic acid] (96:3.6:0.4)-methanol,the related substances in etimicinsulfate were separated and detected by electrospray ionization and positive ion monitoring,the ESI ion source condition was following: temperature is 350℃,nebulizing pressure is 50 psi,dry gas flow is 10 L /min.some related substances in etimicinsulfate were identified by comparing the retention time in chromatography,~+ spectrum and MS~2 spectrum with reference substances\',the others which haven\'t reference substances were identified or speculated by analyzing their MS~2 fragmentation with the help of a rule summarized from the MS~2 fragmentation of gentamicin C1a,micronomicin and etimicin.Results nineteen related substances in etimicinsulfate were separated and detected.

方法利用宽pH范围的Gemini NX C18(4.6mm×150mm，5μm)色谱柱，在碱性条件下，以[水-氨水-冰醋酸(96：3.6：0.4)]-甲醇(70：30)为流动相，直接分离各组分；并用HPLC-ESI-MS~2检测样品中各组分，质谱条件：ESI离子源，离子源温度350□，雾化室压力50 psi，干燥气流速10 L/min，正离子检测方式；对有对照品的有关物质采用比对有关物质与对照品的色谱保留时间、准分子离子的质荷比及二级质谱方法进行鉴定，无对照品的有关物质，则是先通过解析庆大霉素Cla、小诺霉素、依替米星的二级质谱，对该类化合物的二级质谱裂解规律进行归纳，并以此推测未知新化合物进行结构，再用推测的结构对二级质谱进行解析，如所有的碎片离子均合理解释，表明推测合理。

The organic layer was evaporated and the residue was redissolved by mobile phase.The concentrations of propofol and lidocaine were assayed on a hypersil BDS C18 column with a mobile phase consisting of acetonitrile-methanol-water（10∶60∶30）（including 0.14%n-butyamine 0.1%acetic acid）at a flow rate of 1 mL*min-1 and detected at 220 nm during 1～7 min and at 273 nm during 7～16 min.

氮气吹干有机层，残留物用流动相重新溶解后，用Hypersil BDS C18柱分析，流动相为乙腈-甲醇-水(10∶60∶30)，内含正丁胺0.14%和冰醋酸0.1%，流速为1 mL*min-1，检测波长：1～7 min用220 nm，7～16 min用273 nm。

The optimum conditions were as follows: the volume proportion of water and glacial acetic acid was 4, the reaction temperature was 30℃ and reaction time was 10 minutes.

由此对反应条件加以优化，得出反应的适宜条件是当水和冰醋酸的体积比为4，反应温度为30℃，反应时间为10 min时，收率可达78%。

Methods Anhydrous acetic acid as solvent, 0.1 mol/L perchloric acid as titrant, crystal violet solution as indicator to establish non-aqueous titrations and ODS column as stationary phase, methanol and a mixture of 0.025 mol/L sodium phosphate monobasic and 0.02 mol/L sodium dedecyl sulfate (80:20) adjusted with phosphoric acid to a pH (4.8±0.1J as mobile phase, 220 nm as detective wavelength to establish HPLC-UV method for determination of piperazinylethylestrone drug substance; FMOC-CL as a derivatization reagent, FD as a detector to establish an HPLC method with derivatization and column switching for determination of piperazinylethylestrone in dog plasma.

分别采用无水冰醋酸为溶剂，0.1mol/L高氯酸为滴定液，结晶紫指示液指示终点的非水滴定法和HPLC-UV法测定哌嗪雌酚酮原料药含量；以FMOC-CL为衍生化试剂，采用柱切换柱前衍生化萤光检测的HPLC法测定狗血浆中哌嗪雌酚酮含量。

Sulfuric acid series, hydrochloric acid (AR hydrochloride, CP hydrochloric acid) series, nitric acid, phosphoric acid, boric acid, protopine, soda ash, ammonia, acetic acid, bleaching powder, chloride, alkaline chlorine of aluminum, nickel chloride, nickel sulphate, polyacrylamide, such as hydrogen peroxide.

硫酸系列，盐酸系列，硝酸，磷酸，硼酸，片碱，纯碱，氨水，冰醋酸，漂白粉，聚合氯化铝，碱式氯化铝，氯化镍，硫酸镍，聚丙烯酰胺、双氧水等。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。