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Silicon phthalocyanine dihydroxide was prepared from silicon phthalocyanine dichloride through two methods. The first was alkali treating that meaned silicon phthalocyanine dihydroxide was treated in the ethanol solution containing sodium methylate .The second was acid treating meaned precipitating its solution in concentrated sulfuric acid into ice water. The product yield of the second method was 77.0%, which was higher than the method of alkali treating.

此外将合成的二氯酞菁硅采用两种方法转化为二羟基酞菁硅,第一种方法是碱处理法即将二氯酞菁硅在甲醇钠的乙醇溶液中回流得到,最高收率为53%第二种方法是酸处理法即采用二氯酞菁硅的硫酸溶液在冰水析出的方法转化为二羟基酞菁硅,其中酸溶析出法收率为77.0%。

All experiments were carried out under the dry and oxygen-free argon atmosphere by using standard Schlenk techniques.

在无水无氧和纯的氩气保护下,使用Schlenk技术,用2-(C1CH2) C5H4N·HC1与2当量的C9H7Li在THF中冰水浴反应,以73%的产率得到3-(2-C5H4NCH2)C9H7(1)。

At less than 3 cents a glass, it is a popular means of relieving the heat. Yet if you are not a native, it's best to avoid it: unboiled, it can wreak havoc upon the foreign gut.

在缅甸,如果想要买冰水,就到像这样的摊子,一杯不到三毛,在高温的缅甸很受欢迎,不过如果不是本地人,可别轻易尝鲜,和自己的肠胃过不去,因为这些水都没煮过。

In order to accurately analyze the thermal and mechanical states of subway tunnel constructed by artificial freezing method,the coupled effects of moisture transfer and phase change of ice and water,the generation of cement hydration heat and thermal creep constitutive relationship were taken into account,and a moisture,thermal and mechanical coupled model was established.

为了准确分析地铁隧道人工冻结施工过程中的热力学状况,考虑水分迁移和冰水相变耦合影响以及水泥水化热的生成,采用热蠕变本构建立了地铁隧道人工冻结施工的水热力耦合分析模型。

The upper layer is modern river deposit; the middle layer is relative thick,mainly consisting of icewater deposit,colluvial deposit and deluvium as well as barrier dam accumulation; the bottom layer is formed by ancient river bed deposit and boulder rocks.

河谷覆盖层是由一套不同时期、不同成因类型的沉积物相互迭置的结果,由表及里宏观上可分为3层:表层为现代河流相堆积;中间主要为以冰水、崩积、坡积、堰塞堆积与冲积混合为主的加积层,厚度相对较大;底部主要为古河床的冲积、冰水漂卵砾石层。

Cups (20 ounces) unbleached all-purpose white flour or white bread flour, plus more as needed1 teaspoon granulated sugarCorn oil, canola oil or other flavorless vegetable oil or oil spray for coating dough

在4杯( 20盎司)没经过漂白的白面粉或白面包粉里加上1茶匙砂糖,2又3 / 4茶匙的盐,在面包机器的酵母里加入2杯冰水,如果需要玉米油,菜籽油或其他无味植物油或沾了油的面团的话,可以稍微加上一点。

For the demands of precooling and cold storage for keeping fruits, vegetables and flowers fresh, a new humid-cool system of water drenching air-cooler was designed based on the analysis on the characteristic of the current type of ice water humid-cool system and the synthesis performance were tested.

针对果蔬、花卉等的预冷、冷藏湿冷保鲜技术过程要求,在综合分析了目前流行的冰水湿冷系统特点的基础上,设计了淋水式冷风机湿冷系统,测试了该系统的综合性能。

Because the primary production were mostly distributed in the bottom of ice and the surface water,the role of ice water interface in the ecosystem was very important.

光辐照度由于在冰水界面的量值仅为冰表入射光的不足5.3%至低于1%,成为水中产量最为可能的限制因子。

Across the rain-drenched roadway was the town park: five acres of grass, giant elm trees and, tonight, an ankle-deep covering of cold water.

泥泞的马路对面是小城公园:5英亩的草地,粗大的榆树,还有,齐脚深的冰水。元培翻译世博陪同口译热招中。。。

The method comprises: adding 4-(3,4-dichlorophenyl)-1-tetralone and solvent at a ratio of 1:(3-4) into a three-necked flask with a stirrer, heating under stirring until 4-(3,4-dichlorophenyl)-1-tetralone is completely dissolved, heating to 60-100 deg.C, refluxing for 0.5-2 h, cooling the filtrate to -5-10 deg.C, filtering, recrystallizing to obtain refined 4-(3,4-dichlorophenyl)-1-tetralone, and drying at 40-80 deg.C to obtain dry 4-(3,4-dichlorophenyl)-1-tetralone.

该方法的步骤是:在带搅拌的三颈瓶中依次加入4-(3,4-二氯苯基)-1-萘满酮和溶剂,溶剂与4-(3,4-二氯苯基)-1-萘满酮的L∶W为3~4∶1,将上述4-(3,4-二氯苯基)-1-萘满酮及混合精制溶剂搅拌下升温,使4-(3,4-二氯苯基)-1-萘满酮全部溶解,升温至60~100℃,回流0.5-2h;滤液用冰水冷却至-5~10℃,过滤,所得物料再用上述方法进行一次重结晶得到精品4-(3,4-二氯苯基)-1-萘满酮,40~80℃干燥后即得到干品4-(3,4-二氯苯基)-1-萘满酮。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。