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The reactants were managed to be colloidal by reaction control and using appropriate nucleating agents. Acerate HA crystal obtained under different conditions was sintered to obtain the nano-HA granule with a diameter of 1-56 nm.

材料:采用磷酸二氢钙和氢氧化钙中和反应构造体系,通过控制反应条件,适量加入形核剂,使反应物成为胶体状态,在不同反应条件下得到针状羟基磷灰石纳米晶体,再进行烧结除处理,得到羟基磷灰石纳米粒子,直径为1~56 nm。

A series of p-toluene sulfonylamido acetacylhydrazone derivatives were synthesized from p-toluenesulfonyl chloride which reacted with glycine to get the intermediate p-toluene sulfonylamido glycine, then through the esterification, hydrazinolysis to afford another intermediate p-toluene sulfonylamido acethydrazide, which condensed with different aldehydes to obtain the target compounds that were characterized by IR, 1H NMR, 13C NMR spectra and elemental analysis.

魏太保 ;冷艳丽;王永成;张建辉;张有明*摘要:以对甲苯磺酰氯为原料,通过与氨基乙酸反应得到中间体对甲苯磺酰氨基乙酸,再经酯化、肼解得到对甲苯磺酰氨基乙酰肼,然后与相应的醛缩合得一系列对甲苯磺酰胺基乙酰腙类化合物。其结构经元素分析, IR, 1H NMR和13C NMR确证。

Preparation of the lateral chain-4-benzyloxy-3-hydroxy butyronitrile is introduced as the substrate, the REFORMATSKY reaction is performed, then obtains the dicarbonyl ester, in the structure of which containing a chiral hydroxyl group, then performs the chiral reduction, take off the benzyl group after the protection reaction with acetonylidene,then obtains the lateral chain by oxidation.

手性侧链醛的合成:采用-4-苄氧基-3-羟基丁腈作为底物,通过REFORMATSKY反应缩合得到含有手性羟基的二羰物酯,再手性还原,丙酮叉保护后氢解脱苄,最后氧化得到侧链醛。

Taking advantage of better solubility and thermal stability of ionic liquid, the ionic liquid supported acetylacetone catalyst can be simply recycled by water washing or vacuumdistillation.The background of this research is renovation on the traditional oxidation reactions by green chemistry principle.

根据离子液体支载催化剂的两个特性:在水中良好的溶解性和具有很好的热稳定性,在反应结束后通过水洗涤或精馏的方法,很方便的对催化剂进行了回收再利用。

In this study, six patients with piebaldism had removal of achromic epidermis via appropriately set erbium:YAG laser followed by application of autologous cultured epidermal grafts on the recipient bed. The 3,4-dihydroxyphenylalanine reaction was used to determine melanocyte content, and a semiautomatic image analysis system calculated the percentage of repigmentation.

在这项研究中,六名通过适当能量设定之铒-雅克雷射,移除色素缺乏表皮的白斑病患,在受体皮肤上以自体培养表皮移植的应用加以追踪。3.4-羟基苯丙胺酸反应用以测定黑色素细胞内容,并以半自动影像分析系统计算再色素沉淀的百分比。

Eight novel N,N′-naphthalene acyl substituted aromatic acylamino thiocarbamides(Ⅱ1~Ⅱ8) were synthesized from aryl acylhydrazine and α-naphthalene acyl isothiocyanate, which was obtained by the reaction of potassium thiocyanate with α-naphthalene acyl chloride obtained from 2-naphthylacetic acid and thionyl chloride in anhydrous benzene.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与芳基酰肼进行加成反应,合成8种新型N,N′-萘乙酰基取代芳乙酰胺基硫脲类化合物(Ⅱ1~Ⅱ8)。

An original exhausted-air reclaiming technical method has been presented, that is to say, the discharging chamber's pressure-air is reclaimed into the air tank through the additory of the exhausted-air reclaiming control devices which can be considered as the mid-pressure air supply for reutilization in order to realize the aim to save energy.

论文提出了一种创新性的气缸排气能量回收技术途径:通过附加排气回收控制装置将气缸排气腔的有压空气回收到储气罐中,并作为中压空气源再利用,以实现节能。

To deal with various risks in the production of space,local governments have to cease the monopolization in land requisition and expropriation,and establish the balance of interests between correlative groups and national institutions in the circulation of lands.To deal with risks in the games of new society,local governments must adjust the systems and policies concerned,and avoid just scratching the surface of a problem.To deal with risks in reallocation of social resources and social administration concerned with policy output,many local governments already have material condition to effectively break them,and the key is to improve their administerial skills in policy making and implementation.To deal with risks in vicious competition between city governments in urbanization,which are actually the manifest of malfunction of market mechanism,local governments must put the centralization mechanism into full play,and strengthen the social check and balance mechanism,in order to effectively regulate market mechanism and realize the organic interactions between social units,democracy,and market.

要破解地方政府在空间生产中风险重重的局面,必须改变政府在土地征用征收上的独裁专断格局,完善土地流转中各个相关利益群体间的权利均衡以及国家机构间的权力均衡机制;地方政府在新型社会博弈中的风险,也需要相关制度与政策的调整,不能停留在治标不治本的层次;在社会资源再分配与社会管制等政策输出方面的风险,许多地方政府已经具备了有效化解的物质条件,主观上提高政策制定与执行的行政技能是解决此类问题的关键;我国城市政府在发展地方经济推进地方城镇化中的恶性竞争风险,本质上是市场机制失灵的一种表现,必须通过充分运用集权机制、强化社会制约机制从而有效规制市场机制,实现科层、民主、市场三种机制的良性对接,政府、社会、企业三种力量的有机互动,才能解决。

The concentrations of CODcr and NH4+ vary from low to high, then from high to low in the process of refuse leaching, that is to say that there are three phases which are aerobian decomposition, facultative aerobian and anaerobian decomposition;(3)The time of landfill reaching to stabilize under the condition of filtration, for landfill of Jinqianpu, is at least 86 years if CODcr is regarded as a index; but is about 98 years when NH4+ as an index;(4)The column leaching experiment simulated is carried on interactivity between leachate and different lithologic characters, water-bearing media of different thickness. Some parameters can be determined by calculation, such as, the retained factor and hydro-chemical transportation rate of pollutants in suspended media, which quantitatively analyse the suspended soil capability of components purification and the pollution scope of water bearing media.

垃圾淋滤过程中和经历了一个由低到高、再由高到低的过程,即垃圾填埋过程中经历了好氧分解、兼性好氧分解及完全厌氧分解等三个阶段;(3)垃圾组分在淋滤条件下分解达到稳定的时间,对于金钱堡垃圾填埋场,若以作为考核指标,填埋场达到稳定化时间至少需要86年;若以作为考核指标,则填埋场达到稳定化至少需98年的时间;(4)对垃圾浸泡液与不同岩性、不同厚度含水层介质之间的作用进行了土柱淋滤模拟试验,通过计算污染质在包气带介质中运移的阻滞因子和水化学迁移率等参数,定量地描述了包气带土层对污染质的净化能力和污染范围。

In term of emergency leave, thecompany has regulation that staff should inform the direct supervisorby SMS or telephone first and submit annual leave application aftercoming back to work, no such record of annual leave reject found in OA.

关于紧急请假,公司有相关规定,可以先通过电话,短信等方式请假,回来工作后再补假,在OA系统中我们亦没有查到相关的补假记录和补假被拒记录。

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Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特,那个是爱朗。

Articulate the aims, objectives and key aspects of a strategic business plan.

明确的宗旨,目标和重点战略业务计划。