再胶凝

The carbonaceous alcosol and the silica alcosol were prepared respectively by using aqua-mesophase and tetraethoxysilane as starting materials. Then the two alcosols were mixed and dried in open air and under supercritical fluid conditions to form binary carbonaceous-silica xerogel powders and aerogel powders respectively.

以正硅酸乙酯和炭质水性中间相为原料，分别制得了炭质醇溶胶和硅醇溶胶，将二者进行混合后再利用常压干燥法和超临界流体干燥法分别制备了二元炭质-二氧化硅干凝胶和气凝胶粉末。

The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

Direction: Massage Shampoo de Mentha into wet hair, lather and rinse thoroughly, Shake for use!

使用方式：使用前请先将冻脑精油配方洗发凝胶摇一摇，再取适量洗发凝胶按摩头皮及头发，3至5分钟后清洗乾净即可。

Scanning electron microscopy,transmission electron microscopy,circular dichroism and small-angle X-ray diffraction were used to analyze the aggregation mode of CSG in the organogel phase.A hierarchical self-assembly model was proposed to explain the transition from molecular to primary and secondary structure.It is shown from our results that CSG can aggregate into a micellar fibril nanostructure with high length-to-width ratio which is bundled and entangled to form a three-dimensional(3D) network that immobilize the fluid component probably by surface tension.Moreover,sol-gel polymerization of tetraethoxysilane was carried out using CSG in the gel phase.

通过扫描电镜(ScanningElectron Microscopy，SEM)、透射电镜(Transmission Electron Microscopy，TEM)、圆二色谱(Circular Dichroism，CD)和小角X—射线衍射仪(Small-angle X-rayDiffraction，SAXRD)考察CSG分子自组装行为结果表明，CSG形成的聚集体具有多级结构：首先CSG通过手性堆叠自组装形成直径在9—10nm的细纳米纤维，这些细的纳米纤维再以不规则的六方堆积的方式进行排列，构成直径在40—100nm的粗纳米纤维(即细纳米纤维的&捆束&)，最后粗纳米纤维互相粘连形成三维网络状结构，使有机溶剂&固定&，从而形成凝胶；以CSG有机凝胶为模板，四乙氧基硅烷为前体，通过溶胶—凝胶聚合的方法制备了直径大约为100nm的二氧化硅纳米管。3。

Using New Zealand rabbit ears cartilage makes chondrocyte suspension, Fibrinogen was mixed with D-hank's makes a final fibrinogen concentration of 50mg/ml mixture solution, then chondrocytes resuspend with fibrinogen solution, chondrocytes-seeded fibrinogen was mixed with thrombin (25U/ml in 40mM calcium choride) to make chondrocytes/fibrin glue polymer. Pluronic F-127 was mixed with D-hank's makes a final Pluronic F-127 concentration of 400mg/ml mixture solution, then chondrocytes resuspend with Pluronic F-127 solution to make chondrocytes/Pluronic F-127 polymer. The chondrocyte concentrations was 10 million chondrocyte/ml of polymer.

为确定纤维蛋白凝胶与Pluronic F-127在注射方式形成组织工程化软骨过程中的优劣，我们进行了如下实验：应用新西兰大白兔耳软骨获取软骨细胞并体外培养，纤维蛋白原应用D-hank's液配制为50mg/ml，然后以纤维蛋白原溶液重悬软骨细胞，再与40mM的氯化钙配制的25U/ml凝血酶混合形成软骨细胞—纤维蛋白凝胶复合物；Pluronic F-127应用D-hank's液配制为400mg/ml，同样用PluronicF-127溶液重悬软骨细胞而形成软骨细胞—Pluronic F-127凝胶复合物。

The sol gel materials are prepared through the hydrolysis and polycondensation of tetramethoxy silicane.

溶胶 凝胶技术是将金属醇盐等原料配制成均质溶液，在饱和条件下经水解缩聚等化学反应，生成物聚集成溶胶，再经蒸发、干燥转变为凝胶，这是一项在低温下制备纳米粉末或多孔玻璃的技术[1] 。

Poly silica hybrids were prepared through polymerization, condensation and sol gel processes of the mixture of methyl methacrylate, poly and a small amount of coupling agent methacryloxylpropyl trimethoxy siliane in tetrahydrofuran.

采用溶胶-凝胶技术，以硅酸钠为原料制备聚硅酸/四氢呋喃溶胶，再与甲基丙烯酸甲酯及少许偶联剂甲基丙烯酰氧丙基三甲氧基硅烷(MPTMS 混合，经聚合、缩合和溶胶-凝胶过程制备了有机/无机两相间有— C—Si—O—键的杂化材料——聚甲基丙烯酸甲酯/二氧化硅(PMMA/Si O2 )。

PAA/PVA IPN hydrogels were prepared by a sequential method by which acrylic acid firstly. polymerizes and cross-links in PVA/water solution with UV irradiation,then PVA physical cross-linked hydrogels are formed in cross-linked PAA networksby freezing-thawing. The orthogonal test design method was used to optimize theexperimental conditions based on the mechanical and swelling properties of thehydrogels. The effect of the PAA and crosslinking agent contents on the microscopicmorphology of the PAA/PVA IPN xerogel was investigated by transmission electronmicroscopy, and on the mechanical properties of the hydogels was studied bymeasurements of mechanical properties.

针对水凝胶强度、生物相容性和刺激响应性的需要，选择了以PVA和PAA为复合水凝胶的基本分子结构；采用顺序IPN方法制备PAA／PVA IPN水凝胶，即将单体丙烯酸与PVA溶液共混，AA经紫外光辐射聚合交联在PVA溶液中形成PAA化学交联网络，再经冰冻—解冻循环过程在PAA网络内形成PVA物理交联网络。

The rheological behaviours of sweet potato starch paste are explained better by Cross equation than Power Law...

如果淀粉糊的浓度足够，就在冷却时转换成凝胶，这种凝胶是由糊化的淀粉颗粒被包埋在高聚物再结晶整合的网

In this paper, the materials for experiments of montmorillonite are prepared by Xinjiang smectite, In the country, Smectite as raw mineral materials, is done to sublimate to the content of montmorillonite more than 95% up through the experiment, concentrate performance is improved, and met the requirement of medical auxiliary materials; And then adopt the activator , glue to congeal the pharmaceutical and congeal the gummed test and prepare inorganic mineral gel, gel viscidity reaches above 40mPa·s.

本课题试验选用国内蒙皂石储量最大的新疆蒙皂石作为矿物原料，通过加入分散剂高速分散方法来进行提纯处理，使其蒙脱石含量提高到了95%以上，精矿性能得到改善，达到了药用辅料的要求；再采用活化剂、胶凝剂凝胶化试验制备无机矿物凝胶，凝胶粘度达到40mPa·s以上。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。