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Experimental process: jing and 3- methyl -2- methyl ethyl ketonesynthesizes by the benzene zong; Again the glacial acetic acidcatalysis produces 2, 3, 3 - trimethyl - 3H - yinduo; Again has thealkylate response production yinduo iodide after the methyl iodide;The iodide takes off molecular HI under NaOH to become freejier thealkali; Adds 5 - nitryls salicylic aldehydes in the ethyl alcohol forthe solvent under if to respond finally produces 6 '- the nitryl yinduolin spiral benzene and pinan; Through the infrared spectrum andthe ultimate analysis irrevocably proved its structure, and studiedthe annulus with to open the annulus the light to send changes colorthe performance, explained in different solvent medium ultravioletabsorption spectrometry solvent effect, and the comparisondiscoloration the response speed number difference, finally mixed itadds to the methyl methacrylate, the peroxidation benzoin formyl in the plexiglass, tested 6 '- the nitryl yinduolin spiralbenzene and pinan in the glass fatigue resistance, thethermostability.
实验过程:由苯肼和3-甲基-2-丁酮合成腙;再冰醋酸催化生成2 ,3 ,3—三甲基—3H—吲哚;再经过碘甲烷发生烷基化反应生成吲哚碘化物;碘化物在NaOH下脱去一分子HI成为费歇尔碱;在乙醇为溶剂下加5-硝基水杨醛与其反应最后生成6'—硝基吲哚啉螺苯并吡喃;通过红外光谱和元素分析确证其结构,并研究了环体与开环体的光致变色性能,解释了在不同溶剂介质中紫外吸收光谱的溶剂效应,并比较褪色反应速率数的差异,最后将其掺加到甲基丙烯酸甲酯,过氧化二苯甲酰有机玻璃中,测试6'—硝基吲哚啉螺苯并吡喃在玻璃中的抗疲劳性、热稳定性。
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Time domain signal is transformed to the frequency domain signal by FFT. Dispersion curve is obtained from phase angle that is calculated by the frequency spectrum analysis. A compound dispersion curve is obtained from the dispersion curves intervale, and the representative dispersion curve is used to evaluate dimensions and quality of soil grouting body.
由FLAC所得不同点位的速度历时透过快速傅立叶转换后,得到频率域讯号,再经过频谱分析计算其相位角,得到其频散曲线,由不同间距的频散曲线集合成复合频散曲线,再绘制成一"代表性"频散曲线,以评估灌浆体品质及范围。
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The present invention adopts the technical proposal of adopting ZSM-5 mesoporous molecular sieve raw powder with a silicon-aluminum mol ratio SiO2Al2O3 of 20 to 1000 and a weight percentage of 20 to 100 percent as well as at least one caking agent selected from SiO2, clay and Al2O3 to extrude, tablet or spray into shape; then treating for 1 to 8 hours by 0.1 to 3 mol/l of at least one ammonium liquor from ammonium nitrate, ammonium chloride or ammonium sulphate or 0.1 to 8.5 mol/l of at least one acid liquor from muriatic acid, nitric acid, vitriol or acetic acid under a temperature of 20 to 90 DEG C; then using steam to treat for 2 to 15 hours under the temperature condition of 400 to 700 DEG C; using a liquor of 0.1 to 3mol/l selected from at least one of oxalic acid, citric acid or maleic acid under a temperature condition of 20 to 90 DEG C to dip for 2 to 5 hours to obtain the modified molecular sieve catalyst, thus better solving the problems.
本发明通过采用硅铝比SiO2/Al2O3为20~1000重量百分比计20~100%的ZSM-5介孔分子筛原粉与余量的选自SiO2、粘土或Al2O3中至少一种粘结剂挤条、压片或喷球成型;再经过0.1~3摩尔/升选自硝酸铵、氯化铵或硫酸铵中的至少一种铵溶液或0.1~8.5摩尔/升选自盐酸、硝酸、硫酸或乙酸中的至少一种酸溶液在温度20~90℃下处理1~8小时;然后在温度为400~700℃条件下水蒸汽处理2~15小时;再用0.1~3摩尔/升选自草酸、柠檬酸或马来酸中至少一种在温度为20~90℃条件下浸渍2~5小时得所需改性分子筛催化剂的技术方案较好地解决了该问题,可用于甲醇转化制丙烯的工业生产中。
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A method for eliminating the internal oxide structure in the gas-phase carbon-nitrogen osmosis of gear features that the CCL4 is added to the kensene as carburizer and then is decomposed to generate Cl2 for reducing the oxide, the ammonia gas as nitrizing agen passes through the cylinder of silica gel or granular calcium chloride for adsorbing residual water vapour and then through the cylinder of 5A molecular sieve for adsorbing residual O2, and the resistance wire is wound on igniting pipe at furnace top to prevent the NH4Cl in exhausted gas from being condensed.
本方法采用在气体渗碳剂煤油中,加入6~8%的CCl 4 ,使共渗炉内的CCl 4 分解出新生的Cl 2 ,使已形成的合金元素内氧化物还原;在渗碳剂氨气入共渗炉前,先经过硅胶瓶或桶及粒状氯化钙瓶或桶过滤,吸附掉氨气中的残留水蒸汽,再经过5A分子筛瓶或桶吸附掉氨气中的残留氧;在靠近炉顶位置的点火管周围缠绕带瓷环的电阻丝,靠电阻丝的副带加热,使排气中的NH 4 Cl不冷凝结块等措施实现内氧化组织的消除。
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Then the extract was distributed between dichloromethane and water, and the organic part was then subjected to HSCCC for the isolation of chromone constituents.
以芦荟全叶为原料,经过一系列的预处理手段,从脱色剂活性炭中获得芦荟色酮粗提物,再经过溶剂分配和富集后采用高速逆流色谱对其中的色酮成分进行分离纯化。
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High-speed countercurrent chromatography is reported for the preparative isolation and purification of a chromone from aloe vera. The crude extract was obtained by a series of pretreatment of aloe vera leaves and extracted from decolorizing active carbon with methanol.
以芦荟全叶为原料,经过一系列的预处理手段,从脱色剂活性炭中获得芦荟色酮粗提物,再经过溶剂分配和富集后采用高速逆流色谱对其中的色酮成分进行分离纯化。
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So because of that, they need to take that bitumen through one more process so that it can be refined, and they take it through a process that will transform it to what's called synthetic crude oil or synthesised bitumen.
正因为如此,他们就需要让这些沥青再经过一道加工,这样才适合提炼。经过这道工序后,沥青就转变成了合成原油,或者叫合成沥青。
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The super high DP cototn linters pulp using cleaning produce technology, with the raw material cotton linters. After dry cleaning,alcoline,hydrogen peroxide cooking, beating, bleaching and pulping process, the products would be in roll or sheet size.
超高聚合度特种棉浆是利用清洁生产技术,以棉短绒为原料,经过干式除杂、碱---过氧化氢清洁蒸煮工艺制浆,再经过打浆、漂白、通过抄粕机抄造成型的卷状或片状产品。
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R12 on the ozone layer due to the destruction of the requirements of the developed countries for environmental protection from 1996 to start using refrigerant R134a Automotive Air-conditioning and the construction of air-conditioning at home in a similar, it is often installed in the compressor engine, and with a belt drive, the condenser installed in the car in front of the radiator, and evaporator in the car inside, and work out from the evaporator of low pressure gaseous refrigerant flows through a high-pressure high-temperature gas compressor After cooling condenser cooling tube cooling into the low-temperature high-pressure liquid, through the desiccant dryers and storage of buffer, and then to a more stable flow of pressure and flow expansion valve, the final expenditure and the flow of relief evaporator.
由于R12对大气臭氧层的破坏,出于环保的要求发达国家从1996年开始改用R134a做制冷剂汽车空调的构造和家用的分体空调类似,它的压缩机往往是安装在发动机上,并用皮带驱动,冷凝器安装在汽车散热器的前方,而蒸发器在车里面,工作时从蒸发器出来的低压气态致冷剂流经压缩机变成高压高温气体,经过冷凝器散热管降温冷却变成高压低温的液体,再经过贮液干燥器除湿与缓冲,然后以较稳定的压力和流量流向膨胀阀,经节流和降压最后流向蒸发器。
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The study showed that silver grass particleboard was made by the processing of crushing, flaking, particle drying, UF resin sizing, pre-pressing and hot-pressing. The performance indexes of the production could meet the related national standards.
根据研究表明:荻草经过一次粉碎、刨片加工后得到的荻草刨花干燥后,通过施加脲醛树脂胶,再经过预压和热压等工序,试验生产的荻草刨花板,其物理力学性能指标均达到了相关标准的要求。
- 推荐网络例句
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Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".
歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。
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This is Kate, and that's Erin.
这是凯特,那个是爱朗。
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Articulate the aims, objectives and key aspects of a strategic business plan.
明确的宗旨,目标和重点战略业务计划。