再热

After the as-cast Ti-Al-Nb-W-B alloys being hot isostatic pressed and annealed, then they were heat treated at 1295℃ for 10 h.

将铸态Ti-Al-Nb-W-B合金经过热等静压和均匀化热处理后，再在1295℃保温10h。

This thesis sets up a new method to synthesize stereoselectively ?ra玸--2,5-disubstituted tetrahydrofurans by introducing two alkyl groups in 3-C and 5-C of lactol, flash decomposition and hydrogenation.

本文独创新的合成方法：以-乳醇，即-4，10-二氧杂三环[5.2.1.0~(2，6)]-癸-8-烯-3-醇为原料，在其3-位和5-位先反向引入两个取代基，再经过热分解和催化加氢反应，高立体选择性地合成反式-2，5-二取代四氢呋喃。

The key problem is to synthesize high stereoselectively trans- 2,5- disubstituted tetrahydrofurans. This thesis sets up a new method to synthesize stereoselectively ?ra玸--2,5-disubstituted tetrahydrofurans by introducing two alkyl groups in 3-C and 5-C of lactol, flash decomposition and hydrogenation.

本文独创新的合成方法：以-乳醇，即-4，10-二氧杂三环[5.2.1.0~(2，6)]-癸-8-烯-3-醇为原料，在其3-位和5-位先反向引入两个取代基，再经过热分解和催化加氢反应，高立体选择性地合成反式-2，5-二取代四氢呋喃。

The method is characterized in that:(1) the reflux of the 2-[N, N- 2amino]-3-cyano-group-4-thiopheneacetic-5-carboxylic acid tetra ester is carried out in the proper sodium hydroxide aqueous solution of alcohol for 5h to 6h and the pH value is kept over 10 during hydrolysis;(2) the ethanol of 20 per cent to 60 per cent is added and then the strontium chloride aqueous solution with 2times to 2.5times molal weight is directly added, precipitates the crystal, is filtered and dried;(3) water is added to carry out the reflux and the little salt packed in the crude product is removed, and the product is collected through heat filtration.

其特征在于：①将2--3-氰基-4-羧甲基噻吩-5-羧酸四酯在适量氢氧化钠水醇溶液中回流5～6小时，水解过程保持pH值10以上；②然后再加入20-60％乙醇，随后直接加入2-2.5倍摩尔量氯化锶水溶液，析出结晶，过滤，晾干；③加水回流，除去粗品中包裹少量盐，热过滤，收集产品。

The properties of turbulence which characterized as the movement of vortexes influenced the heat and mass transfer, propagation of flame in the combustion process deeply, at the same time, the turbulent combustion based on the turbulent flow coupled with the intense chemical reactions, meanwhile, the heat releasing and the transfer of species concentration cause the nonnegligible effects on the turbulence and its structure.

以涡运动为特征的湍流的性质对燃烧过程中传热、传质和火焰传播都具有重要的影响；同时，湍流燃烧过程则是在湍流流动基础上再耦合以强烈的化学反应，其间由于燃烧造成的热释放、组份浓度的迁移等同样会对湍流流场产生不可忽视的作用。

The coarse needle-like or nubby Al9FeNi phase existed in the cast microstructure of high content Fe and Ni alloy 2618(2#). After hot extrusion, it was broken into coarse multi-angle Al9FeNi particles. The contents of Fe and Ni have no effect on aging characteristic and the hardness of the alloy after aging.

含锆的高铁、镍2618合金经熔体高温过热处理后(4#)，在合金铸态组织中获得均匀细小的针片状Al_9FeNi相，热挤压后获得均匀细小的颗粒Al_9FeNi相；弥散Al_3Zr粒子的存在可使2618合金得到细小的再结晶晶粒组织，该合金既可获得较高的高温强度，还可获得较高的延伸率。

As described previously,hot working is defined as plastically deforming the metallic material at above the recrystallization temperature.

如前所述，热变形被定义为金属材料在再结晶温度以上的塑性变形。

Based on 26B4APBN monomer, polyamic acid was obtained by polymerization with pyromellitic dianhydride, and further imidized into polyimide film by heating process.

由二胺单体和均苯四甲酸二酐进行聚合得到26B4APBN/PMDA聚酰胺酸，再经热亚胺化得到聚酰亚胺薄膜；测试了该薄膜的接触角，讨论了单体分子结构对聚合物接触角的影响。

A series of polyimide/talc composite films with different contents of talc were prepared via thermal imidization of in-situ polymerized poly/talc solutions based on pyromellitic anhydride, 4,4'-oxydianiline and talc.

用原位聚合法合成一系列不同滑石粉含量的聚酰胺酸／滑石粉溶液，再将其热酰亚胺化制备出聚酰亚胺／滑石粉复合薄膜。

For the first time we synthesized nanoscale metal hydrides of lanthanum, neodymium, samarium, dysprosium, and ytterbium with high efficiency under mild condition by complexometric catalysis instead of traditional preparation at high temperature and high pressure. It is for the first time that we synthesized lanthanide organic compounds with catalysts or initiating agents at atmosphere and ambient temperature,and some of them are new compounds. Nanometric lanthanide metal powders are prepared by thermal decomposition of the compounds in vacuum. Differently from the traditional method, size of the products prepared by our method is less than 40nm, and the activity of the reaction is very high. They are pyrophoric at atmosphere. They can make some reactions without activity or low activity show extremely high activity .We investigated influent regulations of methods, conditions to scale and special surface.

我们首次成功地用络合催化等方法取代需在高温高压下进行的传统方法，在温和条件下高效率地合成出纳米尺寸镧、钕、钐、镝、镱的金属氢化物；首次在常压常温的条件下，通过催化、引发等方法合成镧系金属有机化合物，再将其真空热分解成功地制备了纳米尺寸的镧、钕、钐、镝、镱等金属粉末；与传统方法不同，这些方法得到的产品基本颗粒尺寸小于 40 nm，遇到空气燃烧，具有极高的化学反应活性，使原来活性很低甚至观察不到活性的反应大幅度提高反应速率和产率；考察了制备方法、制备条件等因素对晶粒尺寸、比表面积大小等的影响规律。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐